Low-level detections of sudan I, II, III and IV in spices and chili-containing foodstuffs using UPLC-ESI-MS/MS

Journal of Agricultural and Food Chemistry

Volumn 61, Issue 9, 2013, Pages 2284-2289

  Schummer, Claude ^a   Sassel, Jeannine ^a   Bonenberger, Pascale ^a   Moris, Gilbert ^a  

^a LABORATOIRE NATIONAL DE SANTÉ   (Luxembourg)

Author keywords

fast peaks; LC MS MS; nonhomogeneous distribution; spices; Sudan dyes

Indexed keywords

CROSS CONTAMINATION; FAST-PEAKS; LC-MS/MS; LIQUID-LIQUID EXTRACTION; LOW CONCENTRATIONS; NON-HOMOGENEOUS DISTRIBUTION; QUANTIFICATION LIMIT; SUDAN DYES;

AZO DYES; BLENDING; SPICE;

FOOD PRODUCTS;

1-PHENYLAZO-2-NAPHTHOL; AZO COMPOUND; COLORING AGENT; NAPHTHOL DERIVATIVE; OIL SCARLET; SCARLET RED; SUDAN I; SUDAN II;

ARTICLE; CHEMISTRY; ELECTROSPRAY MASS SPECTROMETRY; EUROPEAN UNION; FOOD ANALYSIS; FOOD CONTAMINATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LAW; METHODOLOGY; PEPPER; REPRODUCIBILITY; SPICE; TANDEM MASS SPECTROMETRY;

AZO COMPOUNDS; CAPSICUM; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; COLORING AGENTS; EUROPEAN UNION; FOOD ANALYSIS; FOOD CONTAMINATION; LEGISLATION, FOOD; NAPHTHOLS; REPRODUCIBILITY OF RESULTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; SPICES; TANDEM MASS SPECTROMETRY;

EID: 84874913890     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf400602a     Document Type: Article

References (24)

1. Pardo, O.; Yusà, V.; León, N.; Pastor, A. Development of a method for the analysis of seven banned azo-dyes in Chili and hot Chili food samples by pressurised liquid extraction and liquid chromatography with electrospray ionization-tandem mass spectrometry Talanta 2009, 78, 178-186
2. Calbiani, F.; Careri, M.; Elviri, L.; Mangia, A.; Pistarà, L.; Zagnoni, I. Development and in-house validation of a liquid chromatography- electrospray tandem mass spectrometry method for the simultaneous determination of Sudan I, Sudan II, Sudan III, and Sudan IV in hot Chili products J. Chromatogr. A 2004, 1042, 123-130
3. Rebane, R.; Leito, I.; Yurchenko, S.; Herodes, K. A review of analytical techniques for determination of Sudan I-IV dyes in food matrixes J. Chromatogr. A 2010, 1217, 2747-2757
4. Puoci, F.; Garreffa, C.; Iemma, F.; Muzzalupo, R.; Spizzirri, U. G.; Picci, N. Molecularly imprinted solid phase extraction for detection of Sudan I in food matrices Food Chem. 2005, 93, 349-353
5. Ertas, E.; Özer, H.; Alasalvar, C. A rapid HPLC method for determination of Sudan dyes and Para Red in red Chili pepper Food Chem. 2007, 105, 756-760
6. European Food Safety Authority, Opinion of the Scientific Panel on Food Additives, Flavourings, Processing Aids and Materials in Contact with Food on a request from the Commission to Review the toxicology of a number of dyes illegally present in food in the EU. EFSA J. 2005, 263, 1-71
7. International Agency for Research on Cancer, Monographs on the Evaluation of Carcinogenic Risks to Humans, Volume 99. Available at http://monographs. iarc.fr/ENG/Monographs/vol99/mono99.pdf.
8. Rapid Alert System for Food and Feed (RASFF), Available at http://ec.europa.eu/food/food/rapidalert/indexen.htm/ (accessed Sept 13, 2012).
9. Hoenicke, K. Detection of Low Amounts of Sudan Dyes and other Illegal Dyes in Food and Oleoresins. Analytical Artefact or Cross-Contamination? Eurofins, Available at http://www.aoaceurope.com/katrinhoenicke.pdf (accessed Sept 13, 2012).
10. Fukuji, T. S.; Castro-Puyana, M.; Tavares, M. F. M.; Cifuentes, A. Fast determination of Sudan dyes in chilli tomato sauces using partial filling micellar electrokinetic chromatography J. Agric. Food Chem. 2011, 59, 11903-11909
11. Zhang, Z.; Xu, S.; Li, J.; Xiong, H.; Peng, H.; Chen, L. Selective solid-phase extraction of Sudan I in chilli sauce by single-hole hollow molecularly imprinted polymers J. Agric. Food Chem. 2012, 60, 180-187
12. Yan, H.; Gao, M.; Qiao, J. New ionic liquid modified polymeric microspheres for solid-phase extraction of four Sudan dyes in foodstuff samples J. Agric. Food Chem. 2012, 60, 6907-6912
13. Qi, Y. H.; Chong, W. S.; Zheng, Y. L.; Zhang, Y. J.; Wang, J. P. Production of the polyclonal antibody against Sudan 3 and immunoassay of Sudan dyes in food samples J. Agric. Food Chem. 2012, 60, 2116-2122
14. Mölder, K.; Künnapas, A.; Herodes, K.; Leito, I. "Fast peaks" in chromatograms of Sudan dyes J. Chromatogr. A 2007, 1160, 227-234
15. Ng, C. K.; Tanaka, N.; Kim, M.; Yap, S. L. A rapid and sensitive analysis method of Sudan Red I, II, III & IV in tomato sauce using ultra performance LC-MS/MS. Waters Poster. Available at http://www.waters.com.
16. Van Tran, K.; Young, M. S.; Neue, U. Effective SPE strategies for LC-MS determination of Sudan dyes in chili products. Waters Poster. Available at http://www.waters.com.
17. Kowalski, J.; Vernon Bartlett, C.; Wittrig, B. Analysis of Sudan I, Sudan II, Sudan III and Sudan IV using LC UV and LC MS. Restek Poster. Available at http://www.restek.com.
18. Stuart, B.; Walker, M.. Analysis of illegal dyes in Paprika powder by LC-MS/MS. LGC Limited. 2006. Available at http://www.governmentchemist.org.uk/ (accessed Aug 29, 2012).
19. Ma, M.; Luo, X.; Chen, B.; Su, S.; Yao, S. Simultaneous determination of water-soluble and fat-soluble synthetic colorants in foodstuff by high-performance liquid chromatography-diode array detection-electrospray mass spectrometry J. Chromatogr. A 2006, 1103, 170-176
20. Mazzotti, F.; Di Donna, L.; Maiuolo, L.; Napoli, A.; Salerno, R.; Sajjad, A.; Sindona, G. Assay of the Set of All Sudan Azodye (I, II, III, IV, and Para-Red) Contaminating Agents by Liquid Chromatography-Tandem Mass Spectrometry and Isotope Dilution Methodology J. Agric. Food Chem. 2008, 56, 63-67
21. International Union of Pure and Applied Chemistry. Harmonized guidelines for internal quality control in analytical chemistry laboratories. Pure Appl. Chem. 1995, 67, 649-666.
22. Liu, S.; Zhang, X.; Lin, X.; Wu, X.; Fu, F.; Xie, Z. Development of a new method for analysis of Sudan dyes by pressurized CEC with amperometric detection Electrophoresis 2007, 28, 1696-1703
23. Sun, H.; Wang, F.; Ai, L. Determination of banned 10 azo-dyes in hot chili products by gel permeation chromatography-liquid chromatography- electrospray ionization-tandem mass spectrometry J. Chromatogr. A 2007, 1164, 120-128
24. Lecomte, M. Noir Soudan B-Noir Soudan III. Available at http://users.skynet.be/Champignons-passion/main.htm (accessed Feb 5, 2013).