Beneficial effects of microwave-assisted heating versus conventional heating in noble metal nanoparticle synthesis

ACS Nano

Volumn 6, Issue 11, 2012, Pages 9433-9446

  Dahal, Naween ^a   García, Stephany ^a   Zhou, Jiping ^b   Humphrey, Simon M ^a  

^a UNIVERSITY OF TEXAS AT AUSTIN   (United States)

^b The University of Texas at Austin   (United States)

Author keywords

ligand exchange; microwave synthesis; palladium nanoparticles; platinum nanoparticles; polyol method; rhodium nanoparticles; seeding and growth; shape control

Indexed keywords

LIGAND EXCHANGES; MICROWAVE SYNTHESIS; PALLADIUM NANOPARTICLES; PLATINUM NANOPARTICLES; POLYOL METHODS; RHODIUM NANOPARTICLES; SHAPE CONTROL;

HEATING; MICROWAVE HEATING; MICROWAVES; NANOPARTICLES; OLEFINS; PLATINUM; PRECIOUS METALS; RHODIUM; TRANSMISSION ELECTRON MICROSCOPY; VAPORS;

SYNTHESIS (CHEMICAL);

METAL NANOPARTICLE;

ARTICLE; CHEMISTRY; CONFORMATION; CRYSTALLIZATION; HEATING; MACROMOLECULE; MATERIALS TESTING; METHODOLOGY; MICROWAVE RADIATION; PARTICLE SIZE; RADIATION DOSE; RADIATION EXPOSURE; SURFACE PROPERTY; ULTRASTRUCTURE;

CRYSTALLIZATION; HEATING; MACROMOLECULAR SUBSTANCES; MATERIALS TESTING; METAL NANOPARTICLES; MICROWAVES; MOLECULAR CONFORMATION; PARTICLE SIZE; RADIATION DOSAGE; SURFACE PROPERTIES;

EID: 84870414684     PISSN: 19360851     EISSN: 1936086X     Source Type: Journal    
DOI: 10.1021/nn3038918     Document Type: Article

References (64)

1. Barnard, A. S.; Lin, X. M.; Curtiss, L. A. Equilibrium Morphology of Face-Centered Cubic Gold Nanoparticles >3 nm and the Shape Changes Induced by Temperature J. Phys. Chem. B 2005, 109, 24465-24472
2. Cuenya, B. R. Synthesis and Catalytic Properties of Metal Nanoparticles: Size, Shape, Support, Composition, and Oxidation State Effects Thin Solid Films 2010, 518, 3127-3150
3. Shultz, M. D.; Reveles, J. U.; Khanna, S. N.; Carpenter, E. E. Reactive Nature of Dopamine as a Surface Functionalization Agent in Iron Oxide Nanoparticles J. Am. Chem. Soc. 2007, 129, 2482-2487
4. 2(101) Nanobelts J. Am. Chem. Soc. 2010, 132, 6679-6685
5. Hammer, B. Special Sites at Noble and Late Transition Metal Catalysts Top. Catal. 2006, 37, 3-16
6. -3 Torr to Liquid Interfaces Phys. Chem. Chem. Phys. 2007, 9, 3500-3513
7. Zhou, W. P.; Lewera, A.; Larsen, R.; Masel, R. I.; Bagus, P. S.; Wieckowski, A. Size Effects in Electronic and Catalytic Properties of Unsupported Palladium Nanoparticles in Electro-oxidation of Formic Acid J. Phys. Chem. B 2006, 110, 13393-13398
8. Semagina, N. V.; Bykov, A. V.; Sulman, E. M.; Matveeva, V. G.; Sidorov, S. N.; Dubrovina, L. V.; Valetsky, P. M.; Kiselyova, O. I.; Khokhlov, A. R.; Stein, B. et al. Selective Dehydrolinalool Hydrogenation with Poly(ethylene oxide)- Block -Poly-2-vinylpyridine Micelles Filled with Pd Nanoparticles J. Mol. Catal. A 2004, 208, 273-284
9. Thomas, J. M.; Johnson, B. F. G.; Raja, R.; Sankar, G.; Midgley, P. A. High-Performance Nanocatalysts for Single-Step Hydrogenations Acc. Chem. Res. 2003, 36, 20-30
10. Astruc, D.; Lu, F.; Aranzaes, J. R. Nanoparticles as Recyclable Catalysts: The Frontier between Homogeneous and Heterogeneous Catalysis Angew. Chem., Int. Ed. 2005, 44, 7852-7872
11. Shen, L.; Bao, N.; Yanagisawa, K.; Domen, K.; Gupta, A.; Grimes, C. A. Direct Synthesis of ZnO Nanoparticles by a Solution-Free Mechanochemical Reaction Nanotechnology 2006, 17, 5117-5123
12. 3 Made by Mechanical Activation Appl. Catal. B 2004, 52, 11-21
13. Bigioni, T. P.; Lin, X. M.; Nguyen, T. T.; Corwin, E. I.; Witten, T. A.; Jaeger, H. M. Kinetically Driven Self Assembly of Highly Ordered Nanoparticle Monolayers Nat. Mater. 2006, 5, 265-270
14. Jana, N. R.; Gearheart, L.; Murphy, C. J. Evidence for Seed-Mediated Nucleation in the Chemical Reduction of Gold Salts to Gold Nanoparticles Chem. Mater. 2001, 13, 2313-2322
15. Sau, T. K.; Murphy, C. J. Room Temperature, High-Yield Synthesis of Multiple Shapes of Gold Nanoparticles in Aqueous Solution J. Am. Chem. Soc. 2004, 126, 8648-8649
16. Sun, Y. G.; Xia, Y. N. Shape-Controlled Synthesis of Gold and Silver Nanoparticles Science 2002, 298, 2176-2179
17. Manna, L.; Scher, E. C.; Alivisatos, A. P. Synthesis of Soluble and Processable Rod, Arrow, Teardrop, and Tetrapod-Shaped CdSe Nanocrystals J. Am. Chem. Soc. 2000, 122, 12700-12706
18. Murphy, C. J.; San, T. K.; Gole, A. M.; Orendorff, C. J.; Gao, J. X.; Gou, L.; Hunyadi, S. E.; Li, T. Anisotropic Metal Nanoparticles: Synthesis, Assembly, and Optical Applications J. Phys. Chem. B 2005, 109, 13857-13870
19. Marqusee, J. A.; Ross, J. Theory of Ostwald Ripening-Competitive Growth and Its Dependence on Volume Fraction J. Chem. Phys. 1984, 80, 536-543
20. Stoeva, S.; Klabunde, K. J.; Sorensen, C. M.; Dragieva, I. Gram-Scale Synthesis of Monodisperse Gold Colloids by the Solvated Metal Atom Dispersion Method and Digestive Ripening and Their Organization into Two- and Three-Dimensional Structures J. Am. Chem. Soc. 2002, 124, 2305-2311
21. Ahmadi, T. S.; Wang, Z. L.; Green, T. C.; Henglein, A.; El-Sayed, M. A. Shape-Controlled Synthesis of Colloidal Platinum Nanoparticles Science 1996, 272, 1924-1925
22. Grace, A. N.; Pandian, K. One Pot Synthesis of Polymer Protected Pt, Pd, Ag and Ru Nanoparticles and Nanoprisms under Reflux and Microwave Mode of Heating in Glycerol-A Comparative Study Mater. Chem. Phys. 2007, 104, 191-198
23. Millstone, J. E.; Hurst, S. J.; Metraux, G. S.; Cutler, J. I.; Mirkin, C. A. Colloidal Gold and Silver Triangular Nanoprisms Small 2009, 5, 646-664
24. Narayanan, R.; El-Sayed, M. A. Effect of Nanocatalysis in Colloidal Solution on the Tetrahedral and Cubic Nanoparticle SHAPE: Electron-Transfer Reaction Catalyzed by Platinum Nanoparticles J. Phys. Chem. B 2004, 108, 5726-5733
25. Wang, Z. L.; Petroski, J. M.; Green, T. C.; El-Sayed, M. A. Shape Transformation and Surface Melting of Cubic and Tetrahedral Platinum Nanocrystals J. Phys. Chem. B 1998, 102, 6145-6151
26. Humphrey, S. M.; Grass, M. E.; Habas, S. E.; Niesz, K.; Somorjai, G. A.; Tilley, T. D. Rhodium Nanoparticles from Cluster Seeds: Control of Size and Shape by Precursor Addition Rate Nano Lett. 2007, 7, 785-790
27. Zettsu, N.; McLellan, J. M.; Wiley, B.; Yin, Y.; Li, Z.-Y.; Xia, Y. Synthesis, Stability, and Surface Plasmonic Properties of Rhodium Multipods, and Their Use as Substrates for Surface-Enhanced Raman Scattering Angew. Chem., Int. Ed. 2006, 45, 1288-1292
28. Cushing, B. L.; Kolesnichenko, V. L.; O'Connor, C. J. Recent Advances in the Liquid-Phase Syntheses of Inorganic Nanoparticles Chem. Rev. 2004, 104, 3893-3946
29. Ashida, T.; Miura, K.; Nomoto, T.; Yagi, S.; Sumida, H.; Kutluk, G.; Soda, K.; Namatame, H.; Taniguchi, M. Synthesis and Characterization of Rh(PVP) Nanoparticles Studied by XPS and NEXAFS Surf. Sci. 2007, 601, 3898-3901
30. Biacchi, A. J.; Schaak, R. E. The Solvent Matters: Kinetic versus Thermodynamic Shape Control in the Polyol Synthesis of Rhodium Nanoparticles ACS Nano 2011, 5, 8089-8099
31. Durap, F.; Zahmakiran, M.; Ozkar, S. Water Soluble Laurate-Stabilized Rhodium(0) Nanoclusters Catalyst with Unprecedented Catalytic Lifetime in the Hydrolytic Dehydrogenation of Ammonia-Borane Appl. Catal. A 2009, 369, 53-59
32. Ewers, T. D.; Sra, A. K.; Norris, B. C.; Cable, R. E.; Cheng, C. H.; Shantz, D. F.; Schaak, R. E. Spontaneous Hierarchical Assembly of Rhodium Nanoparticles into Spherical Aggregates and Superlattices Chem. Mater. 2005, 17, 514-520
33. Filot, I. A. W.; Shetty, S. G.; Hensen, E. J. M.; van Santen, R. A. Size and Topological Effects of Rhodium Surfaces, Clusters and Nanoparticles on the Dissociation of CO J. Phys. Chem. C 2011, 115, 14204-14212
34. Harada, M.; Abe, D.; Kimura, Y. Synthesis of Colloidal Dispersions of Rhodium Nanoparticles under High Temperatures and High Pressures J. Colloid Interface Sci. 2005, 292, 113-121
35. Hoefelmeyer, J. D.; Liu, H.; Somorjai, G. A.; Tilley, T. D. Reverse Micelle Synthesis of Rhodium Nanoparticles J. Colloid Interface Sci. 2007, 309, 86-93
36. Hoefelmeyer, J. D.; Niesz, K.; Somorjai, G. A.; Tilley, T. D. Radial Anisotropic Growth of Rhodium Nanoparticles Nano Lett. 2005, 5, 435-438
37. Jang, K.; Kim, H. J.; Son, S. U. Low-Temperature Synthesis of Ultrathin Rhodium Nanoplates via Molecular Orbital Symmetry Interaction between Rhodium Precursors Chem. Mater. 2010, 22, 1273-1275
38. Leger, B.; Denicourt-Nowicki, A.; Olivier-Bourbigou, H.; Roucoux, A. Rhodium Nanocatalysts Stabilized by Various Bipyridine Ligands in Nonaqueous Ionic Liquids: Influence of the Bipyridine Coordination Modes in Arene Catalytic Hydrogenation Inorg. Chem. 2008, 47, 9090-9096
39. Mittendorfer, F.; Seriani, N.; Dubay, O.; Kresse, G. Morphology of Mesoscopic Rh and Pd Nanoparticles under Oxidizing Conditions Phys. Rev. B 2007, 76, 233413
40. Mu, X. D.; Meng, J. Q.; Li, Z. C.; Kou, Y. Rhodium Nanoparticles Stabilized by Ionic Copolymers in Ionic Liquids: Long Lifetime Nanocluster Catalysts for Benzene Hydrogenation J. Am. Chem. Soc. 2005, 127, 9694-9695
41. 2 Reaction Appl. Catal. A 2004, 274, 33-41
42. Pradhan, M.; Sarkar, S.; Sinha, A. K.; Basu, M.; Pal, T. High-Yield Synthesis of 1D Rh Nanostructures from Surfactant Mediated Reductive Pathway and Their Shape Transformation J. Phys. Chem. C 2011, 114, 16129-16142
43. Quek, X. Y.; Guan, Y. J.; van Santen, R. A.; Hensen, E. J. M. Ionic-Liquid-Stabilized Rhodium Nanoparticles for Citral Cyclodehydration ChemSusChem 2010, 3, 1264-1267
44. Redel, E.; Kramer, J.; Thomann, R.; Janiak, C. Synthesis of Co, Rh and Ir Nanoparticles from Metal Carbonyls in Ionic Liquids and Their Use as Biphasic Liquid-Liquid Hydrogenation Nanocatalysts for Cyclohexene J. Organomet. Chem. 2009, 694, 1069-1075
45. Zhang, H.; Li, W. Y.; Jin, M. S.; Zeng, J. E.; Yu, T. K.; Yang, D. R.; Xia, Y. N. Controlling the Morphology of Rhodium Nanocrystals by Manipulating the Growth Kinetics with a Syringe Pump Nano Lett. 2011, 11, 898-903
46. Zhang, Y. W.; Grass, M. E.; Kuhn, J. N.; Tao, F.; Habas, S. E.; Huang, W. Y.; Yang, P. D.; Somorjai, G. A. Highly Selective Synthesis of Cataytically Active Monodisperse Rhodium Nanocubes J. Am. Chem. Soc. 2008, 130, 5868-5869
47. Zhang, Y. W.; Grass, M. E.; Huang, W. Y.; Somorjai, G. A. Seedless Polyol Synthesis and CO Oxidation Activity of Monodisperse (111) and (100) Oriented Rhodium Nanocrystals in Sub-10 nm Sizes Langmuir 2011, 26, 16463-16468
48. Kappe, C. O. Controlled Microwave Heating in Modern Organic Synthesis Angew. Chem., Int. Ed. 2004, 43, 6250-6284
49. Lidstrom, P.; Tierney, J.; Wathey, B.; Westman, J. Microwave Assisted Organic Synthesis-A Review Tetrahedron 2001, 57, 9225-9283
50. Bilecka, I.; Niederberger, M. Microwave Chemistry for Inorganic Nanomaterials Synthesis Nanoscale 2010, 2, 1358-1374
51. Nadagouda, M. N.; Speth, T. F.; Varma, R. S. Microwave-Assisted Green Synthesis of Silver Nanostructures Acc. Chem. Res. 2011, 44, 469-478
52. Panda, A. B.; Glaspell, G.; El-Shall, M. S. Microwave Synthesis of Highly Aligned Ultra Narrow Semiconductor Rods and Wires J. Am. Chem. Soc. 2006, 128, 2790-2791
53. Zedan, A. F.; Sappal, S.; Moussa, S.; El-Shall, M. S. Ligand-Controlled Microwave Synthesis of Cubic and Hexagonal CdSe Nanocrystals Supported on Graphene. Photoluminescene Quenching by Graphene J. Phys. Chem. C 2010, 114, 19920-19927
54. Panda, A. B.; Glaspell, G.; El-Shall, M. S. Microwave Synthesis and Optical Properties of Uniform Nanorods and Nanoplates of Rare Earth Oxides J. Phys. Chem. C 2007, 111, 1861-1864
55. Abdelsayed, V.; Aljarash, A.; El-Shall, M. S. Microwave Synthesis of Bimetallic Nanoalloys and CO Oxidation on Ceria-Supported Nanoalloys Chem. Mater. 2009, 21, 2825-2834
56. Njoki, P. N.; Wu, W.; Zhao, H.; Hutter, L.; Schiff, E. A.; Maye, M. M. Layer-by-Layer Processing and Optical Properties of Core/Alloy Nanostructures J. Am. Chem. Soc. 2011, 133, 5224-5227
57. Herring, N. P.; AbouZeid, K.; Mohammed, M. B.; Pinsk, J.; El-Shall, M. S. Formation Mechanisms of Gold-Zinc Oxide Hexagonal Nanopyramids by Heterogeneous Nucleation Using Microwave Synthesis Langmuir 2011, 27, 15146-15154
58. Zhang, Y. W.; Grass, M. E.; Habas, S. E.; Tao, F.; Zhang, T. F.; Yang, P. D.; Somorjai, G. A. One-Step Polyol Synthesis and Langmuir-Blodgett Monolayer Formation of Size-Tunable Monodisperse Rhodium Nanocrystals with Catalytically Active (111) Surface Structures J. Phys. Chem. C 2007, 111, 12243-12253
59. Jose-Yacaman, M.; Marin-Almazo, M.; Ascencio, J. A. High Resolution TEM Studies on Palladium Nanoparticles J. Mol. Catal. A 2001, 173, 61-74
60. Borodko, Y.; Humphrey, S. M.; Tilley, T. D.; Frei, H.; Somorjai, G. A. Charge-Transfer Interaction of Poly(vinylpyrrolidone) with Platinum and Rhodium Nanoparticles J. Phys. Chem. C 2007, 111, 6288-6295
61. Bagaria, H. G.; Ada, E. T.; Shamsuzzoha, M.; Nikles, D. E.; Johnson, D. T. Understanding Mercapto Ligand Exchange on the Surface of FePt Nanoparticles Langmuir 2006, 22, 7732-7737
62. Grass, M. E.; Joo, S. H.; Zhang, Y. W.; Somorjai, G. A. Colloidally Synthesized Monodisperse Rh Nanoparticles Supported on SBA-15 for Size- and Pretreatment-Dependent Studies of CO Oxidation J. Phys Chem. C 2009, 113, 8616-8623
63. Borodko, Y.; Habas, S. E.; Koebel, M.; Yang, P.; Frei, H.; Somorjai, G. A. Probing the Interaction of Poly(vinylpyrrolidone) with Platinum Nanocrystals by UV-Raman and FTIR J. Phys. Chem. B 2006, 110, 23052-23059
64. Cimpeanu, V.; Kočevar, M.; Parvulescu, V. I.; Leitner, W. Preparation of Rhodium Nanoparticles in Carbon Dioxide Induced Ionic Liquids and Their Application to Selective Hydrogenation Angew. Chem., Int. Ed. 2008, 48, 1085-1088