Characterization of perchlorate in a new frozen human urine standard reference material

Analytical and Bioanalytical Chemistry

Volumn 404, Issue 6-7, 2012, Pages 1877-1886

  Yu, Lee L ^a   Jarrett, Jeffery M ^b   Davis, W Clay ^a   Kilpatrick, Eric L ^a   Oflaz, Rabia ^a   Turk, Gregory C ^a   Leber, Dennis D ^c   Valentin, Liza ^b   Morel, Maria Espinosa ^b   Blount, Benjamin C ^b  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

^b NATIONAL CENTER FOR ENVIRONMENTAL HEALTH   (United States)

^c NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

Certified reference material; Perchlorate; Standard reference material; Urine

Indexed keywords

BIOMONITORING; CENTERS FOR DISEASE CONTROL AND PREVENTIONS; CERTIFIED REFERENCE MATERIALS; CERTIFIED VALUES; ENVIRONMENTAL CONTAMINANT; HUMAN EXPOSURES; HUMAN URINE; INORGANIC ANIONS; MEASUREMENT TECHNIQUES; NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY; PERCHLORATE; POTENTIAL SOURCES; STANDARD REFERENCE MATERIAL; TANDEM MASS SPECTROMETRY; URINE; US ENVIRONMENTAL PROTECTION AGENCY;

BODY FLUIDS; ENVIRONMENTAL PROTECTION AGENCY; IODINE; MASS SPECTROMETRY; MATERIALS; MERCURY (METAL); METRIC SYSTEM; NEGATIVE IONS; QUALITY ASSURANCE;

INORGANIC COMPOUNDS;

PERCHLORATE; PERCHLORIC ACID;

ARTICLE; CHEMISTRY; ENVIRONMENTAL EXPOSURE; HUMAN; LIQUID CHROMATOGRAPHY; METHODOLOGY; STANDARD; TANDEM MASS SPECTROMETRY; UNITED STATES; URINE;

CHROMATOGRAPHY, LIQUID; ENVIRONMENTAL EXPOSURE; HUMANS; PERCHLORIC ACID; REFERENCE STANDARDS; TANDEM MASS SPECTROMETRY; UNITED STATES; URINE;

EID: 84867337908     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-012-6263-5     Document Type: Article

References (23)

1. Dasgupta PK, Dyke JV, Kirk AB, Jackson WA (2006) Perchlorate in the United States. Analysis of relative source contributions to the food chain. Environ Sci Technol 40: 6608-6614
2. Urbansky ET, Brown SK, Magnuson ML, Kelty CA (2001) Perchlorate levels in samples of sodium nitrate fertilizer derived from Chilean caliche. Environ Pollut 112: 299-302
3. Huber DR, Blount BC, Mage DT, Letkiewicz FJ, Kumar A, Allen RH (2011) Estimating perchlorate exposure from food and tap water based on US biomonitoring and occurrence data. J Expo Sci Environ Epidemiol 21: 395-407
4. Perchlorate (2012) US EPA, available at http://water.epa.gov/drink/ contaminants/unregulated/perchlorate.cfm Accessed 9 July 2012
5. Greer MA, Goodman G, Pleus RC, Greer SE (2002) Health effects assessment for environmental perchlorate contamination: the dose response for inhibition of thyroidal radioiodine uptake in humans. Environ Health Perspect 110: 927-937
6. Blount BC, Pirkle JL, Osterloh JD, Valentin-Blasini L, Caldwell KL (2006) Urinary perchlorate and thyroid hormone levels in adolescent and adult men and women living in the United States. Environ Health Perspect 114: 1865-1871
7. Braverman LE, Utiger RD (2000) "Introduction to hypothyroidism" In: Braverman LE,Utiger RD(eds)Werner and Ingbar's The thyroid: a fundamental and clinical text. Philadelphia, PA, Lippincott Williams and Wilkins.
8. Glinoer D (2000) "Thyroid disease during pregnancy" In: Braverman LE, Utiger RD (eds)Werner and Ingbar's The thyroid: a fundamental and clinical text. Philadelphia, PA, Lippincott Williams and Wilkins
9. Haddow JE, Palomaki GE, Allan WC, Williams JR, Knight GJ, Gagnon J, O'Heir CE, Mitchell ML, Hermos RJ, Waisbren SE, Faix JD, Klein RZ (1999) Maternal thyroid deficiency during pregnancy and subsequent neuropsychological development of the child. N Engl J Med 341: 549-555
10. Klein RZ, Sargent JD, Larsen PR, Waisbren SE, Haddow JE, Mitchell ML (2001) Relation of severity of maternal hypothyroidism to cognitive development of offspring. J Med Screen 8: 18-20
11. CDC (2012) National Report on Human Exposure to Environmental Chemicals. Center for Disease Control and Prevention, Atlanta, GA, available at http://www.cdc.gov/exposurereport/Accessed 9 July 2012
12. Blount BC, Valentin-Blasini L, Osterloh JD, Maldin JP, Pirkle JL (2007) Perchlorate exposure of the US population, 2001-2002. J Expo Sci Environ Epidemiol 17: 400-407
13. Tonacchera M, Pinchera A, Dimida A, Ferrarini E, Agretti P, Vitti P, Santini F, Crump K, Gibbs J (2004) Relative potencies and additivity of perchlorate, thiocyanate, nitrate, and iodide on the inhibition of radioactive iodide uptake by the human sodium iodide symporter. Thyroid 14: 1012-1019
14. May WE, Parris RM, Beck II CM, Fassett JD, Greenberg RR, Guenther FR, Kramer GW, Wise SA, Gills TE, Colbert JC, Gettings RJ, MacDonald BS (2000) Definitions of terms and modes used at NIST for value-assignment of reference materials for chemical measurements; NIST Spec. Pub. 260-136, U.S. Government Printing Office: Washington, DC; available athttp://www.nist.gov/srm/upload/SP 260-136.PDF. See also the certificate of analysis for SRM 3668, available at https://www-s.nist.gov/srmors/certificates/3668.pdf? CFID02127979& CFTOKEN0489d86dccd1c99da-2F 599806-00DD- 9A 72- 1C94E6809A293E24&jsessionid0f030c1f8511d9de3c d22262a6d587852775b. Accessed 9 July 2012
15. Valentin-Blasini L, Mauldin JP, Maple D, Blount BC (2005) Analysis of perchlorate in human urine using ion chromatography and electrospray tandem mass spectrometry. Anal Chem 77: 2475-2481
16. Table of radioactive isotopes (2012) http://nucleardata.nuclear.lu.se/ NuclearData/toi/listnuc.asp?sql0&Z017. Accessed 9 July 2012
17. Joint Committee for Guides in Metrology (2008) Evaluation of measurement data - supplement 1 to the "Guide to the expression of uncertainty in measurement" - propagation of distributions using a Monte Carlo method. Sevres Cedex, France. Available at http://www.bipm.org/utils/common/documents/ jcgm/JCGM-101-2008- E.pdf. Accessed 9 July 2012
18. Mackay LG, Taylor CP, Myors RB, Hearn R, King B (2003) High accuracy analysis by isotope dilution mass spectrometry using an iterative exact matching technique. Accred Qual Assur 8: 191-194
19. DerSimonian R, Laird N (1986) Meta-analysis in clinical trials. Control Clin Trials 7: 177-188
20. Efron B, Tibshirani RJ (1993) An introduction to the bootstrap. Chapman & Hall, New York
21. Rukhin AL (2009) Weighted means statistics in interlaboratory studies. Metrol 46: 323-331
22. Rukhin AL, Vangel MG (1998) Estimation of a common mean and weighted means statistics. J Am Stat Assoc 93: 303-308
23. Toman B, Possolo A (2009) Laboratory effects models for interlaboratory comparisons. Accred Qual Assur 14: 553-563