Detailed analysis of the TIMES and TIMES0 high-resolution MAS methods for high-resolution proton NMR

Journal of Magnetic Resonance

Volumn 223, Issue , 2012, Pages 219-227

  Lu, Xingyu ^a   Lafon, Olivier ^a   Trébosc, Julien ^a   Thankamony, Aany Sofia Lilly ^a   Nishiyama, Yusuke ^b   Gan, Zhehong ^c   Madhu, P K ^d   Amoureux, Jean Paul ^a  

^a UNIV LILLE   (France)

^b JEOL LTD   (Japan)

^c FLORIDA STATE UNIVERSITY   (United States)

^d TATA INSTITUTE OF FUNDAMENTAL RESEARCH   (India)

Author keywords

1H; CRAMPS; rf Field homogeneity; Scaling factor; Solid state NMR; TIMES methods; Ultra fast MAS

Indexed keywords

1H; CRAMPS; RF-FIELD HOMOGENEITY; SCALING FACTORS; SOLID STATE NMR; TIMES METHODS; ULTRA-FAST MAS;

INTELLIGENT CONTROL; MAGIC ANGLE SPINNING; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROTONS;

SPEED;

AMINE; GLYCINE; PROTON;

ALGORITHM; ARTICLE; CHEMISTRY; ELECTROMAGNETIC FIELD; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ALGORITHMS; AMINES; ELECTROMAGNETIC FIELDS; GLYCINE; MAGNETIC RESONANCE SPECTROSCOPY; PROTONS;

EID: 84866145726     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2012.07.015     Document Type: Article

References (58)

1. U. Haeberlen High Resolution NMR in Solids-selective Averaging 1976 Academic Press New York
2. E. Vinogradov, P.K. Madhu, and S. Vega Strategies for high-resolution proton spectroscopy in solid-state NMR Topics Curr. Chem. 246 2005 3390
3. B.C. Gerstein, C. Clor, R.G. Pembleton, and R.C. Wilson Utility of pulse NMR in studying protons in coals J. Phys. Chem. 81 1977 565 570
4. 1H chemical shift tensors J. Chem. Phys. 71 1979 4541 4545
5. D.P. Burum, and W.K. Rhim Analysis of multiple pulse NMR in solids J. Chem. Phys. 71 1979 944 956
6. D.P. Burum, and W.K. Rhim An improved NMR technique for homo-nuclear dipolar decoupling in solids: application to polycrystalline ice J. Chem. Phys. 70 1979 3553 3554
7. C.E. Bronnimann, B.L. Hawkings, M. Zhang, and G.E. Maciel Combined Rotation and Multiple Pulse Spectroscopy as an analytical proton NMR technique for solids Anal. Chem. 60 1988 1743 1750
8. J.S. Waugh, L.M. Huber, and U. Haeberlen Approach to high-resolution NMR in solids Phys. Rev. Lett. 20 1968 180 182
9. M. Mehring, and J.S. Waugh Magic-angle NMR experiments in solids Phys. Rev. B 5 1972 3459 3471
10. K. Takegoshi, and C.A. McDowell A "magic echo" pulse sequence for the high-resolution NMR spectra of abundant spins in solids Chem. Phys. Lett. 116 1985 100 104
11. A. Bielecki, A.C. Kolbert, and M.H. Levitt Frequency-switched pulse sequences: homo-nuclear decoupling and dilute spin NMR in solids Chem. Phys. Lett. 155 1989 341 346
12. D.G. Cory A new multiple-pulse cycle for homo-nuclear dipolar decoupling J. Magn. Reson. 94 1991 526 534
13. 1H NMR in solids with frequency-switched multiple-pulse sequences Solid State Nucl. Magn. Reson. 2 1993 151 163
14. 1H CRAMPS based on TREV J. Magn. Reson. A 103 1993 183 187
15. D. Demco, S. Hafner, and H.W. Spiess Rotation-synchronized homo-nuclear dipolar decoupling J. Magn. Reson. A 116 1995 36 45
16. S. Hafner, and H.W. Spiess Multiple-Pulse line narrowing under fast Magic-Angle Spinning J. Magn. Reson. A 121 1996 160 166
17. M. Howhy, P.V. Bower, H.J. Jakobsen, and N.C. Nielsen A high-order and broadband CRAMPS experiment using z-rotational decoupling Chem. Phys. Lett. 273 1997 297 303
18. M. Hohwy, and N.C. Nielsen Elimination of high order terms in multiple pulse nuclear magnetic resonance spectroscopy: application to homo-nuclear decoupling in solids J. Chem. Phys. 106 1997 7571 7586
19. E. Vinogradov, P.K. Madhu, and S. Vega High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment Chem. Phys. Lett. 314 1999 443 450
20. D. Sakellariou, A. Lesage, P. Hodgkinson, and L. Emsley Homo-nuclear dipolar decoupling in solid-state NMR using continuous phase modulation Chem. Phys. Lett. 319 2000 253 260
21. 1H NMR in the solid state using symmetry-based pulse sequences Chem. Phys. Lett. 346 2001 142 148
22. 1H homo-nuclear dipolar decoupling at high magic-angle spinning frequencies with rotor-synchronized symmetry sequences Chem. Phys. Lett. 456 2008 253 256
23. 1H homo-nuclear dipolar decoupling using rotor-synchronized pulse sequences: towards pure absorption phase spectra J. Magn. Reson. 205 2010 269 275
24. 1H homo-nuclear dipolar decoupling using symmetry-based pulse sequences at ultra fast magic-angle spinning frequencies J. Magn. Reson. 206 2010 241 245
25. E. Vinogradov, P.K. Madhu, and S. Vega Phase modulated Lee-Goldburg magic angle spinning proton nuclear magnetic resonance experiments in the solid state: a bimodal Floquet theoretical treatment J. Chem. Phys. 115 2001 8983 9000
26. A. Lesage, D. Sakellariou, S. Hediger, B. Eléna, P. Charmont, S. Steuernagel, and L. Emsley Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homo-nuclear dipolar decoupling J. Magn. Reson. 163 2003 105 113
27. B. Eléna, G. de Paepe, and L. Emsley Direct spectral optimization of proton-proton homo-nuclear dipolar decoupling in solid-state NMR Chem. Phys. Lett. 398 2004 532 538
28. M. Leskes, S. Steuernagel, D. Schneider, P.K. Madhu, and S. Vega Homo-nuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance Chem. Phys. Lett. 466 2008 95 99
29. 1H spectrum and higher spinning rates J. Chem. Phys. 128 2008 052309
30. J.P. Amoureux, B. Hu, and J. Trebosc Enhanced resolution in proton solid-state NMR with very-fast MAS experiments J. Magn. Reson. 193 2008 305 307
31. J.P. Amoureux, B. Hu, J. Trébosc, and F. Deng Homo-nuclear dipolar decoupling schemes for fast MAS Solid State Nucl. Magn. Reson. 35 2009 19 24
32. O. Lafon, Q. Wang, B. Hu, J. Trébosc, F. Deng, and J.P. Amoureux Proton-proton homo-nuclear dipolar decoupling in solid-state NMR using rotor-synchronized z-rotation pulse sequences J. Chem. Phys. 130 2009 014504
33. M. Leskes, P.K. Madhu, and S. Vega Why does PMLG proton decoupling work at 65 kHz MAS? J. Magn. Reson. 199 2009 208 213
34. 1H solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS Chem. Phys. Lett. 469 2009 336 341
35. 1H solid-state NMR spectroscopy Chem. Phys. Lett. 498 2010 214 220
36. K. Mao, and M. Pruski Homonuclear dipolar decoupling under fast MAS: resolution patterns and simple optimization strategy J. Magn. Reson. 203 2010 144 149
37. 14N 2D solid-state NMR: sub-micro-liter sample data collection in a few minutes J. Magn. Reson. 208 2011 44 48 (Also, poster from the Jeol Company at 53rd ENC, Miami-USA, 15-20 April 2012)
38. 1H-{X} HMQC experiments at ultra-fast MAS J. Magn. Reson. 214 2012 151 158
39. 1H NMR spectroscopy of solids Solid State Nucl. Magn. Reson. 20 2001 130 136
40. D.H. Zhou, G. Shah, M. Cormos, C. Mullen, D. Sandoz, and C.M. Rienstra Proton-detected Solid-State NMR spectroscopy of fully protonated proteins at 40 kHz Magic-Angle Spinning J. Am. Chem. Soc. 129 2007 11791 11801
41. 13C NMR hetero-nuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homo-nuclear decoupling J. Magn. Reson. 124 1997 516 519
42. S. Cavadini, V. Vitzthum, S. Ulzega, A. Abraham, and G. Bodenhausen Line-narrowing in proton-detected nitrogen-14 NMR J. Magn. Reson. 202 2010 57 63
43. Z. Gan, P.K. Madhu, J.P. Amoureux, J. Trébosc, and O. Lafon A tunable homo-nuclear dipolar decoupling scheme for high-resolution proton NMR of solids from slow to fast magic-angle spinning Chem. Phys. Lett. 503 2011 167 170
44. M. Bak, J.T. Rasmussen, and N.C. Nielsen SIMPSON: a general simulation program for solid-state NMR spectroscopy J. Magn. Reson. 147 2000 296 330
45. M.R. Bendall, and R.E. Gordon Depth and refocusing pulses designed for multi-pulse NMR with surface coils J. Magn. Reson. 53 1983 365 385
46. D.G. Cory, and W.M. Ritchey Suppression of signals from the probe in Bloch decay spectra J. Magn. Reson. 80 1988 128 132
47. S. Wimperis Broadband, narrow-band and pass-band composite pulses for use in advanced NMR experiments J. Magn. Reson. A 109 1994 221 231
48. R. Tycko, and A. Pines Spatial localization of NMR signals by narrowband inversion J. Magn. Reson. 60 1984 156 160
49. R. Tycko, and A. Pines Iterative schemes for broad-band and narrow-band population inversion in NMR Chem. Phys. Lett. 111 1984 462 467
50. J. Baum, R. Tycko, and A. Pines Spatially selective NMR with broad-band radiofrequency pulses Chem. Phys. 105 1986 7
51. A.J. Shaka, and R. Freeman A composite 180° pulse for spatial localization J. Magn. Reson. 63 1985 596 600
52. A.J. Shaka, and R. Freeman Pre-pulses for spatial localization J. Magn. Reson. 64 1985 145 150
53. 1H MAS NMR using composite pulses J. Magn. Reson. 221 2012 41 50
54. M. Ernst, A. Samoson, and B.H. Meier Low-power decoupling in fast magic-angle spinning NMR Chem. Phys. Lett. 348 2001 293 302
55. M. Ernst, A. Samoson, and B.H. Meier Low-power XiX decoupling in MAS NMR experiments J. Magn. Reson. 163 2003 332 339
56. 13C high-resolution solid-state NMR under fast magic angle spinning Magn. Reson. Chem. 45 2007 S221 S230
57. M. Weingarth, G. Bodenhausen, and P. Tekely Low-power decoupling at high spinning frequencies in high static fields J. Magn. Reson. 199 2009 238 241
58. M. Weingarth, J. Trébosc, J.P. Amoureux, G. Bodenhausen, and P. Tekely Efficiency at high spinning frequencies of hetero-nuclear decoupling methods designed to quench rotary resonance Solid State Nucl. Magn. Reson. 40 2011 21 26