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Volumn 202, Issue 1, 2010, Pages 57-63

Line-narrowing in proton-detected nitrogen-14 NMR

Author keywords

14N; HMQC; Homonuclear dipolar decoupling; HSQC; Magic angle spinning (MAS); Solid state NMR; Symmetry based pulse sequence

Indexed keywords

ACCURATE MEASUREMENT; ASYMMETRY PARAMETER; DOUBLE-QUANTUM; FOURIER TRANSFORMATIONS; HETERONUCLEAR; HIGHEST RESOLUTIONS; HOMONUCLEAR; HOMONUCLEAR DIPOLAR DECOUPLING; INDIRECT DETECTION; L-ALANINE; LINE-NARROWING; MAGIC ANGLE; MAGIC ANGLE SPINNING; NITROGEN-14; PEPTIDE BONDS; PROTON INTERACTIONS; QUADRUPOLAR COUPLING CONSTANTS; QUANTUM CORRELATIONS; R-SEQUENCES; SOLID STATE NMR; SPIN COHERENCE; SYMMETRY-BASED PULSE SEQUENCES; TRIPEPTIDE;

EID: 72149114876     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2009.09.018     Document Type: Article
Times cited : (41)

References (54)
  • 1
    • 36149012226 scopus 로고
    • The dependence of a nuclear magnetic resonance frequency upon chemical compound
    • Proctor W.G., and Yu F.C. The dependence of a nuclear magnetic resonance frequency upon chemical compound. Phys. Rev. 77 (1950) 717
    • (1950) Phys. Rev. , vol.77 , pp. 717
    • Proctor, W.G.1    Yu, F.C.2
  • 2
    • 36749117561 scopus 로고
    • N-14 NMR determination of NH bond lengths in solids
    • Stark R.E., Haberkorn R.A., and Griffin R.G. N-14 NMR determination of NH bond lengths in solids. J. Chem. Phys. 68 (1978) 1996
    • (1978) J. Chem. Phys. , vol.68 , pp. 1996
    • Stark, R.E.1    Haberkorn, R.A.2    Griffin, R.G.3
  • 3
    • 0000368696 scopus 로고
    • Peptide plane orientations determined by fundamental and overtone N-14 NMR
    • Tycko R., Stewart P.L., and Opella S.J. Peptide plane orientations determined by fundamental and overtone N-14 NMR. J. Am. Chem. Soc. 108 (1986) 5419
    • (1986) J. Am. Chem. Soc. , vol.108 , pp. 5419
    • Tycko, R.1    Stewart, P.L.2    Opella, S.J.3
  • 6
    • 0041967618 scopus 로고    scopus 로고
    • Chemical bonding differences evidenced from J-coupling in solid state NMR experiments involving quadrupolar nuclei
    • Massiot D., Fayon F., Alonso B., Trébosc J., and Amoureux J.P. Chemical bonding differences evidenced from J-coupling in solid state NMR experiments involving quadrupolar nuclei. J. Magn. Reson. 164 (2003) 160
    • (2003) J. Magn. Reson. , vol.164 , pp. 160
    • Massiot, D.1    Fayon, F.2    Alonso, B.3    Trébosc, J.4    Amoureux, J.P.5
  • 8
    • 33646524732 scopus 로고    scopus 로고
    • Measuring amide nitrogen quadrupolar coupling by high-resolution N-14/C-13 NMR correlation under magic-angle spinning
    • Gan Z. Measuring amide nitrogen quadrupolar coupling by high-resolution N-14/C-13 NMR correlation under magic-angle spinning. J. Am. Chem. Soc. 128 (2006) 6040
    • (2006) J. Am. Chem. Soc. , vol.128 , pp. 6040
    • Gan, Z.1
  • 10
    • 33747871346 scopus 로고    scopus 로고
    • Indirect detection of nitrogen-14 in solids via protons by nuclear magnetic resonance spectroscopy
    • Cavadini S., Antonijevic S., Lupulescu A., and Bodenhausen G. Indirect detection of nitrogen-14 in solids via protons by nuclear magnetic resonance spectroscopy. J. Magn. Reson. 182 (2006) 168
    • (2006) J. Magn. Reson. , vol.182 , pp. 168
    • Cavadini, S.1    Antonijevic, S.2    Lupulescu, A.3    Bodenhausen, G.4
  • 12
    • 33750965453 scopus 로고    scopus 로고
    • Rotary resonance echo double resonance for measuring heteronuclear dipolar coupling under MAS
    • Gan Z. Rotary resonance echo double resonance for measuring heteronuclear dipolar coupling under MAS. J. Magn. Reson. 183 (2006) 235
    • (2006) J. Magn. Reson. , vol.183 , pp. 235
    • Gan, Z.1
  • 13
    • 33845981864 scopus 로고    scopus 로고
    • 13C/14N heteronuclear multiple-quantum correlation with rotary resonance and REDOR dipolar recoupling
    • Gan Z. 13C/14N heteronuclear multiple-quantum correlation with rotary resonance and REDOR dipolar recoupling. J. Magn. Reson. 184 (2006) 39
    • (2006) J. Magn. Reson. , vol.184 , pp. 39
    • Gan, Z.1
  • 14
    • 33846422346 scopus 로고    scopus 로고
    • Proton-detected N-14 MAS NMR using homonuclear decoupled rotary resonance
    • Gan Z., Amoureux J.P., and Trébosc J. Proton-detected N-14 MAS NMR using homonuclear decoupled rotary resonance. Chem. Phys. Lett. 435 (2007) 163
    • (2007) Chem. Phys. Lett. , vol.435 , pp. 163
    • Gan, Z.1    Amoureux, J.P.2    Trébosc, J.3
  • 15
    • 2542487776 scopus 로고
    • Quadrupolar effects transferred to spin-1/2 magic-angle spinning spectra of solids
    • Harris R.K., and Olivieri A.C. Quadrupolar effects transferred to spin-1/2 magic-angle spinning spectra of solids. Prog. NMR Spectrosc. 24 (1992) 435
    • (1992) Prog. NMR Spectrosc. , vol.24 , pp. 435
    • Harris, R.K.1    Olivieri, A.C.2
  • 16
    • 0000715150 scopus 로고    scopus 로고
    • Second-order quadrupolar-dipolar broadening in two-dimensional multiple-quantum MAS NMR
    • McManus J., Kemp-Harper R., and Wimperis S. Second-order quadrupolar-dipolar broadening in two-dimensional multiple-quantum MAS NMR. Chem. Phys. Lett. 311 (1999) 292
    • (1999) Chem. Phys. Lett. , vol.311 , pp. 292
    • McManus, J.1    Kemp-Harper, R.2    Wimperis, S.3
  • 17
    • 85005747434 scopus 로고
    • Rotary resonance recoupling in heteronuclear spin pair systems
    • Levitt M.H., Oas T.G., and Griffin R.G. Rotary resonance recoupling in heteronuclear spin pair systems. Isr. J. Chem. 28 (1988) 271
    • (1988) Isr. J. Chem. , vol.28 , pp. 271
    • Levitt, M.H.1    Oas, T.G.2    Griffin, R.G.3
  • 18
    • 0000785903 scopus 로고
    • Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic-resonance spectroscopy
    • Oas T.G., Griffin R.G., and Levitt M.H. Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic-resonance spectroscopy. J. Chem. Phys. 89 (1988) 692
    • (1988) J. Chem. Phys. , vol.89 , pp. 692
    • Oas, T.G.1    Griffin, R.G.2    Levitt, M.H.3
  • 19
    • 0001050857 scopus 로고
    • Rotational resonance in a spin-lock field for solid-state NMR
    • Gan Z.H., and Grant D.M. Rotational resonance in a spin-lock field for solid-state NMR. Chem. Phys. Lett. 168 (1990) 304
    • (1990) Chem. Phys. Lett. , vol.168 , pp. 304
    • Gan, Z.H.1    Grant, D.M.2
  • 20
    • 0030607947 scopus 로고    scopus 로고
    • NMR chemical shift anisotropy measurements by RF driven rotary resonance
    • Gan Z.H., Grant D.M., and Ernst R.R. NMR chemical shift anisotropy measurements by RF driven rotary resonance. Chem. Phys. Lett. 254 (1996) 349
    • (1996) Chem. Phys. Lett. , vol.254 , pp. 349
    • Gan, Z.H.1    Grant, D.M.2    Ernst, R.R.3
  • 21
    • 0041327067 scopus 로고    scopus 로고
    • Symmetry principles for the design of radiofrequency pulse sequences in the nuclear magnetic resonance of rotating solids
    • Carravetta M., Eden M., Zhao X., Brinkmann A., and Levitt M.H. Symmetry principles for the design of radiofrequency pulse sequences in the nuclear magnetic resonance of rotating solids. Chem. Phys. Lett. 321 (2000) 205
    • (2000) Chem. Phys. Lett. , vol.321 , pp. 205
    • Carravetta, M.1    Eden, M.2    Zhao, X.3    Brinkmann, A.4    Levitt, M.H.5
  • 23
    • 34548029485 scopus 로고    scopus 로고
    • Proton-detected nitrogen-14 NMR by recoupling of heteronuclear dipolar interactions using symmetry-based sequences
    • Cavadini S., Abraham A., and Bodenhausen G. Proton-detected nitrogen-14 NMR by recoupling of heteronuclear dipolar interactions using symmetry-based sequences. Chem. Phys. Lett. 445 (2007) 1
    • (2007) Chem. Phys. Lett. , vol.445 , pp. 1
    • Cavadini, S.1    Abraham, A.2    Bodenhausen, G.3
  • 24
    • 33645839335 scopus 로고    scopus 로고
    • Symmetry-based recoupling of O-17-H-1 spin pairs in magic-angle spinning NMR
    • van Beek J.D., Dupree R., and Levitt M.H. Symmetry-based recoupling of O-17-H-1 spin pairs in magic-angle spinning NMR. J. Magn. Reson. 179 (2006) 38
    • (2006) J. Magn. Reson. , vol.179 , pp. 38
    • van Beek, J.D.1    Dupree, R.2    Levitt, M.H.3
  • 25
    • 33748574257 scopus 로고    scopus 로고
    • Sensitivity enhancement and heteronuclear distance measurements in biological O-17 solid-state NMR
    • Brinkmann A., and Kentgens A.P.M. Sensitivity enhancement and heteronuclear distance measurements in biological O-17 solid-state NMR. J. Phys. Chem. B 110 (2006) 16089
    • (2006) J. Phys. Chem. B , vol.110 , pp. 16089
    • Brinkmann, A.1    Kentgens, A.P.M.2
  • 26
    • 33845187569 scopus 로고    scopus 로고
    • Proton-selective O-17-H-1 distance measurements in fast magic-angle-spinning solid-state NMR spectroscopy for the determination of hydrogen bond lengths
    • Brinkmann A., and Kentgens A.P.M. Proton-selective O-17-H-1 distance measurements in fast magic-angle-spinning solid-state NMR spectroscopy for the determination of hydrogen bond lengths. J. Am. Chem. Soc. 128 (2006) 14758
    • (2006) J. Am. Chem. Soc. , vol.128 , pp. 14758
    • Brinkmann, A.1    Kentgens, A.P.M.2
  • 27
    • 34249088004 scopus 로고    scopus 로고
    • Probing proton-proton proximities in the solid state
    • Brown S.P. Probing proton-proton proximities in the solid state. Prog. NMR Spectrosc. 50 (2007) 199
    • (2007) Prog. NMR Spectrosc. , vol.50 , pp. 199
    • Brown, S.P.1
  • 28
    • 0345665855 scopus 로고
    • Utility of pulse nuclear magnetic-resonance in studying protons in coals
    • Gerstein B.C., Chow C., Pembleton R.G., and Wilson R.C. Utility of pulse nuclear magnetic-resonance in studying protons in coals. J. Phys. Chem. 81 (1977) 565
    • (1977) J. Phys. Chem. , vol.81 , pp. 565
    • Gerstein, B.C.1    Chow, C.2    Pembleton, R.G.3    Wilson, R.C.4
  • 29
    • 33646745803 scopus 로고    scopus 로고
    • Multiple-pulse line narrowing under fast magic-angle spinning
    • Hafner S., and Spiess H.W. Multiple-pulse line narrowing under fast magic-angle spinning. J. Magn. Reson., Ser. A 121 (1996) 160
    • (1996) J. Magn. Reson., Ser. A , vol.121 , pp. 160
    • Hafner, S.1    Spiess, H.W.2
  • 30
    • 0035965185 scopus 로고    scopus 로고
    • High-resolution H-1 NMR in the solid state using symmetry-based pulse sequences
    • Madhu P.K., Zhao X., and Levitt M.H. High-resolution H-1 NMR in the solid state using symmetry-based pulse sequences. Chem. Phys. Lett. 346 (2001) 142
    • (2001) Chem. Phys. Lett. , vol.346 , pp. 142
    • Madhu, P.K.1    Zhao, X.2    Levitt, M.H.3
  • 31
    • 42249115493 scopus 로고    scopus 로고
    • H-1 homonuclear dipolar decoupling at high magic-angle spinning frequencies with rotor-synchronised symmetry
    • Paul S., Thakur R.S., and Madhu P.K. H-1 homonuclear dipolar decoupling at high magic-angle spinning frequencies with rotor-synchronised symmetry. Chem. Phys. Lett. 456 (2008) 253
    • (2008) Chem. Phys. Lett. , vol.456 , pp. 253
    • Paul, S.1    Thakur, R.S.2    Madhu, P.K.3
  • 32
    • 36149023808 scopus 로고
    • Nuclear-magnetic-resonance line narrowing by a rotating rf field
    • Lee M., and Goldburg W.I. Nuclear-magnetic-resonance line narrowing by a rotating rf field. Phys. Rev. 140 (1965) A1261
    • (1965) Phys. Rev. , vol.140
    • Lee, M.1    Goldburg, W.I.2
  • 33
    • 0000204974 scopus 로고
    • Magic-angle NMR experiments in solids
    • Mehring M., and Waugh J.S. Magic-angle NMR experiments in solids. Phys. Rev. B 5 (1972) 3459
    • (1972) Phys. Rev. B , vol.5 , pp. 3459
    • Mehring, M.1    Waugh, J.S.2
  • 35
    • 0000227547 scopus 로고    scopus 로고
    • High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment
    • Vinogradov E., Madhu P.K., and Vega S. High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment. Chem. Phys. Lett. 314 (1999) 443
    • (1999) Chem. Phys. Lett. , vol.314 , pp. 443
    • Vinogradov, E.1    Madhu, P.K.2    Vega, S.3
  • 36
    • 0035890370 scopus 로고    scopus 로고
    • Phase modulated Lee-Goldburg magic angle spinning proton nuclear magnetic resonance experiments in the solid state: a bimodal Floquet theoretical treatment
    • Vinogradov E., Madhu P.K., and Vega S. Phase modulated Lee-Goldburg magic angle spinning proton nuclear magnetic resonance experiments in the solid state: a bimodal Floquet theoretical treatment. J. Chem. Phys. 115 (2001) 8983
    • (2001) J. Chem. Phys. , vol.115 , pp. 8983
    • Vinogradov, E.1    Madhu, P.K.2    Vega, S.3
  • 37
    • 33749246021 scopus 로고    scopus 로고
    • Proton line narrowing in solid-state nuclear magnetic resonance: new insights from windowed phase-modulated Lee-Goldburg sequence
    • Leskes M., Madhu P.K., and Vega S. Proton line narrowing in solid-state nuclear magnetic resonance: new insights from windowed phase-modulated Lee-Goldburg sequence. J. Chem. Phys. 125 (2006)
    • (2006) J. Chem. Phys. , vol.125
    • Leskes, M.1    Madhu, P.K.2    Vega, S.3
  • 38
    • 35248833771 scopus 로고    scopus 로고
    • A broad-banded z-rotation windowed phase-modulated Lee-Goldburg pulse sequence for H-1 spectroscopy in solid-state NMR
    • Leskes M., Madhu P.K., and Vega S. A broad-banded z-rotation windowed phase-modulated Lee-Goldburg pulse sequence for H-1 spectroscopy in solid-state NMR. Chem. Phys. Lett. 447 (2007) 370
    • (2007) Chem. Phys. Lett. , vol.447 , pp. 370
    • Leskes, M.1    Madhu, P.K.2    Vega, S.3
  • 39
    • 42649111299 scopus 로고    scopus 로고
    • Supercycled homonuclear dipolar decoupling in solid-state NMR: toward cleaner H-1 spectrum and higher spinning rates
    • Leskes M., Madhu P.K., and Vega S. Supercycled homonuclear dipolar decoupling in solid-state NMR: toward cleaner H-1 spectrum and higher spinning rates. J. Chem. Phys. 128 (2008)
    • (2008) J. Chem. Phys. , vol.128
    • Leskes, M.1    Madhu, P.K.2    Vega, S.3
  • 40
    • 0001315175 scopus 로고    scopus 로고
    • Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation
    • Sakellariou D., Lesage A., Hodgkinson P., and Emsley L. Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation. Chem. Phys. Lett. 319 (2000) 253
    • (2000) Chem. Phys. Lett. , vol.319 , pp. 253
    • Sakellariou, D.1    Lesage, A.2    Hodgkinson, P.3    Emsley, L.4
  • 41
    • 0043175468 scopus 로고    scopus 로고
    • Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling
    • Lesage A., Sakellariou D., Hediger S., Elena B., Charmont P., Steuernagel S., and Emsley L. Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling. J. Magn. Reson. 163 (2003) 105
    • (2003) J. Magn. Reson. , vol.163 , pp. 105
    • Lesage, A.1    Sakellariou, D.2    Hediger, S.3    Elena, B.4    Charmont, P.5    Steuernagel, S.6    Emsley, L.7
  • 42
    • 59249104564 scopus 로고    scopus 로고
    • Enhanced sensitivity in high-resolution H-1 solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS
    • Salager E., Stein R.S., Steuernagel S., Lesage A., Elena B., and Emsley L. Enhanced sensitivity in high-resolution H-1 solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS. Chem. Phys. Lett. 469 (2009) 336
    • (2009) Chem. Phys. Lett. , vol.469 , pp. 336
    • Salager, E.1    Stein, R.S.2    Steuernagel, S.3    Lesage, A.4    Elena, B.5    Emsley, L.6
  • 43
    • 47549096967 scopus 로고    scopus 로고
    • Enhanced resolution in proton solid-state NMR with very-fast MAS experiments
    • Amoureux J.P., Hu B., and Trébosc J. Enhanced resolution in proton solid-state NMR with very-fast MAS experiments. J. Magn. Reson. 193 (2008) 305
    • (2008) J. Magn. Reson. , vol.193 , pp. 305
    • Amoureux, J.P.1    Hu, B.2    Trébosc, J.3
  • 45
    • 18844387115 scopus 로고    scopus 로고
    • High-resolution NMR spectroscopy in solids by truly magic-angle spinning
    • Antonijevic S., and Bodenhausen G. High-resolution NMR spectroscopy in solids by truly magic-angle spinning. Angew. Chem. Int. Edit. 44 (2005) 2935
    • (2005) Angew. Chem. Int. Edit. , vol.44 , pp. 2935
    • Antonijevic, S.1    Bodenhausen, G.2
  • 46
    • 3142715374 scopus 로고    scopus 로고
    • Second order average Hamiltonian theory of symmetry-based pulse schemes in the nuclear magnetic resonance of rotating solids: application to triple-quantum dipolar recoupling
    • Brinkmann A., and Eden M. Second order average Hamiltonian theory of symmetry-based pulse schemes in the nuclear magnetic resonance of rotating solids: application to triple-quantum dipolar recoupling. J. Chem. Phys. 120 (2004) 11726
    • (2004) J. Chem. Phys. , vol.120 , pp. 11726
    • Brinkmann, A.1    Eden, M.2
  • 47
    • 0035397081 scopus 로고    scopus 로고
    • Symmetry principles in the nuclear magnetic resonance of spinning solids: heteronuclear recoupling by generalized Hartmann-Hahn sequences
    • Brinkmann A., and Levitt M.H. Symmetry principles in the nuclear magnetic resonance of spinning solids: heteronuclear recoupling by generalized Hartmann-Hahn sequences. J. Chem. Phys. 115 (2001) 357
    • (2001) J. Chem. Phys. , vol.115 , pp. 357
    • Brinkmann, A.1    Levitt, M.H.2
  • 48
    • 55649120023 scopus 로고    scopus 로고
    • Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance
    • Leskes M., Steuernagel S., Schneider D., Madhu P.K., and Vega S. Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance. Chem. Phys. Lett. 466 (2008) 95
    • (2008) Chem. Phys. Lett. , vol.466 , pp. 95
    • Leskes, M.1    Steuernagel, S.2    Schneider, D.3    Madhu, P.K.4    Vega, S.5
  • 49
    • 0035983179 scopus 로고    scopus 로고
    • Homonuclear zero-quantum recoupling in fast magic-angle spinning nuclear magnetic resonance
    • Brinkmann A., auf der Günne J.S., and Levitt M.H. Homonuclear zero-quantum recoupling in fast magic-angle spinning nuclear magnetic resonance. J. Magn. Reson. 156 (2002) 79
    • (2002) J. Magn. Reson. , vol.156 , pp. 79
    • Brinkmann, A.1    auf der Günne, J.S.2    Levitt, M.H.3
  • 50
    • 36849069439 scopus 로고    scopus 로고
    • Coherence transfer between spy nuclei and nitrogen-14 in solids
    • Cavadini S., Abraham A., and Bodenhausen G. Coherence transfer between spy nuclei and nitrogen-14 in solids. J. Magn. Reson. 190 (2008) 160
    • (2008) J. Magn. Reson. , vol.190 , pp. 160
    • Cavadini, S.1    Abraham, A.2    Bodenhausen, G.3
  • 51
    • 50249187653 scopus 로고    scopus 로고
    • Evidence for dynamics on a 100 ns time scale from single- and double-quantum nitrogen-14 NMR in solid peptides
    • Cavadini S., Abraham A., Ulzega S., and Bodenhausen G. Evidence for dynamics on a 100 ns time scale from single- and double-quantum nitrogen-14 NMR in solid peptides. J. Am. Chem. Soc. 130 (2008) 10850
    • (2008) J. Am. Chem. Soc. , vol.130 , pp. 10850
    • Cavadini, S.1    Abraham, A.2    Ulzega, S.3    Bodenhausen, G.4
  • 52
    • 0009580882 scopus 로고
    • Investigations of a nonrandom numerical-method for multidimensional integration
    • Cheng V.B., Suzukawa H.H., and Wolfsberg M. Investigations of a nonrandom numerical-method for multidimensional integration. J. Chem. Phys. 59 (1973) 3992
    • (1973) J. Chem. Phys. , vol.59 , pp. 3992
    • Cheng, V.B.1    Suzukawa, H.H.2    Wolfsberg, M.3
  • 53
    • 36849108849 scopus 로고
    • Molecular Schrödinger equation. VIII. A new method for the evaluation of multidimensional integrals
    • Conroy H. Molecular Schrödinger equation. VIII. A new method for the evaluation of multidimensional integrals. J. Chem. Phys. 47 (1967) 5307
    • (1967) J. Chem. Phys. , vol.47 , pp. 5307
    • Conroy, H.1
  • 54
    • 33745379666 scopus 로고
    • Good lattice points, discrepancy, and numerical integration
    • Zaremba S.K. Good lattice points, discrepancy, and numerical integration. Ann. Mat. Pure Appl. 4-54 (1966) 325
    • (1966) Ann. Mat. Pure Appl. , vol.4-54 , pp. 325
    • Zaremba, S.K.1


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