Elimination of high order terms in multiple pulse nuclear magnetic resonance spectroscopy: Application to homonuclear decoupling in solids

Journal of Chemical Physics

Volumn 106, Issue 18, 1997, Pages 7571-7586

  Hohwy, M ^a   Nielsen, N C ^a  

^a AARHUS UNIVERSITY   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

COMPUTER SIMULATION; INTEGRAL EQUATIONS; PERTURBATION TECHNIQUES; PHASE SHIFT; QUANTUM THEORY; SOLIDS; TENSORS; HAMILTONIANS; MAGNETIC RESONANCE SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE;

COMMUTATOR RELATIONS; HIGH ORDER TRUNCATION DECOUPLING METHODS; MAGNUS EXPANSION; PULSE CYCLE DECOUPLING PRINCIPLE; Z ROTATIONAL DECOUPLING;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

HOMONUCLEAR DECOUPLING; MULTIPLE PULSE TECHNIQUE; ORDERS OF MAGNITUDE; PHASE SHIFTED PULSE; ROTATIONAL DECOUPLING; SOLID-STATE NUCLEAR MAGNETIC RESONANCE; STATE-OF-THE-ART METHODS; TIME-DEPENDENT PERTURBATION THEORY;

EID: 0031559298     PISSN: 00219606     EISSN: None     Source Type: Journal    
DOI: 10.1063/1.473760     Document Type: Article

References (48)

1. M. Lee and W. I. Goldburg, Phys. Rev. A 140, 1261 (1965).
2. J. S. Waugh, L. M. Huber, and U. Haeberlen, Phys. Rev. Lett. 20, 180 (1968).
3. U. Haeberlen and J. S. Waugh, Phys. Rev. 175, 453 (1968).
4. M. Mehring and J. S. Waugh, Phys. Rev. B 5, 3459 (1972).
5. M. Mehring, Rev. Sci. Instrum. 44, 64 (1973).
6. P. Mansfield, M. J. Orchard, D. C. Stalker, and K. H. B. Richards, Phys. Rev. B 7, 90 (1973).
7. W. -K. Rhim, D. D. Elleman, and R. W. Vaughan, J. Chem. Phys. 59, 3740 (1973).
8. W. -K. Rhim, D. D. Elleman, L. B. Schreiber, and R. W. Vaughan, J. Chem. Phys. 60, 4595 (1974).
9. D. P. Burum and W. -K. Rhim, J. Chem. Phys. 71, 944 (1979).
10. W. -K. Rhim, A. Pines, and J. S. Waugh, Phys. Rev. B 3, 684 (1971).
11. R. G. Pembleton, L. M. Ryan, and B. C. Gerstein, Rev. Sci. Instrum. 48, 1286 (1977).
12. R. E. Taylor, R. G. Pembleton, L. M. Ryan, and B. C. Gerstein, J. Chem. Phys. 71, 4541 (1979).
13. D. P. Burum, M. Linder, and R. R. Ernst, J. Magn. Reson. 44, 173 (1981).
14. K. Takegoshi and C. A. McDowell, Chem. Phys. Lett. 116, 100 (1985).
15. D. E. Demco, S. Hafner, and H. W. Spiess, J. Magn. Reson. A 116, 36 (1995).
16. D. G. Cory, J. Magn. Reson. 94, 526 (1991).
17. A. Bielecki, A. C. Kolbert, and M. H. Levitt, Chem. Phys. Lett. 155, 341 (1989).
18. M. H. Levitt, A. C. Kolbert, A. Bielecki, and D. J. Ruben, Sol. Stat. Nucl. Magn. Reson. 2, 151 (1993).
19. R. K. Hester, J. L. Ackerman, V. R. Cross, and J. S. Waugh, Phys. Rev. Lett. 34, 993 (1975).
20. J. S. Waugh, Proc. Natl. Acad. Sci. USA 73, 1394 (1976).
21. R. K. Hester, J. L. Ackerman, B. L. Neff, and J. S. Waugh, Phys. Rev. Lett. 36, 1081 (1976).
22. E. F. Rybaczewski, B. L. Neff, J. S. Waugh, and J. S. Sherfinski, J. Chem. Phys. 67, 1231 (1977).
23. T. Terao, H. Miura, and A. Saika, J. Chem. Phys. 75, 1573 (1981).
24. T. Terao, H. Miura, and A. Saika, J. Am. Chem. Soc. 104, 5228 (1982).
25. C. L. Mayne, R. J. Pugmire, and D. M. Grant, J. Magn. Reson. 56, 151 (1984).
26. H. Miura, T. Terao, and A. Saika, J. Magn. Reson. 68, 593 (1986).
27. K. Takegoshi and C. A. McDowell, J . Chem. Phys. 84, 2084 (1986).
28. P. Caravatti, G. Bodenhausen, and R. R. Ernst, Chem. Phys. Lett. 89, 363 (1982).
29. P. Caravatti, L. Braunschweiler, and R. R. Ernst, Chem. Phys. Lett. 100, 305 (1983).
30. J. E. Roberts, S. Vega, and R. G. Griffin, J. Am. Chem. Soc. 106, 2506 (1984).
31. D. P. Burum and A. Bielecki, J. Magn. Reson. 94, 645 (1991).
32. C. E. Bronnimann, C. F. Ridenour, D. R. Kinney, and G. E. Maciel, J. Magn. Reson. 97, 522 (1992).
33. A. Ramamoorthy, C. H. Wu, and S. J. Opella, J. Magn. Reson. B 107, 88 (1995)
34. A. Ramamoorthy, L. M. Gierasch, and S. J. Opella, J. Magn. Reson. B 109, 112 (1995).
35. U. Haeberlen, High-Resolution NMR in Solids. Selective Averaging (Academic, New York, 1976).
36. M. Mehring, Principles of High Resolution NMR of Solids, 2nd ed. (Springer, New York, 1983).
37. M. M. Maricq, Phys. Rev. B 25, 6622 (1982).
38. B. C. Gerstein and C. R. Dybowski, Transient Techniques in NMR of Solids (Academic, New York, 1985).
39. R. R. Ernst, G. Bodenhausen, and A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions (Clarendon, Oxford, 1987).
40. H. Liu, S. J. Glaser, and G. P. Drobny, J. Chem. Phys. 93, 7543 (1990).
41. It is noted that we in the following sections refer to orders as being one order larger which agrees with the ordering resulting from time dependent perturbation theory given in Section II B.
42. W. Magnus, Commun. Pure Appl. Math. 7, 649 (1954).
43. A. Messiah, Quantum Mechanics (North-Holland, Amsterdam, 1964).
44. D. P. Burum, Phys. Rev. B 24, 3684 (1981).
45. I. Bialynicki-Birula, B. Mielnik, and J. Plebański, Ann. Phys. 51, 187 (1969).
46. H. J. Jakobsen, P. Daugaard, and V. Langer, J. Magn. Reson, 76, 162 (1988).
47. N. C. Nielsen, H. Bildsøe, and H. J. Jakobsen, J. Magn. Reson. 98, 665 (1992).
48. A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569 (1973).