메뉴 건너뛰기




Volumn 199, Issue 2, 2009, Pages 208-213

Why does PMLG proton decoupling work at 65 kHz MAS?

Author keywords

Fast MAS; Floquet theory; Homonuclear dipolar decoupling; PMLG; Solid state NMR

Indexed keywords

FAST MAS; FLOQUET THEORY; HOMONUCLEAR DIPOLAR DECOUPLING; PMLG; SOLID-STATE NMR;

EID: 67649439149     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2009.05.003     Document Type: Article
Times cited : (33)

References (39)
  • 1
    • 0000127208 scopus 로고
    • Combined rotation and multiple pulse spectrosocpy as an analytical proton nuclear magnetic resonance technique for solids
    • Bronnimann C.E., Hawkins B.L., Zhang M., and Maciel G.E. Combined rotation and multiple pulse spectrosocpy as an analytical proton nuclear magnetic resonance technique for solids. Anal. Chem. 60 (1988) 1743-1750
    • (1988) Anal. Chem. , vol.60 , pp. 1743-1750
    • Bronnimann, C.E.1    Hawkins, B.L.2    Zhang, M.3    Maciel, G.E.4
  • 2
    • 0345665855 scopus 로고
    • Utility of pulse nuclear magnetic resonance in studying protons in coals
    • Gerstein B.C., Clor C., Pembelton R.G., and Wilson R.C. Utility of pulse nuclear magnetic resonance in studying protons in coals. J. Phys. Chem. 81 (1977) 565
    • (1977) J. Phys. Chem. , vol.81 , pp. 565
    • Gerstein, B.C.1    Clor, C.2    Pembelton, R.G.3    Wilson, R.C.4
  • 3
    • 25144503942 scopus 로고    scopus 로고
    • Strategies for high-resolution proton spectroscopy in solid-state NMR
    • Vinogradov E., Madhu P.K., and Vega S. Strategies for high-resolution proton spectroscopy in solid-state NMR. Topics Curr. Chem. 246 (2005) 33
    • (2005) Topics Curr. Chem. , vol.246 , pp. 33
    • Vinogradov, E.1    Madhu, P.K.2    Vega, S.3
  • 4
    • 36149055062 scopus 로고
    • Symmetrized pulse sequences in high resolution NMR in solids
    • Mansfield P. Symmetrized pulse sequences in high resolution NMR in solids. J. Phys. C Solid State Phys. 4 (1971) 1444
    • (1971) J. Phys. C Solid State Phys. , vol.4 , pp. 1444
    • Mansfield, P.1
  • 5
    • 33646620078 scopus 로고
    • Time-reversal experiments in dipolar-coupled spin systems
    • Rhim W.-K., Pines A., and Waugh J.S. Time-reversal experiments in dipolar-coupled spin systems. Phys. Rev. B3 (1971) 684-696
    • (1971) Phys. Rev. , vol.B3 , pp. 684-696
    • Rhim, W.-K.1    Pines, A.2    Waugh, J.S.3
  • 6
    • 0000204974 scopus 로고
    • Magic-angle NMR experiments in solids
    • Mehring M., and Waugh J.S. Magic-angle NMR experiments in solids. Phys. Rev. B5 (1972) 3459
    • (1972) Phys. Rev. , vol.B5 , pp. 3459
    • Mehring, M.1    Waugh, J.S.2
  • 7
  • 8
    • 36749120596 scopus 로고
    • Analysis of multiple pulse NMR in solids-part 3
    • Burum D.P., and Rhim W.-K. Analysis of multiple pulse NMR in solids-part 3. J. Chem. Phys. 71 (1979) 944-956
    • (1979) J. Chem. Phys. , vol.71 , pp. 944-956
    • Burum, D.P.1    Rhim, W.-K.2
  • 9
    • 0001579498 scopus 로고
    • An improved NMR technique for homonuclear dipolar decoupling in solids: application to polycrystalline ice
    • Burum D.P., and Rhim W.-K. An improved NMR technique for homonuclear dipolar decoupling in solids: application to polycrystalline ice. J. Chem. Phys. 70 (1979) 3553-3554
    • (1979) J. Chem. Phys. , vol.70 , pp. 3553-3554
    • Burum, D.P.1    Rhim, W.-K.2
  • 10
    • 0000511293 scopus 로고
    • Low-power multipulse line narrowing in solid-state NMR
    • Burum D.P., Linder M., and Ernst R.R. Low-power multipulse line narrowing in solid-state NMR. J. Magn. Reson. 44 (1981) 173-188
    • (1981) J. Magn. Reson. , vol.44 , pp. 173-188
    • Burum, D.P.1    Linder, M.2    Ernst, R.R.3
  • 11
    • 33646725943 scopus 로고
    • A "magic echo" pulse sequence for the high-resolution NMR spectra of abundant spins in solids
    • Takegoshi K., and McDowell C.A. A "magic echo" pulse sequence for the high-resolution NMR spectra of abundant spins in solids. Chem. Phys. Lett. 116 (1985) 100-104
    • (1985) Chem. Phys. Lett. , vol.116 , pp. 100-104
    • Takegoshi, K.1    McDowell, C.A.2
  • 12
    • 0000125327 scopus 로고
    • A new multiple-pulse cycle for homonuclear dipolar decoupling
    • Cory D.G. A new multiple-pulse cycle for homonuclear dipolar decoupling. J. Magn. Reson. 94 (1991) 526-534
    • (1991) J. Magn. Reson. , vol.94 , pp. 526-534
    • Cory, D.G.1
  • 13
    • 0031559298 scopus 로고    scopus 로고
    • Elimination of high order terms in multiple pulse nuclear magnetic resonance spectroscopy: application to homonuclear decoupling in solids
    • Hohwy M., and Nielsen N.C. Elimination of high order terms in multiple pulse nuclear magnetic resonance spectroscopy: application to homonuclear decoupling in solids. J. Chem. Phys. 106 (1997) 7571-7586
    • (1997) J. Chem. Phys. , vol.106 , pp. 7571-7586
    • Hohwy, M.1    Nielsen, N.C.2
  • 14
    • 0031586188 scopus 로고    scopus 로고
    • A high-order and broadband CRAMPS experiment using z-rotational decoupling
    • Hohwy M., Bower P.V., Jakobsen H.J., and Nielsen N.C. A high-order and broadband CRAMPS experiment using z-rotational decoupling. Chem. Phys. Lett. 273 (1997) 297-303
    • (1997) Chem. Phys. Lett. , vol.273 , pp. 297-303
    • Hohwy, M.1    Bower, P.V.2    Jakobsen, H.J.3    Nielsen, N.C.4
  • 15
    • 0000227547 scopus 로고    scopus 로고
    • High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment
    • Vinogradov E., Madhu P.K., and Vega S. High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment. Chem. Phys. Lett. 314 (1999) 443-450
    • (1999) Chem. Phys. Lett. , vol.314 , pp. 443-450
    • Vinogradov, E.1    Madhu, P.K.2    Vega, S.3
  • 16
    • 0035890370 scopus 로고    scopus 로고
    • Phase modulated Lee-Goldburg magic angle spinning proton nuclear magnetic resonance experiments in the solid state: a bimodal Floquet theoretical treatment
    • Vinogradov E., Madhu P.K., and Vega S. Phase modulated Lee-Goldburg magic angle spinning proton nuclear magnetic resonance experiments in the solid state: a bimodal Floquet theoretical treatment. J. Chem. Phys. 115 (2001) 8983-9000
    • (2001) J. Chem. Phys. , vol.115 , pp. 8983-9000
    • Vinogradov, E.1    Madhu, P.K.2    Vega, S.3
  • 17
    • 0000204974 scopus 로고
    • Magic-angle NMR experiments in solids
    • Mehring M., and Waugh J.S. Magic-angle NMR experiments in solids. Phys. Rev. B5 (1972) 3459-3471
    • (1972) Phys. Rev. , vol.B5 , pp. 3459-3471
    • Mehring, M.1    Waugh, J.S.2
  • 18
    • 0027671249 scopus 로고
    • High-resolution 1H NMR in solids with frequency-switched multiple-pulse sequences
    • Levitt M.H., Bielecki A., Kolbert A.C., and Ruben D.J. High-resolution 1H NMR in solids with frequency-switched multiple-pulse sequences. Solid State NMR 2 (1993) 151-163
    • (1993) Solid State NMR , vol.2 , pp. 151-163
    • Levitt, M.H.1    Bielecki, A.2    Kolbert, A.C.3    Ruben, D.J.4
  • 19
    • 0001315175 scopus 로고    scopus 로고
    • Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation
    • Sakellariou D., Lesage A., Hodgkinson P., and Emsley L. Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation. Chem. Phys. Lett. 319 (2000) 253-260
    • (2000) Chem. Phys. Lett. , vol.319 , pp. 253-260
    • Sakellariou, D.1    Lesage, A.2    Hodgkinson, P.3    Emsley, L.4
  • 20
    • 34249088004 scopus 로고    scopus 로고
    • Probing proton-proton proximities in the solid state
    • Brown S.P. Probing proton-proton proximities in the solid state. Prog. Nucl. Magn. Reson. Spectrosc. 50 (2007) 199-251
    • (2007) Prog. Nucl. Magn. Reson. Spectrosc. , vol.50 , pp. 199-251
    • Brown, S.P.1
  • 21
    • 0037066031 scopus 로고    scopus 로고
    • Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences
    • Vinogradov E., Madhu P.K., and Vega S. Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences. Chem. Phys. Lett. 354 (2002) 193-202
    • (2002) Chem. Phys. Lett. , vol.354 , pp. 193-202
    • Vinogradov, E.1    Madhu, P.K.2    Vega, S.3
  • 22
    • 0043175468 scopus 로고    scopus 로고
    • Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling
    • Lesage A., Sakellariou D., Hedier S., Elena B., Charmont P., Steuerngel S., and Emsley L. Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling. J. Magn. Reson. 163 (2003) 105-113
    • (2003) J. Magn. Reson. , vol.163 , pp. 105-113
    • Lesage, A.1    Sakellariou, D.2    Hedier, S.3    Elena, B.4    Charmont, P.5    Steuerngel, S.6    Emsley, L.7
  • 24
    • 0035965185 scopus 로고    scopus 로고
    • High-resolution 1H NMR in the solid state using symmetry-based pulse sequences
    • Madhu P.K., Zhao X., and Levitt M.H. High-resolution 1H NMR in the solid state using symmetry-based pulse sequences. Chem. Phys. Lett. 346 (2001) 142-148
    • (2001) Chem. Phys. Lett. , vol.346 , pp. 142-148
    • Madhu, P.K.1    Zhao, X.2    Levitt, M.H.3
  • 25
    • 42249115493 scopus 로고    scopus 로고
    • 1H homonuclear dipolar decoupling at high magic-angle spinning frequencies with rotor-synchronised symmetry sequences
    • Paul S., Thakur R.S., and Madhu P.K. 1H homonuclear dipolar decoupling at high magic-angle spinning frequencies with rotor-synchronised symmetry sequences. Chem. Phys. Lett. 456 (2008) 253-256
    • (2008) Chem. Phys. Lett. , vol.456 , pp. 253-256
    • Paul, S.1    Thakur, R.S.2    Madhu, P.K.3
  • 26
    • 47549096967 scopus 로고    scopus 로고
    • Enhanced resolution in proton solid-state NMR with very-fast MAS experiments
    • Amoureux J.P., Hu B., and Trebosc J. Enhanced resolution in proton solid-state NMR with very-fast MAS experiments. J. Magn. Reson. 193 (2008) 305-307
    • (2008) J. Magn. Reson. , vol.193 , pp. 305-307
    • Amoureux, J.P.1    Hu, B.2    Trebosc, J.3
  • 27
    • 58849159099 scopus 로고    scopus 로고
    • Homonuclear dipolar decoupling schemes for fast MAS
    • Amoureux J.P., Hu B., Trebosc J., and Deng F. Homonuclear dipolar decoupling schemes for fast MAS. Solid State NMR 35 (2009) 19-24
    • (2009) Solid State NMR , vol.35 , pp. 19-24
    • Amoureux, J.P.1    Hu, B.2    Trebosc, J.3    Deng, F.4
  • 28
    • 55649120023 scopus 로고    scopus 로고
    • Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance
    • Leskes M., Steuernagel S., Schneider D., Madhu P.K., and Vega S. Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance. Chem. Phys. Lett. 466 (2008) 95-99
    • (2008) Chem. Phys. Lett. , vol.466 , pp. 95-99
    • Leskes, M.1    Steuernagel, S.2    Schneider, D.3    Madhu, P.K.4    Vega, S.5
  • 29
    • 59249104564 scopus 로고    scopus 로고
    • Enhanced sensitivity in high-resolution 1H solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS
    • Salager E., Stein R.S., Steuernagel S., Lesage A., Elena B., and Emsley L. Enhanced sensitivity in high-resolution 1H solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS. Chem. Phys. Lett. 469 (2009) 336-341
    • (2009) Chem. Phys. Lett. , vol.469 , pp. 336-341
    • Salager, E.1    Stein, R.S.2    Steuernagel, S.3    Lesage, A.4    Elena, B.5    Emsley, L.6
  • 30
    • 36149022366 scopus 로고
    • Solution of the Schrodinger equation with a Hamiltonian periodic in time
    • Shirley J.H. Solution of the Schrodinger equation with a Hamiltonian periodic in time. Phy. Rev. B138 (1965) 979-987
    • (1965) Phy. Rev. , vol.B138 , pp. 979-987
    • Shirley, J.H.1
  • 31
    • 0004974066 scopus 로고    scopus 로고
    • Floquet theory
    • Grant D.M., and Harris R.K. (Eds), John Wiley & Sons, Chichester
    • Vega S. Floquet theory. In: Grant D.M., and Harris R.K. (Eds). Encyc. of NMR (1996), John Wiley & Sons, Chichester
    • (1996) Encyc. of NMR
    • Vega, S.1
  • 32
    • 0002960267 scopus 로고
    • Recouling of homo-heteronuclear dipolar interactions in rotating solids
    • Bennett A.E., Griffin R.G., and Vega S. Recouling of homo-heteronuclear dipolar interactions in rotating solids. NMR Basic Princ. Prog. 33 (1994) 1-77
    • (1994) NMR Basic Princ. Prog. , vol.33 , pp. 1-77
    • Bennett, A.E.1    Griffin, R.G.2    Vega, S.3
  • 33
    • 0001267241 scopus 로고    scopus 로고
    • A physical interpretation of the Floquet description of magic angle spinning nuclear magnetic resonance spectroscopy
    • Boender G.J., Vega S., and De Groot H.J.M. A physical interpretation of the Floquet description of magic angle spinning nuclear magnetic resonance spectroscopy. Mol. Phys. 95 (1998) 921-934
    • (1998) Mol. Phys. , vol.95 , pp. 921-934
    • Boender, G.J.1    Vega, S.2    De Groot, H.J.M.3
  • 34
    • 0347929584 scopus 로고
    • On U3c3-type doubling and electron spin in the spectra of diatomic molecules
    • van Vleck J.H. On U3c3-type doubling and electron spin in the spectra of diatomic molecules. Phys. Rev. 33 (1929) 467-506
    • (1929) Phys. Rev. , vol.33 , pp. 467-506
    • van Vleck, J.H.1
  • 35
    • 35248833771 scopus 로고    scopus 로고
    • A broad-banded z-rotation windowed phase-modulated Lee-Goldburg pulse sequence for 1H spectroscopy in solid-state NMR
    • Leskes M., Madhu P.K., and Vega S. A broad-banded z-rotation windowed phase-modulated Lee-Goldburg pulse sequence for 1H spectroscopy in solid-state NMR. Chem. Phys. Lett. 447 (2007) 370-374
    • (2007) Chem. Phys. Lett. , vol.447 , pp. 370-374
    • Leskes, M.1    Madhu, P.K.2    Vega, S.3
  • 36
    • 42649111299 scopus 로고    scopus 로고
    • Supercycled homonuclear dipolar decoupling in solid-state NMR: toward cleaner 1H spectrum and higher spinning rates
    • Leskes M., Madhu P.K., and Vega S. Supercycled homonuclear dipolar decoupling in solid-state NMR: toward cleaner 1H spectrum and higher spinning rates. J. Chem. Phys. 128 (2008) 52309-52320
    • (2008) J. Chem. Phys. , vol.128 , pp. 52309-52320
    • Leskes, M.1    Madhu, P.K.2    Vega, S.3
  • 37
    • 30844458347 scopus 로고    scopus 로고
    • SPINEVOLUTION: a powerful tool for the simulation of solid and liquid state NMR experiments
    • Veshtort M., and Griffin R.G. SPINEVOLUTION: a powerful tool for the simulation of solid and liquid state NMR experiments. J. Magn. Reson. 178 (2006) 248-282
    • (2006) J. Magn. Reson. , vol.178 , pp. 248-282
    • Veshtort, M.1    Griffin, R.G.2
  • 38
    • 33749246021 scopus 로고    scopus 로고
    • Proton line narrowing in solid-state nuclear magnetic resonance: new insights from windowed phase-modulated Lee-Goldburg sequence
    • Leskes M., Madhu P.K., and Vega S. Proton line narrowing in solid-state nuclear magnetic resonance: new insights from windowed phase-modulated Lee-Goldburg sequence. J. Chem. Phys. 125 (2006) 124506-124524
    • (2006) J. Chem. Phys. , vol.125 , pp. 124506-124524
    • Leskes, M.1    Madhu, P.K.2    Vega, S.3
  • 39
    • 2942562536 scopus 로고    scopus 로고
    • Improvement of homonuclear dipolar decoupling sequences in solid-state nuclear magnetic resonance utilising radiofrequency imperfections
    • Bosman L., Madhu P.K., Vega S., and Vinogradov E. Improvement of homonuclear dipolar decoupling sequences in solid-state nuclear magnetic resonance utilising radiofrequency imperfections. J. Magn. Reson. 169 (2004) 39-48
    • (2004) J. Magn. Reson. , vol.169 , pp. 39-48
    • Bosman, L.1    Madhu, P.K.2    Vega, S.3    Vinogradov, E.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.