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Volumn 4, Issue SUPPL.1, 2012, Pages 10-16

Guidelines for the validation of qualitative multi-residue methods used to detect pesticides in food

Author keywords

Food; Method validation; Multi residue methods; Pesticides; Qualitative

Indexed keywords

CHEMICAL CONTAMINATION; GAS CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

EID: 84864409339     PISSN: 19427603     EISSN: 19427611     Source Type: Journal    
DOI: 10.1002/dta.1364     Document Type: Article
Times cited : (9)

References (20)
  • 1
    • 85152997653 scopus 로고    scopus 로고
    • Codex Alimentarius, Pesticide Residues in Food, Maximum Residue Limits. Available at: [Accessed 5 April 2012].
    • Codex Alimentarius, Pesticide Residues in Food, Maximum Residue Limits. Available at: [Accessed 5 April 2012].
  • 2
    • 85152988029 scopus 로고    scopus 로고
    • Regulation (EC) NO 396/2005 of the European Parliament and the council of 23 February 2005, on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC, OJEU, L70 1-16. Available at: [Accessed on 5 April 2012].
    • Regulation (EC) NO 396/2005 of the European Parliament and the council of 23 February 2005, on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC, OJEU, L70 1-16. Available at: [Accessed on 5 April 2012].
  • 3
    • 84875137269 scopus 로고    scopus 로고
    • v5.1, BCPC Publishers: UK
    • The e-Pesticide Manual v5.1, BCPC Publishers: UK, 2010.
    • (2010) The e-Pesticide Manual
  • 4
    • 0034665350 scopus 로고    scopus 로고
    • Pesticide residue analysis in foodstuffs applying capillary gas chromatography with mass spectrometric detection State-of-the-art use of modified DFG-multimethod S19 and automated data evaluation
    • H.-J. Stan. Pesticide residue analysis in foodstuffs applying capillary gas chromatography with mass spectrometric detection State-of-the-art use of modified DFG-multimethod S19 and automated data evaluation. J. Chromatogr. A 2000, 829, 347.
    • (2000) J. Chromatogr. A , vol.829 , pp. 347
    • Stan, H.-J.1
  • 5
    • 77950042977 scopus 로고    scopus 로고
    • Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables
    • S.J. Lehotay, K.A. Son, H. Kwon, U. Koesukwiwat, W. Fu, K. Mastovska, et al. Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables. J. Chromatogr. A 2010, 1217, 2548.
    • (2010) J. Chromatogr. A , vol.1217 , pp. 2548
    • Lehotay, S.J.1    Son, K.A.2    Kwon, H.3    Koesukwiwat, U.4    Fu, W.5    Mastovska, K.6
  • 6
    • 36849070798 scopus 로고    scopus 로고
    • Modification and re-validation of the ethyl acetate-based multi-residue method for pesticides in produce
    • H.G.J. Mol, A. Rooseboom, R. van Dam, M. Roding, K. Arondeus, S. Sunarto. Modification and re-validation of the ethyl acetate-based multi-residue method for pesticides in produce. Anal. Bioanal. Chem. 2007, 389, 1715.
    • (2007) Anal. Bioanal. Chem. , vol.389 , pp. 1715
    • Mol, H.G.J.1    Rooseboom, A.2    van Dam, R.3    Roding, M.4    Arondeus, K.5    Sunarto, S.6
  • 7
    • 36849079273 scopus 로고    scopus 로고
    • Analysis of pesticide residues in fruit and vegetables with ethyl acetate extraction using gas and liquid chromatography with tandem mass spectrometric detection
    • T. Pihlström, G. Blomkvist, P. Friman, U. Pagard, B.-G. Österdahl. Analysis of pesticide residues in fruit and vegetables with ethyl acetate extraction using gas and liquid chromatography with tandem mass spectrometric detection. Anal. Bioanal. Chem. 2007, 389, 1773.
    • (2007) Anal. Bioanal. Chem. , vol.389 , pp. 1773
    • Pihlström, T.1    Blomkvist, G.2    Friman, P.3    Pagard, U.4    Österdahl, B.-G.5
  • 8
    • 85152983279 scopus 로고    scopus 로고
    • Intercomparison study of two multi-residue methods for the enforcement of EU MRLs for pesticide residues in fruit, vegetables and grain. Phase IV Intercomparison Study of Test materials Containing Incurred Residues. Report EUR 19443
    • Intercomparison study of two multi-residue methods for the enforcement of EU MRLs for pesticide residues in fruit, vegetables and grain. Phase IV Intercomparison Study of Test materials Containing Incurred Residues. Report EUR 19443, 2001.
    • (2001)
  • 9
    • 85152995856 scopus 로고    scopus 로고
    • SANCO/12495/2011, Method Validation and Quality Control Procedures for Pesticide Residues Analysis in Food and Feed. Available at: [Accessed on 5 April 2012].
    • SANCO/12495/2011, Method Validation and Quality Control Procedures for Pesticide Residues Analysis in Food and Feed. Available at: [Accessed on 5 April 2012].
  • 10
    • 85153025281 scopus 로고    scopus 로고
    • OECD Environment, Health and Safety Publications, Series on testing and Assessment, No.72 and Series on Pesticides No. 39, Guidance document on pesticide residue analytical methods, ENV/JM/MONO. Available at: [Accessed on 5 April 2012].
    • OECD Environment, Health and Safety Publications, Series on testing and Assessment, No.72 and Series on Pesticides No. 39, Guidance document on pesticide residue analytical methods, ENV/JM/MONO. Available at: [Accessed on 5 April 2012].
  • 11
    • 0033037860 scopus 로고    scopus 로고
    • Guidelines for in-house validation of analytical methods for pesticide residues in food and animal feeds
    • A.R.C. Hill, S.L. Reynolds. Guidelines for in-house validation of analytical methods for pesticide residues in food and animal feeds. Analyst 1999, 124, 953.
    • (1999) Analyst , vol.124 , pp. 953
    • Hill, A.R.C.1    Reynolds, S.L.2
  • 12
    • 34249851036 scopus 로고    scopus 로고
    • Measurement uncertainty associated with sample processing of oranges and tomatoes for pesticide residues analysis
    • R.J. Fussell, M.T. Hetmanski, R. Macarthur, D. Findlay, F. Smith, Á. Ambrus, et al. Measurement uncertainty associated with sample processing of oranges and tomatoes for pesticide residues analysis. J. Agric. Food Chem. 2007, 55, 1062.
    • (2007) J. Agric. Food Chem. , vol.55 , pp. 1062
    • Fussell, R.J.1    Hetmanski, M.T.2    Macarthur, R.3    Findlay, D.4    Smith, F.5    Ambrus, A.6
  • 13
    • 42049094441 scopus 로고    scopus 로고
    • Optimisation of programmable temperature vaporiser-based large volume injection for determination of pesticide residues in fruits and vegetables using gas chromatography-mass spectrometry
    • D. Štajnbaher, L. Zupančič-Kralj. Optimisation of programmable temperature vaporiser-based large volume injection for determination of pesticide residues in fruits and vegetables using gas chromatography-mass spectrometry. J. Chromatogr. A 2008, 1190, 316.
    • (2008) J. Chromatogr. A , vol.1190 , pp. 316
    • Štajnbaher, D.1    Zupančič-Kralj, L.2
  • 14
    • 85153000325 scopus 로고    scopus 로고
    • Screening for 926 pesticides and endocrine disruptors by GC/MS with deconvolution reportins Software and a new pesticide library. Agilent Application Note 2006, 5989-5076EN.
    • P.L. Wylie. Screening for 926 pesticides and endocrine disruptors by GC/MS with deconvolution reportins Software and a new pesticide library. Agilent Application Note 2006, 5989-5076EN.
    • Wylie, P.L.1
  • 15
    • 76149096872 scopus 로고    scopus 로고
    • Simultaneous screening and target analytical approach by gas chromatography-quadrupole-mass spectrometry for pesticide residues in fruits and vegetables
    • M. Mezcua, M.A. Martinez-Uroz, P.L. Wylie, A.R. Fernandez-Alba. Simultaneous screening and target analytical approach by gas chromatography-quadrupole-mass spectrometry for pesticide residues in fruits and vegetables. J. AOAC Int. 2009, 92, 1790.
    • (2009) J. AOAC Int. , vol.92 , pp. 1790
    • Mezcua, M.1    Martinez-Uroz, M.A.2    Wylie, P.L.3    Fernandez-Alba, A.R.4
  • 16
    • 77349105487 scopus 로고    scopus 로고
    • Independent evaluation of a commercial deconvolution reporting software for gas chromatography mass spectrometry analysis of pesticide residues in fruits and vegetables
    • H.R. Norli, A. Christiansen, B. Hole. Independent evaluation of a commercial deconvolution reporting software for gas chromatography mass spectrometry analysis of pesticide residues in fruits and vegetables. J. Chromatogr. A 2010, 1217, 2056.
    • (2010) J. Chromatogr. A , vol.1217 , pp. 2056
    • Norli, H.R.1    Christiansen, A.2    Hole, B.3
  • 17
    • 16644403077 scopus 로고    scopus 로고
    • Use of buffering and other means to improve results of problematic pesticides in a fast and easy method for residue analysis of fruits and vegetables
    • S.J. Lehotay, K. Maštovska, A.R. Lightfield. Use of buffering and other means to improve results of problematic pesticides in a fast and easy method for residue analysis of fruits and vegetables. J. AOAC Int. 2005, 88, 615.
    • (2005) J. AOAC Int. , vol.88 , pp. 615
    • Lehotay, S.J.1    Maštovska, K.2    Lightfield, A.R.3
  • 18
    • 36849020950 scopus 로고    scopus 로고
    • Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometer
    • P. Paya, M. Anastassiades, D. Mack, I. Sigalova, B. Tasdelen, J. Oliva, et al. Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometer. Anal. Bioanal. Chem. 2007, 389, 1697.
    • (2007) Anal. Bioanal. Chem. , vol.389 , pp. 1697
    • Paya, P.1    Anastassiades, M.2    Mack, D.3    Sigalova, I.4    Tasdelen, B.5    Oliva, J.6
  • 19
    • 61449150478 scopus 로고    scopus 로고
    • Accurate-mass databases for comprehensive screening of pesticide residues in food by fast liquid chromatography time-of-flight mass spectrometry
    • M. Mezua, O. Malato, J.F. García-Reyes, A. Molina-Díaz, A.R. Fernández-Alba. Accurate-mass databases for comprehensive screening of pesticide residues in food by fast liquid chromatography time-of-flight mass spectrometry. Anal. Chem. 2009, 81, 913.
    • (2009) Anal. Chem. , vol.81 , pp. 913
    • Mezua, M.1    Malato, O.2    García-Reyes, J.F.3    Molina-Díaz, A.4    Fernández-Alba, A.R.5
  • 20
    • 79960616633 scopus 로고    scopus 로고
    • Validation of automated library-based qualitative screening of pesticides by comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry
    • accepted for publication.
    • H.G.J. Mol, H. van der Kamp, G. van der Weg, M. van der Lee, A. Punt, T.C. de Rijk. Validation of automated library-based qualitative screening of pesticides by comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry. J. AOAC Int. 2011, accepted for publication.
    • (2011) J. AOAC Int.
    • Mol, H.G.J.1    van der Kamp, H.2    van der Weg, G.3    van der Lee, M.4    Punt, A.5    de Rijk, T.C.6


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