Recoupled separated-local-field experiments and applications to study intermediate-regime molecular motions

Journal of Magnetic Resonance

Volumn 221, Issue , 2012, Pages 85-96

  Cobo, Marcio Fernando ^a   Achilles, Anja ^b   Reichert, Detlef ^b   Deazevedo, Eduardo Ribeiro ^a   Saalwächter, Kay ^b  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

^b MARTIN LUTHER UNIVERSITY HALLE WITTENBERG   (Germany)

Author keywords

Dipolar couplings; DIPSHIFT; Dynamics; Organic solids

Indexed keywords

ANALYTICAL CALCULATION; DIPOLAR COUPLINGS; DIPSHIFT; DYNAMICS SIMULATION; EXPERIMENTAL CONDITIONS; LITERATURE DATA; MOLECULAR MOTIONS; ORGANIC SOLIDS; PROTON DECOUPLING; PULSE TRAIN; RECOUPLING; SEPARATED LOCAL FIELDS;

COUPLINGS; DYNAMICS; EXPERIMENTS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

SEPARATION;

EID: 84864184035     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2012.05.003     Document Type: Article

References (34)

1. G.C. Faria, R.M. Faria, E.R. deAzevedo, and H. von Seggern Temperature dependence of the drift mobility of poly(9,9'-dioctylfluorene-co- benzothiadiazole)-based thin-film devices J. Phys. Chem. C 115 51 2011 25479 25483
2. G.C. Faria, T.S. Plivelic, R.F. Cossiello, A.A. Souza, T.D.Z. Atvars, I.L. Torriani, and E.R. deAzevedo A multitechnique study of structure and dynamics of polyfluorene cast films and the influence on their photoluminescence J. Phys. Chem. B 113 33 2009 11403 11413
3. 1H NMR Macromolecules 44 11 2011 4017 4021
4. J.L. Valentin, P. Posadas, A. Fernandez-Torres, M.A. Malmierca, L. Gonzalez, W. Chasse, and K. Saalwächter Inhomogeneities and chain dynamics in diene rubbers vulcanized with different cure systems Macromolecules 43 9 2010 4210 4222
5. M. Hong, and Y.C. Su Structure and dynamics of cationic membrane peptides and proteins: insights from solid-state NMR Protein Sci. 20 4 2011 641 655
6. V. Andronis, and G. Zografi The molecular mobility of supercooled amorphous indomethacin as a function of temperature and relative humidity Pharm. Res. 15 6 1998 835 842 (Pubitemid 28307823)
7. 3 glass Phys. Rev. B 77 10 2008 104301
8. 15N-exchange NMR Chem. Phys. Lett. 321 1-2 2000 43 48
9. A.G. Palmer, C.D. Kroenke, and J.P. Loria Nuclear magnetic resonance methods for quantifying microsecond-to-millisecond motions in biological macromolecules Methods Enzymol. 339 2001 204 238 (Pubitemid 32666562)
10. A. Krushelnitsky, E. deAzevedo, R. Linser, B. Reif, K. Saalwächter, and D. Reichert Direct observation of millisecond to second motions in proteins by dipolar CODEX NMR spectroscopy J. Am. Chem. Soc. 131 34 2009 12097 12099
11. F. Lange, K. Schwenke, M. Kurakazu, Y. Akagi, U.I. Chung, M. Lane, J.U. Sommer, T. Sakai, and K. Saalwächter Connectivity and structural defects in model hydrogels: a combined proton NMR and Monte Carlo simulation study Macromolecules 44 24 2011 9666 9674
12. M. Munowitz, R.G. Griffin, G. Bodenhausen, and T.H. Huang Two-dimensional rotational spin-echo nuclear magnetic resonance in solids: correlation of chemical shift and dipolar interaction J. Am. Chem. Soc. 103 1981 2529 2533
13. E.R. deAzevedo, K. Saalwächter, O. Pascui, A.A. De Souza, T.J. Bonagamba, and D. Reichert Intermediate motions as studied by solid-state separated local field NMR experiments J. Chem. Phys. 128 10 2008 104505
14. W.P. Rothwell, and J.S. Waugh Transverse relaxation of dipolar coupled spin systems under rf-irradiation - detecting motions in solids J. Chem. Phys. 74 5 1981 2721 2732
15. M. Hong, J.D. Gross, C.M. Rienstra, R.G. Griffin, K.K. Kumashiro, and K. Schmidt-Rohr Coupling amplification in 2D MAS NMR and its application to torsion angle determination in peptides J. Magn. Reson. 129 1 1997 85 92 (Pubitemid 127454056)
16. T. Gullion, and J. Schaefer Rotational-echo double-resonance NMR J. Magn. Reson. 81 1 1989 196 200
17. D. Huster, L.S. Xiao, and M. Hong Solid-state NMR investigation of the dynamics of the soluble and membrane-bound colicin Ia channel-forming domain Biochemistry 40 25 2001 7662 7674 (Pubitemid 32578030)
18. D. Reichert, O. Pascui, E.R. deAzevedo, T.J. Bonagamba, K. Arnold, and D. Huster A solid-state NMR study of the fast and slow dynamics of collagen fibrils at varying hydration levels Magn. Reson. Chem. 42 2 2004 276 284 (Pubitemid 38178097)
19. G. Zernia, and D. Huster Collagen dynamics in articular cartilage under osmotic pressure NMR Biomed. 19 8 2006 1010 1019 (Pubitemid 46017722)
20. T. Suga, S. Wi, and T.E. Long Synthesis of diazocine-containing poly(arylene ether sulfone)s for tailored mechanical and electrochemical performance Macromolecules 42 5 2009 1526 1532
21. 13C solid-state NMR Magn. Reson. Chem. 48 9 2010 704 711
22. J.-X. Lu, S. Sharpe, R. Ghirlando, W.-M. Yau, and R. Tycko Oligomerization state and supramolecular structure of the HIV-1 Vpu protein transmembrane segment in phospholipid bilayers Protein Sci. 19 10 2010 1877 1896
23. M. Mehring High Resolution NMR of Solids 1983 Springer-Verlag Berlin
24. M. Veshtort, and R.G. Griffin SPINEVOLUTION: a powerful tool for the simulation of solid and liquid state NMR experiments J. Magn. Reson. 178 2 2006 248 282 (Pubitemid 43107933)
25. M.J. Duer Introduction to Solid-State NMR Spectroscopy 2004 Blackwell Publishing Ltd. Oxford
26. K. Takegoshi, and K. Hikichi Effects of blending on local chain dynamics and glass-transition - polystyrene poly(vinyl methyl-ether) blends as studied by high-resolution solid-State C-13 nuclear-magnetic-resonance spectroscopy J. Chem. Phys. 94 4 1991 3200 3206
27. T.G. Oas, R.G. Griffin, and M.H. Levitt Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic resonance spectroscopy J. Chem. Phys. 89 2 1988 692 695
28. 13C-heteronuclear correlation NMR in solids J. Magn. Reson. 149 1 2001 139 143
29. P. Barre, S. Yamaguchi, H. Saito, and D. Huster Backbone dynamics of bacteriorhodopsin as studied by C-13 solid-state NMR spectroscopy Eur. Biophys. J. Biophys. Lett. 32 6 2003 578 584 (Pubitemid 37408661)
30. 15N heteronuclear dipolar recoupling by R-symmetry sequences under fast magic angle spinning for dynamics analysis of biological and organic solids J. Am. Chem. Soc. 133 46 2011 18646 18655
31. M. Lee, and W.I. Goldburg Nuclear-magnetic-resonance line narrowing by a rotating Rf field Phys. Rev. 140 4A 1965 1261 1268
32. J.R. Long, B.Q. Sun, A. Bowen, and R.G. Griffin Molecular dynamics and magic angle spinning NMR J. Am. Chem. Soc. 116 1994 11950 11956
33. M.F. Cobo, K. Malinakova, D. Reichert, K. Saalwächter, and E.R. DeAzevedo Intermediate motions and dipolar couplings as studied by Lee-Goldburg cross-polarization NMR: Hartmann-Hahn matching profiles Phys. Chem. Chem. Phys. 11 32 2009 7036 7047
34. L.J. Schwartz, E. MeirovHch, J.A. Ripmeester, and J.H. Freed Quadrupole echo study of internal motions in polycrystalline media J. Phys. Chem. 87 22 1983 4446 4453