메뉴 건너뛰기




Volumn 129, Issue 1, 1997, Pages 85-92

Coupling Amplification in 2D MAS NMR and Its Application to Torsion Angle Determination in Peptides

Author keywords

Dipolar coupling; Magic angle spinning; Peptide structure; Solid state NMR; Torsion angle

Indexed keywords

PEPTIDE;

EID: 0031264701     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.1997.1242     Document Type: Article
Times cited : (131)

References (33)
  • 1
    • 0001444750 scopus 로고
    • Measurement of heteronuclear bond distances in polycrystalline solids by solid-state NMR techniques
    • J. E. Roberts, G. S. Harbison, M. G. Munowitz, J. Herzfeld, and R. G. Griffin, Measurement of heteronuclear bond distances in polycrystalline solids by solid-state NMR techniques, J. Am. Chem. Soc. 109, 4163-4169 (1987).
    • (1987) J. Am. Chem. Soc. , vol.109 , pp. 4163-4169
    • Roberts, J.E.1    Harbison, G.S.2    Munowitz, M.G.3    Herzfeld, J.4    Griffin, R.G.5
  • 2
    • 0346168028 scopus 로고
    • Orientation of tensorial interactions determined from two dimensional NMR powder spectra
    • M. Linder, A. Hoehener, and R. R. Ernst, Orientation of tensorial interactions determined from two dimensional NMR powder spectra, J. Chem. Phys. 73, 4959-4970 (1980).
    • (1980) J. Chem. Phys. , vol.73 , pp. 4959-4970
    • Linder, M.1    Hoehener, A.2    Ernst, R.R.3
  • 3
    • 33845557418 scopus 로고
    • Two-dimensional rotational spin-echo NMR in solids: Correlation of chemical shift and dipolar interactions
    • M. G. Munowitz, R. G. Griffin, G. Bodenhausen, and T. H. Huang, Two-dimensional rotational spin-echo NMR in solids: Correlation of chemical shift and dipolar interactions, J. Am. Chem. Soc. 103, 2529-2533 (1981).
    • (1981) J. Am. Chem. Soc. , vol.103 , pp. 2529-2533
    • Munowitz, M.G.1    Griffin, R.G.2    Bodenhausen, G.3    Huang, T.H.4
  • 4
    • 0029274597 scopus 로고
    • Measurement of signs and magnitudes of C-H dipolar couplings in lecithin
    • M. Hong, K. Schmidt-Rohr, and A. Pines, Measurement of signs and magnitudes of C-H dipolar couplings in lecithin, J. Am. Chem. Soc. 117, 3310-3311 (1995).
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 3310-3311
    • Hong, M.1    Schmidt-Rohr, K.2    Pines, A.3
  • 5
    • 0031051178 scopus 로고    scopus 로고
    • Dipolar recoupling in MAS NMR: A probe for segmental order in lipid bilayers
    • J. D. Gross, D. E. Waschawski, and R. G. Griffin, Dipolar recoupling in MAS NMR: A probe for segmental order in lipid bilayers, J. Am. Chem. Soc. 119, 796-802 (1997).
    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 796-802
    • Gross, J.D.1    Waschawski, D.E.2    Griffin, R.G.3
  • 6
    • 0038230678 scopus 로고
    • Nematic ordering of 4-n-alkyl-4′-cyanobiphenyls studied by carbon-13 NMR with offmagic-angle spinning
    • B. M. Fung, J. Afzal, T. L. Foss, and M. Chau, Nematic ordering of 4-n-alkyl-4′-cyanobiphenyls studied by carbon-13 NMR with offmagic-angle spinning, J. Chem. Phys. 85, 4808-4814 (1986).
    • (1986) J. Chem. Phys. , vol.85 , pp. 4808-4814
    • Fung, B.M.1    Afzal, J.2    Foss, T.L.3    Chau, M.4
  • 8
    • 0031189051 scopus 로고    scopus 로고
    • Site-resolved determination of peptide torsion angle phi from the relative orientations of backbone N-H and C-H bonds by solid-state NMR
    • M. Hong, J. D. Gross, and R. G. Griffin, Site-resolved determination of peptide torsion angle phi from the relative orientations of backbone N-H and C-H bonds by solid-state NMR, J. Phys. Chem. B 101, 5869-5874 (1997).
    • (1997) J. Phys. Chem. B , vol.101 , pp. 5869-5874
    • Hong, M.1    Gross, J.D.2    Griffin, R.G.3
  • 10
    • 36749113829 scopus 로고
    • Spinning-sideband-free and spinning-sideband-only NMR spectra in spinning samples
    • W. T. Dixon, Spinning-sideband-free and spinning-sideband-only NMR spectra in spinning samples, J. Chem. Phys. 77, 1800-1809 (1982).
    • (1982) J. Chem. Phys. , vol.77 , pp. 1800-1809
    • Dixon, W.T.1
  • 11
    • 0001024713 scopus 로고
    • Magic angle spinning sideband elimination by temporary interruption of the chemical shift
    • J. Hong and G. S. Harbison, Magic angle spinning sideband elimination by temporary interruption of the chemical shift, J. Magn. Reson. 105, 128-136 (1993).
    • (1993) J. Magn. Reson. , vol.105 , pp. 128-136
    • Hong, J.1    Harbison, G.S.2
  • 12
    • 0027639014 scopus 로고
    • Sideband suppression in magic-angle spinning NMR by a sequence of 5 pi pulses
    • Z. Song, O. N. Antzutkin, X. Feng, and M. H. Levitt, Sideband suppression in magic-angle spinning NMR by a sequence of 5 pi pulses, Solid State NMR 2, 143-146 (1993).
    • (1993) Solid State NMR , vol.2 , pp. 143-146
    • Song, Z.1    Antzutkin, O.N.2    Feng, X.3    Levitt, M.H.4
  • 13
    • 85011817347 scopus 로고
    • Detection of weak heteronuclear dipolar coupling by rotational-echo double-resonance nuclear magnetic resonance
    • W. S. Warren, Ed., Academic Press, San Diego
    • T. Gullion and J. Schaefer, Detection of weak heteronuclear dipolar coupling by rotational-echo double-resonance nuclear magnetic resonance, in "Advances in Magnetic Resonance" (W. S. Warren, Ed.), pp. 57-83, Academic Press, San Diego (1989).
    • (1989) Advances in Magnetic Resonance , pp. 57-83
    • Gullion, T.1    Schaefer, J.2
  • 15
    • 36749120883 scopus 로고
    • Two-dimensional NMR in rotating solids: Time reversal effects in chemical shift-dipolar spectra
    • M. G. Munowitz and R. G. Griffin, Two-dimensional NMR in rotating solids: Time reversal effects in chemical shift-dipolar spectra, J. Chem. Phys. 78, 613-617 (1983).
    • (1983) J. Chem. Phys. , vol.78 , pp. 613-617
    • Munowitz, M.G.1    Griffin, R.G.2
  • 17
  • 18
    • 0000539530 scopus 로고
    • NMR in rotating solids
    • M. M. Maricq and J. S. Waugh, NMR in rotating solids, J. Chem. Phys. 70, 3300-3316 (1979).
    • (1979) J. Chem. Phys. , vol.70 , pp. 3300-3316
    • Maricq, M.M.1    Waugh, J.S.2
  • 19
    • 0000116734 scopus 로고
    • Two-dimensional spin-echo nuclear magnetic resonance in rotating solids
    • A. C. Kolbert, D. P. Raleigh, M. H. Levitt, and R. G. Griffin, Two-dimensional spin-echo nuclear magnetic resonance in rotating solids, J. Chem. Phys. 90, 679-689 (1989).
    • (1989) J. Chem. Phys. , vol.90 , pp. 679-689
    • Kolbert, A.C.1    Raleigh, D.P.2    Levitt, M.H.3    Griffin, R.G.4
  • 21
    • 0009927484 scopus 로고
    • Two-dimensional spin-echo dipolarsideband enhancement in magic-angle-spinning NMR
    • A. C. Kolbert and R. G. Griffin, Two-dimensional spin-echo dipolarsideband enhancement in magic-angle-spinning NMR, J. Magn. Reson. 93, 242-255 (1991).
    • (1991) J. Magn. Reson. , vol.93 , pp. 242-255
    • Kolbert, A.C.1    Griffin, R.G.2
  • 22
    • 0029977896 scopus 로고    scopus 로고
    • Detection of intercatechol cross-links in insect cuticle by solid-state carbon-13 and nitrogen-15 NMR
    • M. E. Merritt, A. M. Christensen, K. J. Kramer, T. L. Hopkins, and J. Schaefer, Detection of intercatechol cross-links in insect cuticle by solid-state carbon-13 and nitrogen-15 NMR, J. Am. Chem. Soc. 118, 11278-11282 (1996).
    • (1996) J. Am. Chem. Soc. , vol.118 , pp. 11278-11282
    • Merritt, M.E.1    Christensen, A.M.2    Kramer, K.J.3    Hopkins, T.L.4    Schaefer, J.5
  • 24
    • 0002377859 scopus 로고
    • Frequency-switched pulse sequences: Homonuclear decoupling and dilute spin NMR in solids
    • A. Bielecki, A. C. Kolbert, and M. H. Levitt, Frequency-switched pulse sequences: Homonuclear decoupling and dilute spin NMR in solids, Chem. Phys. Lett. 155, 341-346 (1989).
    • (1989) Chem. Phys. Lett. , vol.155 , pp. 341-346
    • Bielecki, A.1    Kolbert, A.C.2    Levitt, M.H.3
  • 25
    • 36149023808 scopus 로고
    • Nuclear-magnetic-resonance line narrowing by a rotating rf field
    • M. Lee and W. I. Goldberg, Nuclear-magnetic-resonance line narrowing by a rotating rf field, Phys. Rev. A 140, 1261-1271 (1965).
    • (1965) Phys. Rev. A , vol.140 , pp. 1261-1271
    • Lee, M.1    Goldberg, W.I.2
  • 26
    • 0001427711 scopus 로고    scopus 로고
    • Measurement and assignment of long-range C-H dipolar couplings in liquid crystals by two-dimensional NMR spectroscopy
    • M. Hong, A. Pines, and S. Caldarelli, Measurement and assignment of long-range C-H dipolar couplings in liquid crystals by two-dimensional NMR spectroscopy, J. Phys. Chem. 100, 14815-14822 (1996).
    • (1996) J. Phys. Chem. , vol.100 , pp. 14815-14822
    • Hong, M.1    Pines, A.2    Caldarelli, S.3
  • 27
    • 45149145322 scopus 로고
    • Rotational echo double resonance NMR
    • T. Gullion and J. Schaefer, Rotational echo double resonance NMR, J. Magn. Reson. 81, 196-200 (1989).
    • (1989) J. Magn. Reson. , vol.81 , pp. 196-200
    • Gullion, T.1    Schaefer, J.2
  • 28
    • 0001115946 scopus 로고
    • Structures of two model peptides: N-acetyl-D,L-valine and N-acetyl-L-valyl-L-leucine
    • P. J. Carroll, P. L. Stewart, and S. J. Opella, Structures of two model peptides: N-acetyl-D,L-valine and N-acetyl-L-valyl-L-leucine, Acta Crystallogr. C 46, 243-246 (1990).
    • (1990) Acta Crystallogr. C , vol.46 , pp. 243-246
    • Carroll, P.J.1    Stewart, P.L.2    Opella, S.J.3
  • 30
    • 85030034649 scopus 로고    scopus 로고
    • note
    • Including sidebands further out, where all the simulated spectra show negligible intensity, would change neither the position nor the shape of the minimum in the rmsd curve. Thus the best-fit angle and its error margin would remain unchanged. It would only add an offset to the whole rmsd curve, due to the constant deviation between the experimental noise and the nearly vanishing intensity in the simulated spectra at these outer sidebands.
  • 31
    • 85030039308 scopus 로고    scopus 로고
    • U.S. Patent 4,446,431
    • R. A. McKay, U.S. Patent 4,446,431.
    • McKay, R.A.1
  • 33
    • 85030039200 scopus 로고    scopus 로고
    • private communication
    • R. A. McKay, private communication.
    • McKay, R.A.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.