Borane-induced dehydration of silica and the ensuing water-catalyzed grafting of B(C 6F 5) 3 to give a supported, single-site lewis acid, ≡siOB(C 6F 5) 2

Journal of the American Chemical Society

Volumn 134, Issue 1, 2012, Pages 355-366

  Wanglee, Ying Jen ^a   Hu, Jerry ^a   White, Rosemary E ^b   Lee, Ming Yung ^b   Stewart, S Michael ^b   Perrotin, Philippe ^b   Scott, Susannah L ^a,b  

^a UNIVERSITY OF CALIFORNIA   (United States)

^b University of California   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AMORPHOUS SILICA; COCATALYST; IN-SITU; LEWIS ACID; LEWIS ACID SITE; NICKEL COMPLEX; OLEFIN POLYMERIZATION; POLYMERIZATION CATALYSTS; ROOM TEMPERATURE; SILANOLS; SURFACE HYDROXYL GROUPS; TRACE AMOUNTS;

BORON COMPOUNDS; CATALYSIS; DEHYDRATION; DEWATERING; NICKEL COMPOUNDS; OLEFINS; POLYMERIZATION; SILICA;

GRAFTING (CHEMICAL);

ALKENE; ALPHA IMINOCARBOXAMIDATE; BORANE DERIVATIVE; BORON; BRONSTED BASE; ELEMENT; LEWIS ACID; NICKEL COMPLEX; SILANOL; SILICON DIOXIDE; UNCLASSIFIED DRUG; WATER;

ARTICLE; CATALYSIS; CATALYST; CHEMICAL STRUCTURE; COCATALYST; CONTROLLED STUDY; DESICCATION; FLUORINE NUCLEAR MAGNETIC RESONANCE; HYDROLYSIS; INFRARED RADIATION; POLYMERIZATION; PROTON NUCLEAR MAGNETIC RESONANCE; ROOM TEMPERATURE; SOLID STATE; SURFACE PROPERTY; WATER CATALYZED GRAFTING;

EID: 84862951315     PISSN: 00027863     EISSN: 15205126     Source Type: Journal    
DOI: 10.1021/ja207838j     Document Type: Article

References (70)

1. Chen, E. Y. X.; Marks, T. J. Chem. Rev. 2000, 100, 1391-1434
2. Yang, X. M.; Stern, C. L.; Marks, T. J. J. Am. Chem. Soc. 1991, 113, 3623-3625
3. Yang, X. M.; Stern, C. L.; Marks, T. J. J. Am. Chem. Soc. 1994, 116, 10015-10031
4. Boardman, B. M.; Bazan, G. C. Acc. Chem. Res. 2009, 42, 1597-1606
5. Clark, J. H. Acc. Chem. Res. 2002, 35, 791-797
6. Sreekanth, P.; Kim, S.-W.; Hyeon, T.; Kim, B. M. Adv. Synth. Catal. 2003, 345, 936-938
7. Hlatky, G. G. Chem. Rev. 2000, 100, 1347-1376
8. Fink, G.; Steinmetz, B.; Zechlin, J.; Przybyla, C.; Tesche, B. Chem. Rev. 2000, 100, 1377-1390
9. Iler, R. K. The Chemistry of Silica: Solubility, Polymerization, Colloid and Surface Properties and Biochemistry of Silica; Wiley: NewYork, 1979.
10. Zurek, E.; Ziegler, T. Prog. Polym. Sci. 2004, 29, 107-148
11. Walzer, J. F., Jr. U.S. Patent 5,643,847, 1997.
12. Holtcamp, M. W.; Lue, C.-T. U.S. Patent 6,476,166, 2002.
13. Holtcamp, M. W.; Cano, D. A. U.S. Patent 6,703,338, 2004.
14. Charoenchaidet, S.; Chavadej, S.; Gulari, E. J. Mol. Catal. A: Chem. 2002, 185, 167-177
15. Tian, J.; Wang, S.; Feng, Y.; Li, J.; Collins, S. J. Mol. Catal. A: Chem 1999, 144, 137-150
16. Millot, N.; Santini, C. C.; Lefebvre, F.; Basset, J.-M. C. R. Chim. 2004, 7, 725-736
17. McKinley, S. G.; Vecchi, P. A.; Ellern, A.; Angelici, R. J. Dalton Trans. 2004, 788-793
18. Wiench, J. W.; Michon, C.; Ellern, A.; Hazendonk, P.; Iuga, A.; Angelici, R. J.; Pruski, M. J. Am. Chem. Soc. 2009, 131, 11801-11810
19. Ward, D. G.; Carnahan, E. M. U.S. Patent 5,939,347, 1996.
20. Hikuma, S.; Kibino, N.; Hori, A.; Myake, S.; Inasawa, S. Japanese Patent 08 113604, 1996.
21. Kristen, M. O.; Lynch, J.; Lux, M.; Lange, A.; Karer, R. Proceedings of Metallocenes Europe, '97 Conference, Düsseldorf, 1997.
22. Carney, M. J.; Shih, K. Y. Proceedings of Metallocenes Europe, '98 Conference, Düsseldorf, 1998.
23. Walzer, J. F., Jr. Abstr. Papers Am. Chem. Soc. 1998, 215, U714 (051-Inor, Apr 2)
24. Bochmann, M.; Pindado, G. J.; Lancaster, S. J. J. Mol. Catal. A: Chem. 1999, 146, 179-190
25. Kristen, M. O. Top. Catal. 1999, 7, 89-95
26. Millot, N.; Cox, A.; Santini, C. C.; Molard, Y.; Basset, J. M. Chem.-Eur. J. 2002, 8, 1438-1442
27. Charoenchaidet, S.; Chavadej, S.; Gulari, E. J. Polym. Sci., Polym. Chem. 2002, 40, 3240-3248
28. Panchenko, V. N.; Danilova, I. G.; Zakharov, V. A.; Paukshtis, E. A. J. Mol. Catal. A: Chem. 2005, 225, 271-277
29. Millot, N.; Santini, C. C.; Baudouin, A.; Basset, J.-M. Chem. Commun. 2003, 2034-2035
30. Millot, N.; Soignier, S.; Santini, C. C.; Baudouin, A.; Basset, J.-M. J. Am. Chem. Soc. 2006, 128, 9361-9370
31. Duchateau, R.; van Santen, R. A.; Yap, G. P. A. Organometallics 2000, 19, 809-816
32. Metcalfe, R. A.; Kreller, D. I.; Tian, J.; Kim, H.; Taylor, N. J.; Corrigan, J. F.; Collins, S. Organometallics 2002, 21, 1719-1726
33. Lee, B. Y.; Bazan, G. C.; Vela, J.; Komon, Z. J. A.; Bu, X. H. J. Am. Chem. Soc. 2001, 123, 5352-5353
34. Rojas, R. S.; Wasilke, J.-C.; Wu, G.; Ziller, J. W.; Bazan, G. C. Organometallics 2005, 24, 5644-5653
35. Ittel, S. D.; Johnson, L. K.; Brookhart, M. Chem. Rev. 2000, 100, 1169-1203
36. Nakamura, A.; Ito, S.; Nozaki, K. Chem. Rev. 2009, 109, 5215-5244
37. Timoshkin, A. Y.; Frenking, G. Organometallics 2008, 27, 371-380
38. Liu, C. H. C.; Maciel, G. E. J. Am. Chem. Soc. 1996, 118, 5103-5119
39. Beringhelli, T.; D'Alfonso, G.; Donghi, D.; Maggioni, D.; Mercandelli, P.; Sironi, A. Organometallics 2004, 23, 5493-5502
40. Bruce, M. I. J. Chem. Soc. A 1968, 1459-1464
41. Doremus, R. H. J. Mater. Res. 1995, 10, 2379-2389
42. Van Ginhoven, R. M.; Jonsson, H.; Park, B.; Corrales, L. R. J. Phys. Chem. B 2005, 109, 10936-10945
43. Taha, Z. A.; Deguns, E. W.; Chattopadhyay, S.; Scott, S. L. Organometallics 2006, 25, 1891-1899
44. Bunker, B. C.; Haaland, D. M.; Michalske, T. A.; Smith, W. L. Surf. Sci. 1989, 222, 95-118
45. Rice, G. L.; Scott, S. L. Langmuir 1997, 13, 1545-1551
46. Morrow, B. A.; Devi, A. J. Chem. Soc., Faraday Trans. 1972, 68, 403-422
47. Possemiers, K.; VanDerVoort, P.; Vansant, E. F. J. Chem. Soc., Faraday Trans. 1996, 92, 679-684
48. Engelhardt, G.; Michel, D. High-Resolution Solid-State NMR of Silicates and Zeolites; Wiley: Chichester, UK, 1987.
49. Busca, G. Catal. Today 1998, 41, 191-206
50. Kohler, K.; Piers, W. E.; Jarvis, A. P.; Xin, S.; Feng, Y.; Bravakis, A. M.; Collins, S.; Clegg, W.; Yap, G. P. A.; Marder, T. B. Organometallics 1998, 17, 3557-3566
51. Beringhelli, T.; Donghi, D.; Maggioni, D.; D'Alfonso, G. Coord. Chem. Rev. 2008, 252, 2292-2313
52. Welch, G. C.; Holtrichter-Roessmann, T.; Stephan, D. W. Inorg. Chem. 2008, 47, 1904-1906
53. Brinker, C. J.; Kirkpatrick, R. J.; Tallant, D. R.; Bunker, B. C.; Montez, B. J. Non-Cryst. Solids 1988, 99, 418-428
54. Bergquist, C.; Bridgewater, B. M.; Harlan, C. J.; Norton, J. R.; Friesner, R. A.; Parkin, G. J. Am. Chem. Soc. 2000, 122, 10581-10590
55. Gouzyr, A. I.; Wessel, H.; Barnes, C. E.; Roesky, H. W.; Teichert, M.; Uson, I. Inorg. Chem. 1997, 36, 3392-3393
56. Guzyr, O. I.; Prust, J.; Roesky, H. W.; Lehmann, C.; Teichert, M.; Cimpoesu, F. Organometallics 2000, 19, 1549-1555
57. Winkhofer, N.; Roesky, H. W.; Noltemeyer, M.; Robinson, W. T. Angew. Chem., Int. Ed. 1992, 31, 599-601
58. Fleischman, S. D. F. S. D.; Scott, S. L. J. Am. Chem. Soc. 2011, 133, 4847-4855
59. Blackwell, J. M.; Piers, W. E.; Parvez, M. Org. Lett. 2000, 2, 695-698
60. Britovsek, G. J. P.; Ugolotti, J.; White, A. J. P. Organometallics 2005, 24, 1685-1691
61. Weiss, J. W. E.; Bryce, D. L. J. Phys. Chem. A 2010, 114, 5119-5131
62. Soraru, G. D.; Dallabona, N.; Gervais, C.; Babonneau, F. Chem. Mater. 1999, 11, 910-919
63. Scholle, K.; Veeman, W. S. Zeolites 1985, 5, 118-122
64. Hwang, S. J.; Fernandez, C.; Amoureux, J. P.; Cho, J.; Martin, S. W.; Pruski, M. Solid State Nucl. Magn. Reson. 1997, 8, 109-121
65. Bray, P. J. Inorg. Chim. Acta 1999, 289, 158-173
66. Bryce, D. L.; Wasylishen, R. E.; Gee, M. J. Phys. Chem. A 2001, 105, 3633-3640
67. Hwang, S. J.; Chen, C. Y.; Zones, S. I. J. Phys. Chem. B 2004, 108, 18535-18546
68. Scott, S. L.; Peoples, B. C.; Yung, C.; Rojas, R. S.; Khanna, V.; Sano, H.; Suzuki, T.; Shimizu, F. Chem. Commun. 2008, 4186-4188
69. Jelinek, L.; Kovats, E. S. Langmuir 1994, 10, 4225-4231
70. Frisch, M. J.; Gaussian 03, Revision C.02; Gaussian, Inc.: Wallingford, CT, 2004.