An ammonium sulfate/ethanol aqueous two-phase system combined with ultrasonication for the separation and purification of lithospermic acid B from Salvia miltiorrhiza Bunge

Ultrasonics Sonochemistry

Volumn 19, Issue 4, 2012, Pages 719-724

  Guo, Y X ^a   Han, J ^a   Zhang, D Y ^a   Wang, L H ^a   Zhou, L L ^a  

^a SHENYANG PHARMACEUTICAL UNIVERSITY   (China)

Author keywords

Aqueous two phase system; Lithospermic acid B; Purification; Response surface methodology; Ultrasonic assisted extraction

Indexed keywords

ETHANOL; LABORATORIES; NITROGEN COMPOUNDS; ORGANIC SOLVENTS; SOLVENT EXTRACTION; SULFUR COMPOUNDS; SURFACE PROPERTIES; ULTRASONICS;

AQUEOUS TWO PHASE SYSTEM; EXTRACTION AND PURIFICATIONS; LITHOSPERMIC ACID; RESPONSE SURFACE METHODOLOGY; SALVIA MILTIORRHIZA BUNGE; SEPARATION AND PURIFICATION; ULTRASONIC-ASSISTED EXTRACTIONS; ULTRASONICATION EXTRACTION;

PURIFICATION;

ALCOHOL; AMMONIUM SULFATE; LITHOSPERMIC ACID; LITHOSPERMIC ACID B; SALVIA MILTIORRHIZA EXTRACT; UNCLASSIFIED DRUG;

ANALYTIC METHOD; AQUEOUS SOLUTION; AQUEOUS TWO PHASE SYSTEM; ARTICLE; CONTROLLED STUDY; DRUG PURIFICATION; DRUG PURITY; MEDICINAL PLANT; NONHUMAN; PARTITION COEFFICIENT; PH; PRIORITY JOURNAL; RESPONSE SURFACE METHOD; SEPARATION TECHNIQUE; TIME; ULTRASOUND;

EID: 84862805713     PISSN: 13504177     EISSN: 18732828     Source Type: Journal    
DOI: 10.1016/j.ultsonch.2011.12.017     Document Type: Article

References (24)

1. National Pharmacopoeia Committee, Pharmacopoeia of the People's Republic of China, Chemical Industry Press, Beijing, 2010.
2. G.R. Zhao, H.M. Zhang, T.X. Ye, Z.J. Xiang, Y.J. Yuan, Z.X. Guo, and L.B. Zhao Characterization of the radical scavenging and antioxidant activities of danshensu and salvianolic acid B Food Chem. Toxicol. 46 2008 73 81
3. X.J. Wu, Y.P. Wang, W. Wang, W.K. Sun, Y.M. Xu, and L.J. Xuan Free radical scavenging and inhibition of lipid peroxidation by magnesium lithospermate B Acta Pharmacol. Sin. 21 2000 855 858
4. T. Yokozawa, T.W. Lee, H. Oura, G. Nonaka, and I. Nishioka Effect of magnesium lithospermate B in rats with sodium-induced hypertension and renal failure Nephron 60 1992 460 465
5. K. Hase, R. Kasimu, P. Basnet, S. Kadota, and T. Namba Preventive effect of lithospermate B from Salvia miltiorrhiza on experimental hepatitis induced by carbon tetrachloride or d-galactosamine/lipopolysaccharide Planta Med. 63 1997 22 26 (Pubitemid 27112432)
6. D.G. Kang, H. Oh, E.J. Sohn, T.Y. Hur, K.C. Lee, K.J. Kim, T.Y. Kim, and H.S. Lee Lithospermic acid B isolated from Salvia miltiorrhiza ameliorates ischemia/reperfusion-induced renal injury in rats Life Sci. 75 2004 1801 1816 (Pubitemid 39070494)
7. B.X. Xu, Q. Liang, Y.B. Shi, and H.J. Wang Determination of tanshinone II A in natural food preservative by HPLC method Sci. Technol. Food Ind. 28 2007 210 211
8. A.T. Robert, C.K. Martin, Z. Liu, R.J. Amen, E.A. Woltering, J.C. Rood, M.K. Caruso, Y. Yu, H. Xie, and F.L. Greenway The safety and efficacy of a dietary herbal supplement and gallic acid for weight loss J. Med. Food 10 2007 184 188 (Pubitemid 46706867)
9. Y.X. Guo, Z.L. Xiu, D.J. Zhang, H. Wang, L.X. Wang, and H.B. Xiao Kinetics and mechanism of degradation of lithospermic acid B in aqueous solution J. Pharm. Biomed. Anal. 43 2007 1249 1255 (Pubitemid 46282367)
10. D.Z. Wu, S.Q. Liu, P.J. Wu, Q.M. Jiang, and N. Zhu Purifying process of water extract solution of danshen (in Chinese) Chinese Tradi. Herb. Drugs 40 2009 889 892
11. J. Xu, T.W. Tan, and J.C. Janson One-step simultaneous purification of three water-soluble constituents in crude extracts from Danshen by adsorption chromatography on oligo-β-cyclodextrin substituted agarose gel media Process Biochem. 42 2007 480 485 (Pubitemid 46329540)
12. S.D. Kana, J.A. Li, W.Y. Huang, L. Shao, and D.J. Chen Microsphere resin chromatography combined with microbial biotransformation for the separation and purification of salvianolic acid B in aqueous extract of roots of Salvia miltiorrihza Bunge J. Chromatogr. A 1216 2009 3881 3886
13. M. Gu, X.L. Wang, Z.G. Su, and F. Ouyang One-step separation purification of 3,4-dihydroxyphenyllactic acid salvianolic acid B and protocatechualdehyde from Salvia miltiorrhiza Bunge by high-speed counter-current chromatography J. Chromatogr. A 1140 2007 107 111 (Pubitemid 46026779)
14. M. Zhang, S. Ignatova, Q.L. Liang, F.W. Jun, I. Sutherland, Y.M. Wang, and G.A. Luo Rapid and high-throughput purification of salvianolic acid B from Salvia miltiorrhiza Bunge by high-performance counter-current chromatography J. Chromatogr. A 1216 2009 3869 3873
15. X.N. Yang, X. Tang, and Y.S. Liu Separation and purification of salvianolic acids from Salvia miltiorrhiza (in Chinese) Chinese Tradi. Herb. Drugs 38 2007 843 846 (Pubitemid 47162506)
16. X. Yu, B.Q. Mo, Z. Wang, and H.B. Qu Recovery prediction of danshensu salvianolic acid B and salvianolic acid D in danshen ethanol precipitation (in Chinese) Chinese Tradi. Herb. Drugs 41 2010 900 903
17. S.F. Shen, Z.D. Chang, J. Liu, X.H. Sun, X. Hu, and H.Z. Liu Separation of glycyrrhizic acid and liquiritin from Glycyrrhiza uralensis Fisch extract by three-liquid-phase extraction systems Sep. Purif. Technol. 53 2007 216 223 (Pubitemid 46108656)
18. W.B. Zhi, and Q.Y. Deng Purification of salvianolic acid B from the crude extract of Salvia miltiorrhiza with hydrophilic organic/salt-containing aqueous two-phase system by counter-current chromatography J. Chromatogr. A 1116 2006 149 152
19. A. Greve, and M.R. Kula Cost structure and estimation for the recycling of salt in a protein extraction process system Bioproc. Biosyst. Eng. 6 1990 173 177
20. A.L. Ahmad, C.J.C. Derek, and M.M.D. Zulkali Optimization of thaumatin extraction by aqueous two-phase system (ATPS) using response surface methodology (RSM) Sep. Purif. Technol. 62 2008 702 708
21. L. Paniwnyk, E. Beaufoy, J.P. Lorimer, and T.J. Mason The extraction of rutin from flower buds of Sophora japonica Ultrson. Sonochem. 8 2001 299 301 (Pubitemid 32544981)
22. S. Zhao, and O.D. Baik Application of ultrasound as pretreatment for extraction of podophyllotoxin from rhizomes of Podophyllum peltatum Ultrason. Sonochem. 19 2012 22 31
23. S. Kim, E.J. Yun, J.S. Bak, H.J. Lee, S.J. Lee, C.T. Kim, J.H. Lee, and K.H. Kim On-line HPLC-ABTS screening and HPLC-DAD-MS/MS identification of free radical scavengers in Gardenia (Gardenia jasminoides Ellis) fruit extracts Food Chem. 121 2010 521 528
24. M. Rezaee, Y. Yamini, and M. Faraji Evolution of dispersive liquid-liquid microextraction method J. Chromatogr. A 1217 2010 2342 2357