One-step simultaneous purification of three water-soluble constituents in crude extracts from Danshen by adsorption chromatography on oligo-β-cyclodextrin substituted agarose gel media

Process Biochemistry

Volumn 42, Issue 3, 2007, Pages 480-485

  Xu, Jun ^a   Tan, Tianwei ^a   Janson, Jan Christer ^b  

^a BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY   (China)

^b UPPSALA UNIVERSITY   (Sweden)

Author keywords

Cyclodextrin; Agarose gel media; Danshensu; Lithospermic acid B; Protocatechuic aldehyde; Salviae miltiorrhizae; Salvianolic acid B

Indexed keywords

ADSORPTION; ALDEHYDES; CELL IMMOBILIZATION; CHROMATOGRAPHIC ANALYSIS; GELS; PURIFICATION;

AGAROSE GEL MEDIA; CRUDE EXTRACTS; CYCLODEXTRIN; DANSHENSU; DISTILLED WATER; PROTOCATECHUIC ALDEHYDE; SALVIAE MILTIORRHIZAE; SALVIANOLIC ACID;

POLYSACCHARIDES;

SALVIA MILTIORRHIZA;

EID: 33847274842     PISSN: 13595113     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.procbio.2006.09.015     Document Type: Article

References (22)

1. Zhou J.J., Xie G.R., and Yan X.J. In: Milne G.W.A. (Ed). Traditional Chinese medicines: molecular structures, natural sources and applications (2003), Ashgate Publishing Limited, England 858
2. Liu L., and Zhang H.Q. Advances in contemporary traditional Chinese medicine (TCM) pharmacology studies of active constituents of Danshen (Salvia miltiorrhiza). Chin Wild Plant Resour 22 (2003) 163-166
3. Kasimu R., Tanaka K., Tezuka Y., Gong Z.N., Li J.X., Basnet P., et al. Comparative study of seventeen Salvia plants: aldose reductase inhibitory activity of water and MeOH extracts and liquid chromatography-mass spectrometry (LC-MS) analysis of water extracts. Chem Pharm Bull (Tokyo) 46 (1998) 500-504
4. Gu S., Wang X.R., Li L., and Lee F. Analysis of active ingredients in Salvia miltiorrhiza Bge. by HPLC-ESI-MS. Anal Sci 17 (2001) 475-478
5. Shi Z., He J., Zhao M., and Chang W. Simultaneous determination of five marker constituents in traditional Chinese medicinal preparation Le-Mai granule by high performance liquid chromatography. J Pharm Biomed Anal 37 (2004) 469-473
6. Hu P., Luo G.A., Zhao Z., and Jiang Z.H. Quality assessment of Radix Salviae miltiorrhizae. Chem Pharm Bull (Tokyo) 53 (2005) 481-486
7. Zhang J.L., Cui M., He Y., Yu H.L., and Guo D.A. Chemical fingerprint and metabolic fingerprint analysis of Danshen injection by HPLC-UV and HPLC-MS methods. J Pharm Biomed Anal 36 (2005) 1029-1035
8. Liu A.H., Li L., Xu M., Lin Y.H., Guo H.Z., and Guo D.A. Simultaneous quantification of six major phenolic acids in the roots of Salvia miltiorrhiza and four related traditional Chinese medicinal preparations by HPLC-DAD method. J Pharm Biomed Anal (2005) [Published on-line ahead of print]
9. Li X., Yu C., Cai Y., Liu G., Jia J., and Wang Y. Simultaneous determination of six phenolic constituents of Danshen in human serum using liquid chromatography/tandem mass spectrometry. J Chromatogr B 820 (2005) 41-47
10. Xiao XL, Gan HT, Liao YM, Feng XT. Supercritical carbon dioxide extraction for active compounds in Salviae radix. Chinese Patent CN1256142A; 2000.
11. Cai JG, Deng X, Tu YB. A method of extraction of Danshensu from Salviae radix. Chinese Patent CN1342638A; 2002.
12. Ye Y, Wang D, Li XD, Dai JP. A method of extraction of salvianolic acids and preparation of its frozen-dry injection solution. Chinese Patent CN1513848A; 2004.
13. Li H.B., Lai J.P., Jiang Y., and Chen F. Preparative isolation and purification of Salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by high-speed counter-current chromatography. J Chromatogr A 943 (2002) 235-239
14. Ai C.B., and Li L.N. Stereostructure of salvianolic acid and isolation of salvianolic acid from Salvia miltiorrhiza. J Nat Prod 51 (1988) 145-149
15. Wu Z.J., Ouyang M.A., and Yang C.R. Polyphenolic constituents of Salvia sconchifolia. Acta Bot Yunnan 21 (1999) 393-398
16. Zhu H., Hou X., Sun Y., and Mao S. Application and characteristics of macroreticular resin in purification study of different effective ingredients in Chinese medicines. Zhongguo Zhong Yao Za Zhi 23 (1998) 607-609
17. Fang X.S., and Tan X.M. The qualitative analysis and quantitative analysis of purification of salvianolic acids by macroreticular resin. Zhongguo Zhong Yao Za Zhi 30 (2005) 1331-1334
18. Wang Z.P., Fan J.Y., Liu Y.Q., and Yuan Y.J. Study on adsorption of Danshen water-soluble compounds with macroporous resin D301. Zhong Guo Zhong Yao Za Zhi 29 (2004) 854-857
19. He X.L., Tan T.W., Xu B.Z., and Janson J.C. Separation and purification of puerarin using β-cyclodextrin-coupled agarose gel media. J Chromatogr A 1022 (2004) 77-82
20. Xu J., Zhang G.F., Tan T.W., and Janson J.C. One-step purification of epigallocatechin gallate from crude green tea extracts by isocratic hydrogen bond adsorption chromatography on β-cyclodextrin substituted agarose gel media. J Chromatogr B 824 (2005) 323-326
21. Pan Y.N., Yuan D., Fu W.W., Wang A.P., and Kano Y. Simultaneous determination of 4 water-soluble components in Danshen containing injections by HPLC. J Shenyang Pharm Univ 21 (2004) 196-200
22. Ross P.D., and Rekharsky M.V. Thermodynamics of hydrogen bond and hydrophobic interactions in cyclodextrin complexes. Biophys J 71 (1996) 2144-2154