Dispersive liquid-liquid microextraction for the determination of organochlorine pesticides residues in honey by gas chromatography-electron capture and ion trap mass spectrometric detection

Food Chemistry

Volumn 134, Issue 3, 2012, Pages 1665-1672

  Zacharis, Constantinos K ^a,b   Rotsias, Ilias ^a   Zachariadis, Petros G ^a   Zotos, Anastasios ^a  

^a ALEXANDER TECHNOLOGICAL EDUCATIONAL INSTITUTE OF THESSALONIKI   (Greece)

^b ARISTOTLE UNIVERSITY OF THESSALONIKI   (Greece)

Author keywords

Dispersive liquid liquid microextraction; Electron capture; Gas chromatography mass spectrometry; Honey; Organochlorine pesticides

Indexed keywords

DISPERSIVE LIQUID-LIQUID MICROEXTRACTION; ELECTRON CAPTURE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HONEY; ORGANOCHLORINE PESTICIDES;

ACETONITRILE; CENTRIFUGATION; CHLORINE COMPOUNDS; FOOD PRODUCTS; GAS CHROMATOGRAPHY; IONIC STRENGTH; LIQUIDS; MASS SPECTROMETRY; ORGANIC SOLVENTS; PESTICIDES; REDUCTION; SOLVENTS;

SOLVENT EXTRACTION;

ACETONITRILE; CHLOROFORM; ORGANIC SOLVENT; ORGANOCHLORINE PESTICIDE; PESTICIDE RESIDUE; CHLORINATED HYDROCARBON; SOLVENT;

ACCURACY; ANALYTIC METHOD; AQUEOUS SOLUTION; ARTICLE; CENTRIFUGATION; ELECTRON CAPTURE DETECTION; EVAPORATION; GAS CHROMATOGRAPHY; GREECE; HONEY; INTERMETHOD COMPARISON; ION TRAP MASS SPECTROMETRY; IONIC STRENGTH; LIQUID LIQUID EXTRACTION; PH; ANALYSIS; CHEMISTRY; ELECTRON; LIMIT OF DETECTION; LIQUID PHASE MICROEXTRACTION; MASS FRAGMENTOGRAPHY; REPRODUCIBILITY;

ELECTRONS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HONEY; HYDROCARBONS, CHLORINATED; HYDROGEN-ION CONCENTRATION; LIMIT OF DETECTION; LIQUID PHASE MICROEXTRACTION; PESTICIDE RESIDUES; REPRODUCIBILITY OF RESULTS; SOLVENTS;

EID: 84861097848     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2012.03.073     Document Type: Article

References (30)

1. B. Albero, C. Sanchez-Brunete, and J.L. Tadeo Analysis of pesticides in honey by solid-phase extraction and gas chromatography-mass spectrometry Journal of Agricultural and Food Chemistry 52 2004 5828 5835
2. A.A. Barakat, H.M.A. Badawy, E. Salama, E. Attallah, and G. Maatook Simple and rapid method of analysis for determination of pesticide residues in honey using dispersive solid phase extraction and GC determination Journal of Food, Agriculture and Environment 5 2007 97 100
3. C. Blasco, M. Fernandez, A. Pena, C. Lino, M. Silveira, G. Font, and Y. Pico Assessment of Pesticide Residues in Honey Samples from Portugal and Spain Journal of Agriculture and Food Chemistry 51 2003 8132 8138
4. C. Blasco, C.M. Lino, Y. Pico, A. Pena, G. Font, and M.I.N. Silveira Determination of organochlorine pesticide residues in honey from the central zone of Portugal and the Valencian community of Spain Journal of Chromatography A 1049 2004 155 160
5. N. Campillo, R. Penalver, N. Aguinaga, and M. Hernandez-Cordoba Solid-phase microextraction and gas chromatography with atomic emission detection for multiresidue determination of pesticides in honey Analytica Chimica Acta 562 2006 9 15
6. H. Chen, H. Chen, L. Liao, J. Ying, and J. Huang Determination of thiamphenicol in honey by dispersive liquid-liquid microextraction with high-performance liquid chromatography Journal of Chromatographic Science 48 2010 450 455
7. H. Chen, H. Chen, J. Ying, J. Huang, and L. Liao Dispersive liquid-liquid microextraction followed by high-performance liquid chromatography as an efficient and sensitive technique for simultaneous determination of chloramphenicol and thiamphenicol in honey Analytica Chimica Acta 632 2009 80 85
8. H. Chen, J. Ying, H. Chen, J. Huang, and L. Liao LC determination of chloramphenicol in honey using dispersive liquid-liquid microextraction Chromatographia 68 2008 629 634
9. L.F. Cuevas-Glory, J.A. Pino, L.S. Santiago, and E. Sauri-Duch A review of volatile analytical methods for determining the botanical origin of honey Food Chemistry 103 2007 1032 1043
10. S.C. Cunha, J.O. Fernandes, and M.B.P.P. Oliveira Comparison of matrix solid-phase dispersion and liquid-liquid extraction for the chromatographic determination of fenthion and its metabolites in olives and olive oils Food Additives and Contaminants 24 2007 156 164
11. G.P. de Pinho, A.A. Neves, M.E.L.R. de Queiroz, and F.O. Silverio Optimization of the liquid-liquid extraction method and low temperature purification (LLE-LTP) for pesticide residue analysis in honey samples by gas chromatography Food Control 21 2010 1307 1311
12. M. Fernandez, Y. Pico, and J. Manes Analytical methods for pesticide residue determination in bee products Journal of Food Protection 65 2002 1502 1511
13. M. Fontcuberta, J.F. Arques, J.R. Villalbi, M. Martinez, F. Centrich, E. Serrahima, L. Pineda, J. Duran, and C. Casas Chlorinated organic pesticides in marketed food: Barcelona, 2001-06 Science of the Total Environment 389 2008 52 57
14. A. Herrera, C. Perez-Arquillue, P. Conchello, S. Bayarri, R. Lazaro, C. Yague, and A. Arino Determination of pesticides and PCBs in honey by solid-phase extraction cleanup followed by gas chromatography with electron-capture and nitrogen-phosphorus detection Analytical and Bioanalytical Chemistry 381 2005 695 701
15. M. LeDoux Analytical methods applied to the determination of pesticide residues in foods of animal origin. A review of the past two decades Journal of Chromatography A 1218 2011 1021 1036
16. M.-I. Leong, and S.-D. Huang Dispersive liquid-liquid microextraction method based on solidification of floating organic drop for extraction of organochlorine pesticides in water samples Journal of Chromatography A 1216 2009 7645 7650
17. R. Montes, I. Rodriguez, E. Rubi, and R. Cela Dispersive liquid-liquid microextraction applied to the simultaneous derivatization and concentration of triclosan and methyltriclosan in water samples Journal of Chromatography A 1216 2009 205 210
18. Regulation (EC) No 396/2005, European Union pesticides database, (Assessed 2011) < http://ec.europa.eu/sanco-pesticides/public/index.cfm >.
19. M. Rezaee, Y. Assadi, M.-R.M. Hosseini, E. Aghaee, F. Ahmadi, and S. Berijani Determination of organic compounds in water using dispersive liquid-liquid microextraction Journal of Chromatography A 1116 2006 1 9
20. M. Rezaee, Y. Yamini, and M. Faraji Evolution of dispersive liquid-liquid microextraction method Journal of Chromatography A 1217 2010 2342 2357
21. R. Rial-Otero, E.M. Gaspar, I. Moura, and J.L. Capelo Chromatographic-based methods for pesticide determination in honey: An overview Talanta 71 2007 503 514
22. S.R. Rissato, M.S. Galhiane, M.V. de Almeida, M. Gerenutti, and B.M. Apon Multiresidue determination of pesticides in honey samples by gas chromatography-mass spectrometry and application in environmental contamination Food Chemistry 101 2007 1719 1726
23. S.R. Rissato, M.S. Galhiane, F.R.N. Knoll, and B.M. Apon Supercritical fluid extraction for pesticide multiresidue analysis in honey: Determination by gas chromatography with electron-capture and mass spectrometry detection Journal of Chromatography A 1048 2004 153 159
24. SANCO/10684/2009 (2011), Method Validation and Quality Control Procedures for Pesticide Residues Analysis in Food and Feed, (Assessed 2011) < http://ec.europa.eu/food/plant/protection/resources/qualcontrol-en.pdf >.
25. A. Sarafraz-Yazdi, and A. Amiri Liquid-phase microextraction TrAC - Trends in Analytical Chemistry 29 2010 1 14
26. Stockholm Convention on Persistent Organic Pollutants, (Assessed 2011), URL: < http://chm.pops.int >.
27. Y.R. Tahboub, M.F. Zaater, and T.A. Barri Simultaneous identification and quantitation of selected organochlorine pesticide residues in honey by full-scan gas chromatography-mass spectrometry Analytica Chimica Acta 558 2006 62 68
28. D. Tsipi, M. Triantafyllou, and A. Hiskia Determination of organochlorine pesticide residues in honey, applying solid phase extraction with RP-C18 material Analyst 124 1999 473 475
29. Y. Wang, J. You, R. Ren, Y. Xiao, S. Gao, H. Zhang, and A. Yu Determination of triazines in honey by dispersive liquid-liquid microextraction high-performance liquid chromatography Journal of Chromatography A 1217 2010 4241 4246
30. C.K. Zacharis, P.D. Tzanavaras, K. Roubos, and K. Dhima Solvent-based de-emulsification dispersive liquid-liquid microextraction combined with gas chromatography-mass spectrometry for determination of trace organochlorine pesticides in environmental water samples Journal of Chromatography A 1217 2010 5896 5900