Origin and correction of magnetic field inhomogeneity at the interface in biphasic NMR samples

Journal of Magnetic Resonance

Volumn 218, Issue , 2012, Pages 147-152

  Martin, Bryan T ^a   Chingas, G C ^a   McDougal, Owen M ^a  

^a BOISE STATE UNIVERSITY   (United States)

Author keywords

Biphasic; Bulk magnetism; Chemical shift; Demagnetization field; Magic angle spinning; MAS; NMR; Octanol; Shimming; Susceptibility

Indexed keywords

BIPHASIC; DEMAGNETIZATION FIELDS; MAS; OCTANOL; SHIMMING;

ALCOHOLS; CHEMICAL SHIFT; MAGIC ANGLE SPINNING; MAGNETIC SUSCEPTIBILITY; NUCLEAR MAGNETIC RESONANCE; PARAMAGNETISM; TUBES (COMPONENTS);

MAGNETIC FIELDS;

DEUTERIUM OXIDE; GADOLINIUM; GADOLINIUM CHLORIDE; OCTANOL; WATER;

ALGORITHM; ARTICLE; CHEMISTRY; ELECTROMAGNETIC FIELD; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; STATISTICAL ANALYSIS;

ALGORITHMS; DATA INTERPRETATION, STATISTICAL; DEUTERIUM OXIDE; ELECTROMAGNETIC FIELDS; GADOLINIUM; MAGNETIC RESONANCE SPECTROSCOPY; OCTANOLS; WATER;

EID: 84861096892     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2012.02.012     Document Type: Article

References (42)

1. S.E. Snyder, and W.H. Pirkle Enantioselective hydrolysis of N-acylated α-amino esters at a biphasic interface: tandem reaction kinetic resolution using a chiral complexing agent Org. Lett. 4 2002 3283 3286
2. X. Wu, C. Chen, N. Liu, and Y. Chen Preparation of ethyl 3R,5S-6-(benzyloxy)-3,5-dihydroxy-hexanoate by recombinant diketoreductase in a biphasic system Bioresource Technol. 102 2011 3649 3652
3. P.C. Stein, M. di Cagno, and A. Bauer-Brandl A novel method for the investigation of liquid/liquid distribution coefficients and interface permeabilities applied to the water-octanol-drug system Pharmaceut. Res. 28 2011 2140 2146
4. Q. Liu, W. Wei, M. Lu, F. Sun, J. Li, and Y. Zhang Chloromethylation of aromatic compounds catalyzed by surfactant micelles in oil-water biphasic system Catal. Lett. 131 2009 485 493
5. T.J. Davies, A.C. Garner, S.G. Davies, and R.G. Compton Insights into the role of the liquid-liquid interface in biphasic reactions: the reaction of vitamin b12s(aq) with vicinal dibromides(oil) ChemPhysChem 6 2005 2633 2639
6. W. Guba, R. Haessner, G. Breipohl, S. Henke, J. Knolle, V. Santagada, and H. Kessler Combined approach of NMR and molecular dynamics within a biphasic membrane mimetic: conformation and orientation of the bradykinin antagonist Hoe 140 J. Am. Chem. Soc. 116 1994 7532 7540
7. M. Manna, and C. Mukhopadhyay Cholesterol driven alteration of the conformation and dynamics of phospholamban in model membranes Phys. Chem. Chem. Phys. 13 2011 20188 20198
8. D. Filip, V.I. Uricanu, M.H.G. Duits, W.G.M. Agterof, and J. Mellema Influence of bulk elasticity and interfacial tension on the deformation of gelled water-in-oil emulsion droplets: an AFM study Langmuir 21 2005 115 126
9. K. Adachi, K. Chayama, and H. Watarai Control of optically active structure of thioether-phthalocyanine aggregates by chiral Pd(II)-BINAP complexes in toluene and at the toluene/water interface Chirality 18 2006 599 608
10. L. Tong, and J.-X. Cheng Label-free imaging through nonlinear optical signals Mater. Today 14 2011 264 273
11. G. Wittstock, M. Burchardt, S. Pust, Y. Shen, and C. Zhao Scanning electrochemical microscopy for direct imaging of reaction rates Angew. Chem. Int. Ed. 46 2007 1584 1617
12. Š. Málková, F. Long, R.V. Stahelin, S.V. Pingali, D. Murray, W. Cho, and M.L. Schlossman X-ray reflectivity studies of cPLA2 α-C2 domains adsorbed onto langmuir monolayers of SOPC Biophys. J. 89 2005 1861 1873
13. A. Zarbakhsh, A. Querol, J. Bowers, M. Yaseen, J.R. Lu, and J.R.P. Webster Neutron reflection from the liquid-liquid interface: adsorption of hexadecylphosphorylcholine to the hexadecane-aqueous solution interface Langmuir 21 2005 11704 11709
14. W. Koźmiński Application of spatially resolved NMR spectroscopy for high resolution spectra of heterogeneous samples Polym. J. Chem. 74 2000 1185 1189
15. J. Lambert, R. Hergenröder, D. Suter, and V. Deckert Probing liquid-liquid interfaces with spatially resolved NMR spectroscopy Angew. Chem. Int. Ed. 48 2009 6343 6345
16. C. Mantel, P.-A. Bayle, S. Hediger, C. Berthon, and M. Bardet Study of liquid-liquid interfaces by an easily implemented localized NMR sequence Magn. Reson. Chem. 48 2010 600 606
17. A. Zdziennicka, and B. Jańczuk Behavior of cationic surfactants and short chain alcohols in mixed surface layers at water-air and polymer-water interfaces with regard to polymer wettability. I. Adsorption at water-air interface J. Colloid. Interf. Sci. 349 2010 374 383
18. H. Carr, and E. Purcell Effects of diffusion on free precession in nuclear magnetic resonance experiments Phys. Rev. 94 1954 630 638
19. R.R. Ernst, and W.A. Anderson Application of Fourier transform spectroscopy to magnetic resonance Rev. Sci. Instrum. 37 1966 93 102
20. W.T. Raynes Nuclear shielding R.K. Harris, Nuclear Magnetic Resonance 1971 Royal Society of Chemistry Cambridge 1 50
21. R. Hoffman Variations on the chemical shift of TMS J. Magn. Reson 163 2003 325 331
22. J.C. Slater, and N.H. Frank Electromagnetism 1 edition 1947 McGraw-Hill Book Co. New York, NY
23. G. Mozurkewich, H.I. Ringermacher, and D.I. Bolef Effect of demagnetization on magnetic resonance line shapes in bulk samples: application to tungsten Phys. Rev. B 20 1979 33 38
24. T.M. Barbara Cylindrical demagnetization fields and microprobe design in high-resolution NMR J. Magn. Reson. Ser. A 109 1994 265 269
25. C.J. Durrant, M. Hertzburg, and P.W. Kuchel Magnetic susceptibility: further insights into macroscopic and microscopic fields and the sphere of lorentz Concept. Magn. Reson. 18 2003 72 95
26. N. Bloembergen, and W.C. Dickinson On the shift of the nuclear magnetic resonance in paramagnetic solutions Phys. Rev. 79 1950 179 180
27. D.R. Lide CRC Handbook Chemistry and Physics 85th edition 2004 CRC Press Boca Raton, FL
28. R.E. Hoffman Standardization of chemical shifts of TMS and solvent signals in NMR solvents Magn. Reson. Chem. 44 2006 606 616
29. J.W. Emsley, J. Feeney, and L.H. Sutcliffe High Resolution Nuclear Magnetic Resonance Spectroscopy 1965 Pergamon
30. F.D. Doty, G. Entzminger, and Y.A. Yang Magnetism in high-resolution NMR probe design. II: HR MAS Concept. Magn. Reson. 10 1998 239 260
31. F.D. Doty, G. Entzminger, and Y.A. Yang Magnetism in high-resolution NMR probe design. I: General methods Concept. Magn. Reson. 10 1998 133 156
32. R.E. Hoffman, H. Arzuan, C. Pemberton, A. Aserin, and N. Garti High-resolution nmr "chromatography" using a liquids spectrometer J. Magn. Reson. 194 2008 295 299
33. A. Leo, C. Hansch, and D. Elkins Partition coefficients and their uses Chem. Rev. 71 1971 525 616
34. E.V. Ivanov Volumetric properties of dilute solutions of water in ethanol and water-d2 in ethanol-d1 between t = (278.15 and 318.15)k J. Chem. Thermodyn. 47 2012 162 170
35. F. Palombo, T. Tassaing, M. Paolantoni, P. Sassi, and A. Morresi Elucidating the association of water in wet 1-octanol from normal to high temperature by near- and mid-infrared spectroscopy J. Phys. Chem. B 114 2010 9083 9085
36. E.R. Andrew, A. Bradbury, and R.G. Eades Removal of dipolar broadening of nuclear magnetic resonance spectra of solids by specimen rotation Nature 183 1959 1802 1803
37. P. Granger, M. Bourdonneau, O. Assémat, and M. Piotto NMR chemical shift measurements revisited: high precision measurements Concept. Magn. Reson. 30A 2007 184 193
38. D. Doskočilová, and B. Schneider Narrowing of proton NMR lines by magic angle rotation Chem. Phys. Lett. 6 1970 381 384
39. A.N. Garroway Magic-angle sample spinning of liquids J. Magn. Reson. 49 1982 168 171
40. C.R. Morcombe, and K.W. Zilm Chemical shift referencing in MAS solid state NMR J. Magn. Reson. 162 2003 479 486
41. W.A. Edelstein, J.M.S. Hutchison, G. Johnson, and T. Redpath Spin warp NMR imaging and applications to human whole-body imaging Phys. Med. Biol. 25 1980 751 756
42. U. Klose Measurement sequences for single voxel proton MR spectroscopy Eur. J. Radiol. 67 2008 194 201