Chemical shift referencing in MAS solid state NMR

Journal of Magnetic Resonance

Volumn 162, Issue 2, 2003, Pages 479-486

  Morcombe, Corey R ^a   Zilm, Kurt W ^a  

^a YALE UNIVERSITY   (United States)

Author keywords

13C NMR; Adamantane; Chemical shift referencing; Demagnetizing field; DSS shift scale; Magic angle spinning; Magnetic susceptibility; Solvent shifts; TMS shift scale

Indexed keywords

DEMAGNETIZATION; MAGNETIC SUSCEPTIBILITY; METHANOL; NUCLEIC ACID SEQUENCES; ORGANIC SOLVENTS; PROTEINS;

MAGIC ANGLE SPINNING (MAS);

NUCLEAR MAGNETIC RESONANCE;

EID: 0042995329     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1090-7807(03)00082-X     Document Type: Article

References (25)

1. Harris R.K., Becker E.D., De Menezes S.M.C., Goodfellow R., Granger P. NMR nomenclature. Nuclear spin properties and conventions for chemical shifts - (IUPAC recommendations 2001). Pure Appl. Chem. 73:2001;1795-1818.
2. Garroway A.N. Magic-angle sample spinning of liquids. J. Magn. Reson. 49:1982;168-171.
3. Dickinson W.C. The time average magnetic field at the nucleus in nuclear magnetic resonance experiments. Phys. Rev. 81:1951;717-731.
4. Doty F.D., Entzminger G., Yang Y.A. Magnetism in high-resolution NMR probe design. I: General methods. Concepts Magn. Resonance. 10:1998;133-156.
5. Earl W.L., VanderHart D.L. Measurement of C-13 chemical-shifts in solids. J. Magn. Reson. 48:1982;35-54.
6. Barbara T.M. Cylindrical demagnetization fields and microprobe design in high-resolution NMR. J. Magn. Reson. Ser. A. 109:1994;265-269.
7. Doskocilova D., Tao D.D., Schneider B. Effects of macroscopic spinning upon linewidth of NMR signals of liquid in magnetically inhomogeneous systems. Czech. J. Phys. B. 25:1975;202-209.
8. Live D.H., Chan S.I. Bulk susceptibility corrections in nuclear magnetic resonance experiments using superconducting solenoids. Anal. Chem. 42:1970;791-792.
9. Bacon M.R., Maciel G.E. Solvent effects on the five shielding constants in tetramethylsilane and cyclohexane. J. Am. Chem. Soc. 95:1973;2413-2426.
10. Emsley J.W., Feeney J., Sutcliffe L.H. High Resolution Nuclear Magnetic Resonance Spectroscopy. vol. 1:1965;Permagon Press, Oxford. pp. 256-279.
11. Bothnerby A.A., Glick R.E. Medium effects in nuclear magnetic resonance spectra of liquids. 2. Simple aliphatic molecules. J. Chem. Phys. 26:1957;1647-1650.
12. Bothnerby A.A., Glick R.E. Medium effects in the nuclear magnetic resonance spectra of liquids. 3. Aromatics. J. Chem. Phys. 26:1957;1651-1654.
13. Bothnerby A.A. Medium effects in the nuclear magnetic resonance spectra of liquids. 4. Nature of the effects. J. Mol. Spectrosc. 5:1960;52-61.
14. Hayashi S., Hayamizu K. Shift references in high-resolution solid-state NMR. Bull. Chem. Soc. Jpn. 62:1989;2429-2430.
15. Hayashi S., Hayamizu K. Chemical-shift standards in high-resolution solid-state NMR (1) C-13, Si-29 and H-1 nuclei. Bull. Chem. Soc. Jpn. 64:1991;685-687.
16. VanderHart D.L. Magnetic, susceptibility & high resolution NMR of liquids & solids. Grant D.M., Harris R.K. Encyclopedia of Nuclear Magnetic Resonance. 1996;Wiley, Chichester.
17. Hayashi S., Yanagisawa M., Hayamizu K. Nuclear-magnetic-resonance chemical-shifts of pure organic-solvents determined by magic angle spinning. Anal. Sci. 7:1991;955-957.
18. Lide D.R. CRC Handbook of Chemistry and Physics. 78th ed. 1997;CRC Press, Boca Raton, FL.
19. Davidson D.W. A dilatometric study of solid methanol-D. Can. J. Chem. 34:1956;1243-1248.
20. Hoare F.E. Diamagnetic susceptibility of heavy water. Nature. 137:1936;497-498.
21. Broersma S. The Magnetic susceptibility of organic compounds. J. Chem. Phys. 17:1949;873-882.
22. Lister M.W., Marson R. Magnetic susceptibilities of some compounds of silicon. Can. J. Chem. 42:1964;2101-2106.
23. Williamson P.T.F., Grobner G., Spooner P.J.R., Miller K.W., Watts A. Probing the agonist binding pocket in the nicotinic acetylcholine receptor: a high-resolution solid-state NMR approach. Biochemistry. 37:1998;10854-10859.
24. Wishart D.S., Bigam C.G., Yao J., Abildgaard F., Dyson H.J., Oldfield E., Markley J.L., Sykes B.D. H-1, C-13 and N-15 chemical-shift referencing in biomolecular NMR. J. Biomol. NMR. 6:1995;135-140.
25. Markley J.L., Bax A., Arata Y., Hilbers C.W., Kaptein R., Sykes B.D., Wright P.E., Wuthrich K. Recommendations for the presentation of NMR structures of proteins and nucleic acids - (IUPAC Recommendations 1998). Pure Appl. Chem. 70:1998;117-142.