Nuclear magnetic resonance to characterize and monitor cultural heritage

Progress in Nuclear Magnetic Resonance Spectroscopy

Volumn 64, Issue , 2012, Pages 29-69

  Capitani, Donatella ^a   Di Tullio, Valeria ^a   Proietti, Noemi ^a  

^a CNR   (Italy)

Author keywords

Ageing detection by NMR; Cultural Heritage; Micro invasive NMR characterization; Moisture detection by NMR; Non invasive NMR characterization; Porous materials

Indexed keywords

CHARACTERIZATION; CHEMICAL MODIFICATION; MOISTURE DETERMINATION; POROUS MATERIALS;

ARCHAEOLOGICAL FINDINGS; ARCHAEOLOGICAL MATERIALS; CHEMICAL CHARACTERIZATION; CHEMICAL-PHYSICAL TRANSFORMATIONS; CULTURAL HERITAGES; MOISTURE DETECTION; NUCLEAR MAGNETIC RESONANCE (NMR); STRUCTURAL MODIFICATIONS;

NUCLEAR MAGNETIC RESONANCE;

EID: 84861092779     PISSN: 00796565     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.pnmrs.2011.11.001     Document Type: Review

References (199)

1. R.R. Ernst, G. Bodenhausen, and A. Wokaun Principles of Nuclear Magnetic Resonance in One and Two dimensions 1987 Clarendon Press Oxford
2. P. Stilbs Fourier transform pulsed-gradient spin-echo studies of molecular diffusion Prog. Nucl. Magn. Reson. Spectrosc. 19 1987 1 45
3. K.F. Morris, and C.S. Johnson Diffusion-ordered two-dimensional nuclear magnetic resonance spectroscopy J. Am. Chem. Soc. 114 1992 3139 3141
4. S. Braun, H.O. Kalinowski, and S. Berger 150 and More Basic NMR Experiments A Practical Course 1998 Wiley-VCH Weinheim Germany
5. M. Spraul, A.S. Feund, R.E. Nast, R.S. Withers, W.E. Maas, and O. Corcoran Advancing NMR sensitivity for LC-NMR-MS using a cryoflow probe: application to the analysis of acetaminophen in urine Anal. Chem. 75 2003 1546 1551
6. G. Schlotterbeck, A. Ross, R. Hochstrasser, H. Senn, T. Kühn, D. Marek, and O. Schett High-resolution capillary tube NMR. A miniaturized 5-(L high-sensitivity TXI Probe for mass-limited samples, off-line LC NMR, and HT NMR Anal. Chem. 74 2002 4464 4471 (Pubitemid 35006435)
7. K.J.D. MacKenzie, M.E. Smith, in: R.W. Cahn (Ed.), Multinuclear Solid-State NMR of Inorganic Materials, Pergamon Materials Series 6, The Netherlands, 2002.
8. K. Schmidt-Rohr, and H.W. Spiess Multidimensional Solid-State NMR and Polymers 1994 Academic Press London
9. B. Blümich NMR Imaging of Materials, Monographs on the Physics and Chemistry of Materials 57 2003 Clarendon Press Oxford
10. A.T. Watson, and C.T. Chang Characterizing porous media with NMR methods Progr. Nucl. Magn. Reson. Spectrosc. 31 1997 343 386 (Pubitemid 127427749)
11. P. Galvosas, and P.T. Callaghan Multi-dimensional inverse Laplace spectroscopy in the NMR of porous media C. R. Phys. 11 2010 172 180
12. 2 distributions, connection with capillary pressure, clay effect, and determination of the surface relaxivity parameter ρ2 Magn. Reson. Imag. 14 1996 761 767 (Pubitemid 26415966)
13. K.J. Dunn, D.J. Bergman, and G.A. Latorraca Nuclear Magnetic Resonance Petrophysical and Logging Applications vol. 32 2002 Pergamon Press
14. M.D. Hürlimann Effective gradients in porous media due to susceptibility differences J. Magn. Reson. 131 1998 232 240 (Pubitemid 128450561)
15. 2 correlation spectra obtained using a fast two-dimensional Laplace inversion J. Magn. Reson. 154 2002 261 268
16. M.D. Hürlimann, and L. Venkataramanan Quantitative measurement of two-dimensional distribution functions of diffusion and relaxation in grossly inhomogeneous fields J. Magn. Reson. 157 2002 31 42
17. M.D. Hürlimann, L. Venkataramanan, and C. Flaum The diffusion-spin relaxation time distribution as an experimental probe to characterize fluid mixtures in porous media J. Chem. Phys. 117 2002 10223 10232
18. A.E. English, K.P. Whittall, M.L.G. Joy, and R.M. Henkelman Quantitative two-dimensional time correlation relaxometry Magn. Reson. Med. 22 1991 425 434
19. J.H. Lee, C. Labadie, C.S. Springer Jr, and G.S. Harbison 2-dimensional inverse Laplace transform NMR - altered relaxation-times allow detection of exchange-correlation J. Am. Chem. Soc. 115 1993 7761 7764
20. B. Blümich, J. Perlo, and F. Casanova Mobile single-sided NMR Progr. Nucl. Magn. Reson. 52 2008 197 269
21. R.L. Kleinberg, A. Sezginer, D.D. Griffin, and M. Fukuhara Novel NMR apparatus for investigating an external sample J. Magn. Reson. 97 1992 466 485
22. G. Eidmann, R. Savelsberg, P. Blümer, and B. Blümich The NMR-MOUSE, a mobile universal surface explorer J. Magn. Reson. A 122 1996 104 109 (Pubitemid 126751817)
23. J. Mitchell, P. Blümer, and P.J. McDonald Spatially resolved nuclear magnetic resonance studies of planar samples Progr. Nucl. Magn. Reson. 48 2006 161 181 (Pubitemid 44308493)
24. R. Kimmich NMR Tomography, Diffusometry, Relaxometry 1997 Springer-Verlag Berlin
25. T.J. Norwood, and R.A. Quilter A robust NMR method for studying diffusion J. Magn. Reson. 97 1992 99 110
26. M. Klein, R. Fechete, D.E. Demco, and B. Blümich Self-diffusion measurements by a constant-relaxation methods in strongly inhomogeneous magnetic fields J. Magn. Reson. 164 2003 310 320
27. A. Marko, B. Walter, and W. Arnold Application of a portable nuclear magnetic resonance surface probe to porous media J. Magn. Reson. 185 2007 19 27 (Pubitemid 46484393)
28. J. Perlo, V. Demas, F. Casanova, C.A. Meriles, J. Reimer, A. Pines, and B. Blümich High resolution NMR spectroscopy with a portable single-sided sensor Science 308 2005 1279 (Pubitemid 40746118)
29. D. Sakellariou, C.A. Meriless, and A. Pines Advances in ex situ nuclear magnetic resonance C. R. Phys. 5 2004 337 347 (Pubitemid 38613153)
30. 1H spectroscopy Science 315 2007 1110 1112 (Pubitemid 46328018)
31. J. Perlo, F. Casanova, and B. Blümich Profiles with microscopic resolution by single-sided NMR J. Magn. Reson. 176 2005 64 70 (Pubitemid 41162476)
32. F. Presciutti, J. Perlo, F. Casanova, S. Glöggler, C. Miliani, B. Blümich, B.G. Brunetti, and A. Sgamellotti Noninvasive nuclear magnetic resonance profiling of painting layers Appl. Phys. Lett. 93 2008 033505-1 033505-3
33. B. Blümich, F. Casanova, J. Perlo, F. Presciutti, C. Anselmi, and B. Doherty Noninvasive testing of art and cultural heritage by mobile NMR Acc. Chem. Res. 43 2010 761 770
34. E. Del Federico, S.A. Centeno, C. Kehlet, P. Currier, D. Stockman, and A. Jerschow Unilateral NMR applied to the conservation of works of art Anal. Bioanal. Chem. 396 2010 213 222
35. 13C CPMAS NMR spectroscopy and micro-analytical techniques for studying the materials and state of conservation of an ancient Egyptian wooden sarcophagus Anal. Bioanal. Chem. 399 2011 3117 3131
36. V. Di Tullio, N. Proietti, D. Capitani, I. Nicolini, and A.M. Mecchi NMR depth profiles as a non-invasive analytical tool to probe the penetration depth of hydrophobic treatments and inhomogeneities in treated porous stones Anal. Bioanal. Chem. 400 2011 3151 3164
37. F.J. Rühli, T. Böni, J. Perlo, F. Casanova, M. Baias, E. Egarter, and B. Blümich Non-invasive spatial tissue discrimination in ancient mummies and bones in situ by portable nuclear magnetic resonance J. Cult. Heritage 8 2007 257 263
38. D. Camuffo Physical weathering of stones Sci. Tot. Environ. 167 1995 1 14
39. G.C. Borgia, V. Bortolotti, M. Camaiti, F. Cerri, P. Fantazzini, and F. Piacenti Performance evolution of hydrophobic treatments for stone conservation investigated by MRI Magn. Reson. Imag. 19 2001 513 516 (Pubitemid 32692225)
40. G.C. Borgia, M. Camaiti, F. Cerri, P. Fantazzini, and F. Piacenti Study of water penetration in rock materials by nuclear magnetic resonance tomography: hydrophobic treatment effects J. Cult. Heritage 1 2000 127 132
41. M. Gombia, V. Bortolotti, R.J.S. Brown, M. Camaiti, and P. Fantazzini Models of water imbibition in untreated and treated porous media validated by quantitative magnetic resonance imaging J. Appl. Phys. 103 2008 094913-1 094913-8
42. M. Alesiani, S. Capuani, B. Maraviglia, R. Giorgi, and P. Baglioni Effects induced in marbles by water repellent compounds: the NMR contributions Appl. Magn. Reson. 23 2002 63 73
43. M. Alesiani, S. Capuani, and B. Maraviglia NMR applications to low porosity carbonate stones Magn. Reson. Imag. 21 2003 799 804 (Pubitemid 37259907)
44. M. Alesiani, S. Capuani, and B. Maraviglia NMR study on the early stages of hydration of a porous carbonate stone Magn. Reson. Imag. 21 2003 333 335 (Pubitemid 36874865)
45. P.T. Callaghan Principles of Nuclear Magnetic Resonance Microscopy 1991 Oxford University Press Oxford
46. L. Apollonia, G.C. Borgia, V. Bortolotti, R.J.S. Brown, P. Fantazzini, and G. Rezzaro Effects of hydrophobic treatments of stone on pore water studied by continuous distribution analysis of NMR relaxation times Magn. Reson. Imag. 19 2001 509 512 (Pubitemid 32692224)
47. P. López-Arce, L.S. Gomez-Villalba, L. Pinho, M.E. Fernández-Valle, M. Álvarez de Buergo, and R. Fort Influence of porosity and relative humidity on consolidation of dolostone with calcium hydroxyde nanoparticles: effectiveness assessment with non-destructive techniques Mater. Charact. 61 2010 168 184
48. J. Arnold, C. Clauser, R. Pechnig, S. Anferova, V. Anferov, and B. Blümich Porosity and permeability from mobile NMR core-scanning Petrophysics 47 2006 306 314 (Pubitemid 44326258)
49. S. Anferova, V. Anferov, D.G. Rata, B. Blümich, J. Arnold, C. Clauser, P. Blümer, and H. Raich A Mobile NMR device for measurements of porosity and pore size distributions of drilled core samples Concepts Magn. Reson. Part B Magn. Reson. Eng. 23B 2004 26 32 (Pubitemid 40646171)
50. B. Blümich, S. Anferova, R. Pechnig, H. Pape, J. Arnold, and C. Clauser Mobile NMR for porosity analysis of core sections J. Geophys. Eng. 1 2004 177 180
51. S. Sharma, F. Casanova, W. Wache, A. Segre, and B. Blümich Analysis of historical porous building materials by the NMR-MOUSE Magn. Reson. Imag. 21 2003 249 255 (Pubitemid 36874852)
52. B. Blümich, S. Anferova, K. Kremer, S. Sharma, V. Herrmann, and A. Segre Unilateral NMR for quality control: the NMR-MOUSE® Spectroscopy 18 2003 18 34
53. N. Proietti, D. Capitani, S. Cozzolino, M. Valentini, E. Pedemonte, E. Princi, S. Vicini, and A.L. Segre In situ and frontal polymerization for the consolidation of porous stones: an unilateral NMR and a magnetic resonance imaging study J. Phys. Chem. B 110 2006 23719 23728 (Pubitemid 46065802)
54. S. Chen, H.K. Liaw, and A.T. Watson Fluid saturation-dependent nuclear magnetic resonance spin-lattice relaxation in porous media and pore structure analysis J. Appl. Phys. 74 1993 1473 1479
55. V. Bortolotti, M. Camaiti, C. Casieri, F. De Luca, P. Fantazzini, and C. Terenzi Water absorption kinetics in different wettability conditions studied at pore and sample scales in porous media by NMR with portable single-sided and laboratory imaging devices J. Magn. Reson. 181 2006 287 295 (Pubitemid 44107746)
56. M. Brai, C. Casieri, F. De Luca, P. Fantazzini, M. Gombia, and C. Terenzi Validity of NMR pore-size analysis of cultural heritage ancient building materials containing magnetic impurities Solid State Nucl. Magn. Reson. 32 2007 129 135
57. J.R. Clifton, and G.J.C. Frohnsdorf Stone-Consolidating Materials: A Status Report, Conservation of Historic Stone Building and Monuments 1982 National Academy Press Washington, DC pp. 287-311
58. L. Pel, H. Huinink, and K. Kopinga Ion transport and crystallization in historical objects as studied by NMR Appl. Phys. Lett. 81 2002 2893 2895
59. L. Pel, H. Huinink, and K. Kopinga Ion transport and crystallization in porous materials as studied by magnetic resonance imaging J.M. Huyghe, IUTAM Proceedings on Physicochemical and Electromechanical Interactions in Porous Media 2005 Springer 149 158
60. K. Kopinga, and L. Pel One-dimensional scanning of moisture in porous materials with NMR Rev. Sci. Instrum. 65 1994 3673 3681
61. L.A. Rijniers, L. Pel, H.P. Huinink, and K. Kopinga Salt crystallization as damage mechanism in porous building materials: a nuclear magnetic resonance study Magn. Reson. Imag. 23 2005 273 276
62. L.A. Rijniers, H.P. Huinink, L. Pel, and K. Kopinga Experimental evidence of crystallization pressure inside porous media Phys. Rev. Lett. 94 2005 075503-1 075503-4
63. K.R. Brownstein, and C.E. Tarr Importance of classical diffusion in NMR studies of water in biological cells Phys. Rev. A 19 1979 2446 2453
64. L.A. Rijniers, P.C.M.M. Magusin, H.P. Huinink, L. Pel, and K. Kopinga Sodium NMR in porous building materials J. Magn. Reson. 167 2004 25 30
65. M. Gombia, V. Bortolotti, R.J. Brown, M. Camaiti, L. Cavallero, and P. Fantazzini Water vapor absorption in porous media polluted by calcium nitrate studied by time domain nuclear magnetic resonance J. Phys. Chem. B 113 2009 10580 10586
66. G.C. Borgia, R J.S. Brown, and P. Fantazzini Uniform-penalty inversion of multiexponential decay data J. Magn. Reson. 1321 1998 65 77 (Pubitemid 128450587)
67. 2 data, systematic data errors, and diagnostics J. Magn. Reson. 147 2000 273 285
68. T. Diaz Gonçalves, L. Pel, and J.D. Rodrigues Influence of paints on drying and salt distributions processes in porous building materials Constr. Build. Mater. 23 2009 1751 1759
69. M. Matteini, An assessment of florentine methods of wall painting conservation based on the use of mineral treatments in the conservation of wall paintings, in: Sharon Cather (Ed.), The Proceedings of a Symposium Organized by the Courtauld Institute of Art and the Getty Conservation Institute, London, Tien Vah Press, Singapore, July 13-16, 1987.
70. V.G.G. Amoroso, and V. Fassina Stone Decay and Conservation 1983 Elsevier Lausanne
71. A. Sansonetti, E. Rosina, and N. Ludwig Moisture damage new tools for the protection of cultural heritage in Italy: innovative techniques for in situ diagnostics Mater. Eval. 69 1 2011 41 46
72. E. Rosina, N. Ludwig, Optimal thermographic procedure for moisture analysis in buildings materials, in: Diagnostic Imaging Technologies and Industrial Applications 1999, Munich, Germany, SPIE Proceedings, vol. 3827, SPIE ed. WA, USA, pp. 22-33.
73. N. Proietti, D. Capitani, E. Rossi, S. Cozzolino, and A.L. Segre Unilateral NMR study of a XVI century wall painted J. Magn. Reson. 186 2007 311 318 (Pubitemid 46880441)
74. D. Capitani, N. Proietti, M. Gobbino, L. Soroldoni, U. Casellato, M. Valentini, and E. Rosina An integrated study for mapping the moisture distribution in an ancient damaged wall painting Anal. Bioanal. Chem. 395 2009 2245 2253
75. R. Olmi, S. Priori, D. Capitani, N. Proietti, L. Capineri, P. Falorni, R. Negrotti, and C. Riminesi Innovative techniques for sub-surface investigation Mater. Eval. 69 2011 89 96
76. V. Di Tullio, N. Proietti, M. Gobbino, D. Capitani, R. Olmi, S. Priori, C. Riminesi, and E. Giani Non-destructive mapping of dampness and salts in degraded wall paintings in hypogeous buildings: the case of St. Clement at mass fresco in St. Clement Basilica, Rome Anal. Bioanal. Chem. 396 2010 1885 1896
77. V. Di Tullio, N. Proietti, G. Gentile, E. Giani, D. Poggi, D. Capitani, Unilateral NMR, a non-invasive tool for monitoring in situ the effectiveness of intervention to reduce the capillary rise of water in an ancient deteriorated wall painting, Int. J. Spectrosc., in press, doi: 10.1155/2012/494301.
78. B. Blümich, A. Haber, F. Casanova, E. Del Federico, V. Boardman, G. Wahl, A. Stilliano, and L. Isolani Noninvasive depth profiling of walls by portable nuclear magnetic resonance Anal. Bioanal. Chem. 397 2010 3117 3125
79. N. Proietti, D. Capitani, F. Presciutti, E. Rossi, A.L. Segre, G. Botticelli, Analysis of the conservation state of frescoes by unilateral NMR, in: U. Baldini, P.A. Vigato, (Eds.), The discovery of a forgotten pictorial cycle: Casa Vasari in Florence. An Interdisciplinary approach to the Restoration Project, Edizion Polistampa, Firenze, 2006, pp. 117-130.
80. N. Proietti, D. Capitani, R. Lamanna, F. Presciutti, E. Rossi, and A.L. Segre Fresco Paintings studied by unilateral NMR J. Magn. Reson. 177 2005 111 117 (Pubitemid 41336670)
81. F. Presciutti, D. Capitani, A. Sgamellotti, B.G. Brunetti, F. Costantino, S. Viel, and A. Segre Electron paramagnetic resonance, scanning electron microscopy with energy dispersion X-ray spectrometry, X-ray powder diffraction, and NMR characterization of iron-rich fired clays J. Phys. Chem. B 109 2005 22147 22158
82. L. Frydman, and J.H. Harwood Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR J. Am. Chem. Soc. 117 1995 5367 5368
83. C. Fernandez, and J.P. Amoureux Triple-quantum MAS-NMR of quadrupolar nuclei Solid State Nucl. Magn. Reson. 5 1996 315 321 (Pubitemid 126412250)
84. D. Massiot, F. Fayon, M. Capron, I. King, S. LeCalvé, B. Alonso, J.O. Durand, B. Bujoli, Z. Gan, and G. Hoatson Modelling one and two-dimensional solid-state NMR spectra Magn. Reson. Chem. 40 2002 70 76 (Pubitemid 37296946)
85. L. Pel, K. Kopinga, G. Bertram, and G. Lang Water absorption in a fired-clay brick observed by NMR scanning J. Phys. D: Appl. Phys. 28 1995 675 680
86. P.J. McDonald, J. Mitchell, M. Mulheron, L. Monteilhet, and J.P. Korb Two-dimensional correlation relaxation studies of cement pastes Magn. Reson. Imag. 25 2007 470 473 (Pubitemid 46656323)
87. P.J. McDonald, P.S. Aptaker, J. Mitchell, and M. Mulheron A unilateral NMR magnet for sub-structure analysis in the built environment: the surface GARField J. Magn. Reson. 185 2007 1 11 (Pubitemid 46484395)
88. S. Anferova, V. Anferov, J. Arnold, E. Talnishnikh, M.A. Voda, K. Kupferschläger, P. Blümer, C. Clauser, and B. Blümich Improved Halbach sensor for NMR scanning of drill cores Magn. Reson. Imag. 25 2007 474 480 (Pubitemid 46656324)
89. Y.Q. Song Novel two-dimensional NMR of diffusion and relaxation for material characterization S. Stapf, S. Han, NMR in Chemical Engineering 2006 Wiley-VCH Weinheim 163 183
90. C. Casieri, C. Terenzi, and F. De Luca Two-dimensional longitudinal and transverse relaxation time correlation as a low-resolution nuclear magnetic resonance characterization of ancient ceramics J. Appl. Phys. 105 2009 034901-1-8
91. C. Terenzi, C. Casieri, A.C. Felici, M. Piacentini, M. Venditelli, and F. De Luca Characterization of elemental and firing-dependent properties of Phlegrean ceramics by non-destructive ED-XRF and NMR techniques J. Archaeol. Sci. 37 2010 1403 1412
92. V. Tudisca, C. Casieri, F. Demma, M. Diaz, L. Piñol, C. Terenzi, and F. De Luca Firing technique characterization of black-slipped pottery in Praeneste by low field 2D NMR relaxometry J. Archaeol. Sci. 38 2011 352 359
93. M. R. Gillespie, M.T. Stiles, BGS Rock Classification Scheme, Vol. 1 Classification of Igneous Rocks British Geological Survey, Research Report RR 96-0, Keyworth, Nottingham, UK, 1999.
94. 27Al MAS NMR as a tool to characterize volcanic tuffs and assess their suitability for industrial applications J. Phys. Chem. C 114 2010 9328 9343
95. M. de Gennaro, and A. Langella Italian zeolitized rocks of technological interest Miner. Deposita 31 1996 452 472
96. P. Ciccioli, C. Cattuto, P. Plescia, V. Valentini, and R. Negrotti Geochemical and engineering geological properties of the volcanic tuffs used in the Etruscan Tombs of Norchia (Northern Latium, Italy) and a study of the factors responsible for their rapid surface and structural decay Archaeometry 52 2010 229 251
97. J. Klinowski, S. Ramdas, J.M. Thomas, C.A. Fyfe, and J.S. Hartmann A re-examination of Si, Al, ordering in zeolites NaX and NaY J. Chem. Soc. Faraday Trans. 2 78 1982 1025 1050
98. 27Al magic angle spinning nuclear magnetic resonance to studies of the building materials of historical monuments Solid State Nucl. Magn. Reson. 13 1999 263 269 (Pubitemid 34867529)
99. G. Demortier PIXE, PIGE and NMR study of the masonry of the pyramid of Cheops at Giza Nucl. Instrm. Meth. Phys. Res. B 226 2004 98 109
100. M.P. Colombini, A. Andreotti, I. Bonaduce, F. Modugno, and E. Ribechini Analytical strategies for characterizing organic paint media using gas chromatography/mass spectrometry Acc. Chem. Res. 43 2010 715 727
101. L. Mannina, A.P. Sobolev, and A. Segre Olive oil as seen by NMR and chemometrics Spectrosc. Eur. 15 2003 6 14
102. 1H nuclear magnetic resonance study of the minor components in virgin olive oils J. Am. Oil. Chem. Soc. 73 1996 747 758 (Pubitemid 126525498)
103. L. Mannina, F. Presciutti, N. Proietti, D. Capitani, A. Sgamellotti, B.B. Brunetti, unpublished results.
104. A. Spyros, and D. Anglos Study of aging in oil paintings by 1D and 2D NMR spectroscopy Anal. Chem. 76 2004 4929 4936 (Pubitemid 39180316)
105. A. Spyros, and D. Anglos Studies of organic paint binders by NMR spectroscopy Appl. Phys. A 83 2006 705 708
106. G. Cipriani, A. Salvini, L. Dei, A. Macherelli, F.S. Cecchi, and C. Giannelli Recent advances in swollen-state NMR spectroscopy for the study of drying oils J. Cult. Heritage 10 2009 388 395
107. M. Paci, C. Federici, D. Capitani, N. Perenze, and A.L. Segre NMR study of paper Carbohyd. Polym. 26 1995 289 297
108. 1H NMR relaxation study of papers a system of cellulose and water Tappi Journal 79 1996 113 122 (Pubitemid 126617061)
109. 1H NMR relaxation study of cellulose and water interaction in paper Tappi J. 82 1999 117 124 (Pubitemid 129636813)
110. D. Attanasio, D. Capitani, C. Federici, and A.L. Segre Electron spin resonance study of paper samples dating from the XV to the XVIII century Archeometry 37 1995 377 384
111. 13C NMR study of paper ACS Symp. Ser. 598 1995 333 353
112. 13C NMR Macromolecules 17 1984 1465 1472
113. 13C NMR study of cellulose polymorphs Macromolecules 22 1989 3168 3172
114. K. Overloop, and L. Van Gerven Freezing phenomena in adsorbed water as studied by NMR J. Magn. Reson. A 101 1993 179 187
115. D. Capitani, N. Proietti, F. Ziarelli, and A.L. Segre NMR study of water-filled pores in one of the most widely used polymeric material: the paper Macromolecules 35 2002 5536 5543 (Pubitemid 34741248)
116. J. Clauss, K. Schmidt-Rohr, A. Adam, C. Boeffel, and H.W. Spiess Stiff macromolecules with aliphatic side chains: side-chain mobility, conformation, and organization from 2D solid-state NMR spectroscopy Macromolecules 25 1992 5208 5214 (Pubitemid 23572155)
117. D. Radloff, C. Boeffel, and H.W. Spiess Cellulose and cellulose/poly(vinyl alcohol) blends. 2. Water organization revealed by solid-state NMR spectroscopy Macromolecules 29 1996 1528 1534 (Pubitemid 126520515)
118. J. Clauss, K. Schmidt Rohr, and H.W. Spiess Determination of domain sizes in heterogeneous polymers by solid-state NMR Acta Polym. 44 1993 1 17
119. M.P. Coughlan, M.G. Touhy, X.F. Filho, J. Puls, M. Claeyssens, M. Vrsanska, and M.M. Hughes Enzymological aspects of microbial emphasis on fungal system M.P. Coughlan, G.P. Hazlewood, Hemicellulose and Hemicellulases 1993 Portland Press London 53 85
120. D. Capitani, M.C. Emanuele, A.L. Segre, C. Fanelli, A.A. Fabbri, D. Attanasio, B. Focher, and G. Capretti Early detection of enzymatic attack on paper by NMR relaxometry, EPR spectroscopy and X-ray powder spectra Nord. Pulp Pap. Res. 13 1998 95 100 (Pubitemid 128434142)
121. C. Boileau, S. Pessanha, C. Tardif, K. Castro, N. Proietti, D. Capitani, S. Vicini, J.M. Madariaga, M.L. Carvahlo, and E. Princi Efficacy of waterborne polyurethane to prevent the enzymatic attack on paper-based materials J. Appl. Polym. Sci. 113 2009 2030 2040
122. 13C CP-MAS NMR spectroscopy Quinio 2 2000 37 43
123. S. Margutti, S. Vicini, N. Proietti, D. Capitani, G. Conio, E. Pedemonte, and A.L. Segre Physical chemical characterization of acrylic polymers grafted on cellulose Polymer 43 2002 6183 6194
124. R.K. Harris Relaxation and double-resonance in solid-state NMR R.K. Harris, P. Granger, Multinuclear Magnetic Resonance in Liquids and Solids-Chemical Application, NATO ASI Series 322 1988 Kluwer Dordrecht 291 309
125. B. Blümich, S. Anferova, S. Sharma, A.L. Segre, and C. Federici Degradation of historical paper non destructive analysis by the NMR-MOUSE J. Magn. Reson. 161 2003 204 209
126. N. Proietti, D. Capitani, E. Pedemonte, B. Blümich, and A.L. Segre Monitoring degradation in paper: non-invasive analysis by unilateral NMR. Part II J. Magn. Reson. 170 2004 113 120
127. K. Castro, E. Princi, N. Proietti, M. Manso, D. Capitani, S. Vicini, J.M. Madariaga, and M.L. Carvahlo Assessment of the weathering effects on cellulose based materials trhough a multianalytical approach Nucl. Instrm. Meth. Phys. Res. B 269 2011 1401 1410
128. K. Castro, S. Pessanha, N. Proietti, E. Princi, D. Capitani, M.L. Carvalho, and J.M. Madariaga Noninvasive and nondestructive NMR, Raman and XRF analysis of a Blaeu coloured map from the seventeenth century Anal. Bioanal. Chem. 391 2008 433 441
129. K. Castro, N. Proietti, E. Princi, S. Pessanha, M.L. Carvalho, S. Vicini, D. Capitani, and J.M. Madariaga Analysis of a coloured Dutch map from the eighteenth century: the need for a multi-analytical spectroscopic approach using portable instrumentation Anal. Chim. Acta 622 2008 187 194
130. E. Del Federico, S.A. Centeno, C. Kehelet, P. Currier, D. Stockman, and A. Jerschow Unilateral NMR Applied to the conservation of works of art Anal. Bioanal. Chem. 396 2010 213 220
131. I. Viola, S. Bubici, C. Casieri, and F. De Luca The codex major of the Collectio Altaempsiana: a non-invasive NMR study of paper J. Cult. Heritage 5 2004 257 261 (Pubitemid 39305427)
132. C. Casieri, S. Bubici, I. Viola, and F. De Luca A low-resolution non-invasive NMR characterization of ancient paper Solid State Nucl. Magn. Reson. 26 2004 65 73
133. R.H. Newman, and J.A. Hemmingson Determination of the degree of cellulose crystallinity in wood by carbon-13 NMR spectroscopy Holzforschung 44 1990 351 355
134. 13C NMR investigation of molecular ordering in celluloses Carbohydr. Res. 302 1997 19 25 (Pubitemid 27343473)
135. S.L. Mannu NMR studies of wood and wood products Progr. Nucl. Magn. Reson. Spectrosc. 40 2002 151 174
136. J.F. Haw, G.E. Maciel, and E.A. Schroeder Carbon-13 nuclear magnetic resonance spectrometric study of wood and wood pulping with cross polarization and magic-angle spinning Anal. Chem. 56 1984 1323 1329
137. 13C assignments of the carbon atoms in the aromatic rings of lignin model compounds of the arylglycerol beta-aryl ether type Magn. Reson. Chem. 44 2006 976 979 (Pubitemid 44482899)
138. 13C NMR using the 2D INADEQUATE experiment Magn. Reson. Chem. 36 1998 597 600 (Pubitemid 128359125)
139. D.S. Argyropoulos D.S. Argyropoulos, Advances in Lignocellulosics Characterization 1999 TAPPI Press Atlanta
140. A.M. Gil, and C. Pascoal Neto Solid state NMR studies of wood and other lignocellulosic materials Annu. Rep. NMR Spectrosc. 37 1999 75 117
141. 13C high-resolution solid-state NMR for structural elucidation of archaeological woods Prog. Nucl. Magn. Reson. Spectrosc. 55 2009 199 214
142. C.D. Araujo, A.L. MacKey, J.R.T. Hailey, K.P. Whittal, and H. Le Proton magnetic resonance techniques for characterization of water in wood: application to white spruce Wood Sci. Technol. 26 1992 101 113
143. 13C CP/MAS NMR Archaeometry 50 2008 129 141
144. M. Bardet, M.F. Foray, and Q.K. Tran High-resolution solid-state CPMAS NMR study of archaeological woods Anal. Chem. 74 2002 4386 4390 (Pubitemid 35006425)
145. M. Bardet, M.F. Foray, S. Maron, P. Goncalves, and Q.K. Tran Characterization of wood components of Portuguese medieval dugout canoes with high-resolution solid-state NMR Carbohyd. Polym. 57 2004 419 424
146. 13C CPMAS NMR spectroscopic analysis applied to wood characterization Appl. Magn. Reson. 29 2005 177 184 (Pubitemid 41767745)
147. 13C high-resolution solid state CP-MAS NMR J. Archaeol. Sci. 34 2007 1670 1676 (Pubitemid 47099447)
148. S. Viel, D. Capitani, N. Proietti, F. Ziarelli, and A.L. Segre NMR spectroscopy applied to the Cultural Heritage: a preliminary study on ancient wood characterization Appl. Phys. A 79 2004 357 361
149. A. Salanti, L. Zoia, E.L. Tolppa, G. Giachi, and M. Orlandi Characterization of waterlogged wood by NMR and GPC techniques Microchem. J. 95 2010 345 352
150. C. Crestini, N.M.N. El Hadidi, and G. Palleschi Characterization of archaeological wood: a case study on deterioration of a coffin Microchem. J. 92 2009 150 154
151. L. Braunschweiler, and R.R. Ernst Coherence transfer by isotropic mixing: application to proton correlation spectroscopy J. Magn. Reson 53 1983 521 528
152. A. Bax, and D.G. Davis MLEV-17-based two-dimensional homonuclear magnetization transfer spectroscopy J. Magn. Reson. 65 1985 355 360
153. 2O in archaeological wood measured by 1-D NMR profiles Appl. Magn. Reson. 17 1999 49 64
154. D.J. Cole-Hamilton, B. Kaye, J.A. Chudek, and G. Hunter Nuclear magnetic resonance imaging of waterlogged wood Studies in Conservation 40 1995 41 50
155. J. Nagyvary, J.A. DiVerdi, N.L. Owen, and H.D. Tolley Wood used by Stradivari and Guarneri Nature 444 2006 565 (Pubitemid 44864427)
156. R. Chûiô, A. Shimaoka, K. Nagaoka, A. Kurata, and M. Inoue Primary structure of archeological silk and ancient climate Polymer 37 1996 3693 3696 (Pubitemid 126375862)
157. R.D.B. Fraser, and T.P. MacRae Conformation in Fibrous Proteins 1973 Academic Press New York
158. J. Kümmerlen, J.D. van Beek, F. Vollrath, and B.H. Meier Local structure in spider dragline silk investigated by two-dimensional spin-diffusion Nucl. Mag. Reson. Macromol. 29 1996 2920 2928 (Pubitemid 126554020)
159. R. Chûiô, K. Fukutani, and Y. Magoshi Estimation of physical properties of archaeological silk with NMR relaxation time and fluctuation-dissipation theorem in NMR spectroscopy of polymers in solution and in solid state ACS Symp. Ser. 834 2002 83 91 (Pubitemid 135694021)
160. 13C solid state NMR characterization Eur. Polym. J. 41 2005 1196 1203 (Pubitemid 40539129)
161. E. Princi, S. Vicini, E. Pedemonte, N. Proietti, D. Capitani, A.L. Segre, L. D'Orazio, G. Gentile, C. Polcaro, and E. Martuscelli Physical and chemical characterization of cellulose based textiles modified by periodate oxidation Macromol. Symp. 218 2004 343 352 (Pubitemid 40065417)
162. G.N. Ramachandran, and A.H. Reddi Biochemistry of Collagen 1976 Plenum Press New York
163. A.E. Aliev Solid-state NMR studies of collagen-based parchments and gelatin Biopolymers 77 2005 230 245 (Pubitemid 40432489)
164. H. Kalinowski, S. Berger, and S. Braun Carbon-13 NMR Spectroscopy 1988 J. Wiley & Sons New York
165. 15N NMR study on crystalline Leu- and Met-enkephalins distinction of polymorphs, backbone dynamics and local conformational rearrangements induced by dehydration or freezing motions of bound solvent J. Phys. Chem. B 102 1998 2826 2834 (Pubitemid 128606330)
166. 13C solid state NMR and micro-thermomechanical studies of historical parchment J. Therm. Anal. Calorim. 71 2003 939 950
167. E. Badea, L. Miu, P. Budrugeac, M. Giurginca, A. Mašic, N. Badea, and G. Della Gatta Study of deterioration of historical parchments by various thermal analysis techniques complemented by SEM, FTIR, UV-VIS-NIR and unilateral NMR investigations J. Therm. Anal. Calorim. 91 2008 17 27 (Pubitemid 351199215)
168. M. Bardet, G. Gerbaud, L. La Pape, S. Hediger, Q.-K. Trân, and N. Boumlil Nuclear magnetic resonance and electron paramagnetic resonance as analytical tools to investigate the structural features of archaeological leathers Anal. Chem. 81 2009 1505 1511
169. W.D. Armstrong, and L. Singer Composition and constitution of the mineral phase of bone Clin. Orthop. Relat. Res. 38 1965 179 196
170. A.L. Boskey, and A.S. Posner Bone structure, composition and mineralization Orthop. Clin. N. Am. 15 1984 597 612
171. W.E. Brown, and L.C. Chow Chemical properties of bone mineral Ann. Rev. Mater. Sci. 6 1976 213 250
172. R.E.M. Hedges Bone diagenesis: an overview of processes Archaeometry 44 2002 319 328
173. M.I. Kay, R.A. Young, and A.S. Posner Crystal structure of hydroxyapatite Nature 204 1964 1050 1052
174. A.P. Lee, J. Klinowski, and E.A. Marseglia Application of nuclear magnetic resonance spectroscopy to bone diagenesis J. Archeol. Sci. 22 1995 257 262
175. D. Alfano, A.R. Albunia, O. Motta, and A. Proto Detection of diagenetic alterations by spectroscopic on archaeological bones from the Necropolis of Poseidonia (Paestum): a case study J. Cult. Heritage 10 2009 509 513
176. D.N. Notman, J. TashJian, A.C. Aufderheide, O.W. Cass, O.C. Shane, T.H. Berquisit, J.E. Gray, and E. Gedgaudas Modern imaging and endoscopic biopsy techniques in Egyptian mummies AJR 146 1986 93 96 (Pubitemid 16174358)
177. D.H. Shin, I.S. Lee, M.J. Kim, C.S. Oh, J.B. Park, G.D. Bok, and D.S. Yoo Magnetic resonance imaging performed on a hydrated mummy of medieval Korea J. Anatom. 216 2010 329 334
178. F.J. Rhli, H. Von Waldburg, S. Nielles-Vallespin, T. Böni, and P. Speier Clinical magnetic resonance imaging of ancient dry human mummies without rehydration JAMA 298 2007 2618 2620 (Pubitemid 350254967)
179. 23Na nuclear magnetic resonance imaging of ancient Egyptian human mummified tissue Mag. Reson. Imag. 25 2007 1341 1345 (Pubitemid 47625924)
180. J.B. Lambert, Y. Wu, and J.A. Santiago-Blay Taxonomic and chemical relationships revealed by nuclear magnetic resonance spectra of plant exudates J. Nat. Prod. 68 2005 635 648 (Pubitemid 40825268)
181. J.B. Lambert, and J.S. Frye Carbon functionalities in amber Science 217 1982 55 57
182. J.B. Lambert, C.W. Beck, and J.S. Frye Analysis of European amber by carbon-13 nuclear magnetic resonance spectroscopy Archaeometry 30 1988 248 263
183. J.B. Lambert, J.S. Frye, and G.O. Poinar Amber from the Dominican republic: analysis by nuclear magnetic resonance spectroscopy Archaeometry 27 1985 43 51
184. J.B. Lambert, J.S. Frye, T.A. Lee, C.J. Welch, and G.O. Poinar Analysis of Mexican amber by carbon-13 NMR spectroscopy Archaeological Chemistry R. Allen, Advances in Chemistry Ser. 220 vol. IV 1989 American Chemical Society Washington, DC 381 388
185. J.B. Lambert, J.S. Frye, and G.O. Poinar Analysis of North American amber by carbon-13 NMR spectroscopy Geoarchaeology 5 1990 43 52
186. J.B. Lambert, S.C. Johnson, G.O. Poinar, and J.S. Frye Recent and fossil resins from New Zealand and Australia Geoarchaeology 8 1993 141 155
187. J.B. Lambert, S.C. Johnson, and G.O. Poinar Nuclear magnetic resonance characterization of Cretaceous amber Archaeometry 38 1996 325 335 (Pubitemid 126333051)
188. A. Martinez-Richa, R. Vera-Graziano, A. Rivera, and P. Joseph-Nathan A solid-state carbon-13 NMR analysis of ambers Polymer 41 2000 743 750 (Pubitemid 30504267)
189. J.B. Lambert, J.S. Frye, and A. Jurkiewicz The provenance and coal rank of jet by carbon-13 nuclear magnetic resonance spectroscopy Archaeometry 34 1992 121 128
190. J.B. Lambert, E. Graham, M.T. Smith, and J.S. Frye Amber and Jet from Tipu, Belize Ancient Mesoamerica 5 1994 55 60
191. D. Hosler, S.L. Burkett, and M.J. Tarkanian Prehistoric polymers: rubber processing in Ancient Mesoamerica Science 284 1999 1988 1991 (Pubitemid 29309446)
192. J.B. Lambert, J.S. Frye, and G.W. Carriveau The structure of oriental lacquer by solid-state nuclear magnetic resonance spectroscopy Archaeometry 33 1991 87 93
193. J. Kumanotani Laccase-catalyzed polymerization of urushiol in precisely confined Japanese lacquer system Makromol. Chem. 179 1978 47 61
194. G. Stamatakis, U. Knuutinen, K. Laitinen, and A. Spyros Analysis and aging of unsaturated polyester resins in contemporary art installations by NMR spectroscopy Anal. Bioanal. Chem. 398 2010 3203 3214
195. C.W. Beck, C.A. Fellows, and E. MacKennan Nuclear magnetic resonance spectrometry in archaeology Archaeol. Chem. 138 1974 226 235
196. E.L. Ghisalberti, and I. Godfrey The application of nuclear magnetic resonance spectroscopy to the analysis of pitches and resins from marine archaeological sites Bull. Aust. Inst. Marit. Archaeol. 14 1990 1 8
197. 13C NMR spectroscopy Nature 303 1983 238 239 (Pubitemid 13276075)
198. B.L. Sherriff, M.A. Tisdale, B.G. Sayer, H.P. Schwarz, and M. Knif Nuclear magnetic resonance spectroscopic and isotopic analysis of carbonized residues from subarctic Canadian prehistoric pottery Archaeometry 37 1995 95 111
199. 13C CP/MAS NMR spectroscopy of charred and non-charred solid organic residues preserved in roman iron age vessels from The Netherlands Archaeometry 49 2007 571 594 (Pubitemid 47316255)