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Volumn 64-65, Issue , 2012, Pages 40-48

Development of a rapid method for the determination and confirmation of nitroimidazoles in six matrices by fast liquid chromatography-tandem mass spectrometry

Author keywords

Kinetex XB HPLC column; LC MS MS; Nitroimidazoles; Real sample analysis; Strata SDB solid phase extraction

Indexed keywords

1 METHYL 5 NITRO 2 IMIDAZOLEMETHANOL; DIMETRIDAZOLE; METRONIDAZOLE; METRONIDAZOLE HYDROXIDE; NITROIMIDAZOLE DERIVATIVE; RONIDAZOLE; UNCLASSIFIED DRUG;

EID: 84859267973     PISSN: 07317085     EISSN: 1873264X     Source Type: Journal    
DOI: 10.1016/j.jpba.2012.02.013     Document Type: Article
Times cited : (53)

References (33)
  • 1
    • 33645769568 scopus 로고    scopus 로고
    • Analysis of four 5-nitroimidazoles and their corresponding hydroxylated metabolites in egg, processed egg and chicken meat by isotope dilution liquid chromatography-tandem mass spectrometry
    • Mottier P., Huré I., Gremaud E., Guy P.A. Analysis of four 5-nitroimidazoles and their corresponding hydroxylated metabolites in egg, processed egg and chicken meat by isotope dilution liquid chromatography-tandem mass spectrometry. J. Agric. Food Chem. 2006, 54:2018-2026.
    • (2006) J. Agric. Food Chem. , vol.54 , pp. 2018-2026
    • Mottier, P.1    Huré, I.2    Gremaud, E.3    Guy, P.A.4
  • 3
    • 77952236689 scopus 로고    scopus 로고
    • Analytical methodologies for the determination of nitroimidazole residues in biological and environmental liquid samples: a review
    • Mahugo-Santana C., Sosa-Ferrera Z., Torres-Padrón M.E., Santana-Rodríguez J.J. Analytical methodologies for the determination of nitroimidazole residues in biological and environmental liquid samples: a review. Anal. Chim. Acta 2010, 665:113-122.
    • (2010) Anal. Chim. Acta , vol.665 , pp. 113-122
    • Mahugo-Santana, C.1    Sosa-Ferrera, Z.2    Torres-Padrón, M.E.3    Santana-Rodríguez, J.J.4
  • 4
    • 84859270538 scopus 로고    scopus 로고
    • CRL Guidance Paper-CRLs view on state of the art analytical methods for the national residue plans for control of residues, available from the EU CRLs for veterinary drug residue analysis
    • CRL Guidance Paper-CRLs view on state of the art analytical methods for the national residue plans for control of residues, available from the EU CRLs for veterinary drug residue analysis, (2007).
    • (2007)
  • 5
    • 0037663202 scopus 로고    scopus 로고
    • Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLC-MS/MS
    • Matuszewski B.K., Constanzer M.L., Chavez-Eng C.M. Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLC-MS/MS. Anal. Chem. 2003, 75:3019-3030.
    • (2003) Anal. Chem. , vol.75 , pp. 3019-3030
    • Matuszewski, B.K.1    Constanzer, M.L.2    Chavez-Eng, C.M.3
  • 6
    • 77952321609 scopus 로고    scopus 로고
    • Quantification of corticosteroids in bovine urine using selective solid phase extraction and reversed-phase liquid chromatography/tandem mass spectrometry
    • Tölgyesi á., Sharma V.K., Kovacsics L., Fekete J. Quantification of corticosteroids in bovine urine using selective solid phase extraction and reversed-phase liquid chromatography/tandem mass spectrometry. J. Chromatogr. B 2010, 878:1471-1479.
    • (2010) J. Chromatogr. B , vol.878 , pp. 1471-1479
    • Tölgyesi, á.1    Sharma, V.K.2    Kovacsics, L.3    Fekete, J.4
  • 7
    • 77955583437 scopus 로고    scopus 로고
    • Quantitative determination of corticosteroids in bovine milk using mixed-mode polymeric strong cation exchange solid-phase extraction and liquid chromatography-tandem mass spectrometry
    • Tölgyesi á., Tölgyesi L., Sharma V.K., Sohn M., Fekete J. Quantitative determination of corticosteroids in bovine milk using mixed-mode polymeric strong cation exchange solid-phase extraction and liquid chromatography-tandem mass spectrometry. J. Pharm. Biomed. Anal. 2010, 53:919-928.
    • (2010) J. Pharm. Biomed. Anal. , vol.53 , pp. 919-928
    • Tölgyesi, á.1    Tölgyesi, L.2    Sharma, V.K.3    Sohn, M.4    Fekete, J.5
  • 8
    • 79451473780 scopus 로고    scopus 로고
    • Development and validation of a method for determination of corticosteroids in pig fat using liquid chromatography-tandem mass spectrometry
    • Tölgyesi á., Sharma V.K., Fekete J. Development and validation of a method for determination of corticosteroids in pig fat using liquid chromatography-tandem mass spectrometry. J. Chromatogr. B 2011, 879:403-410.
    • (2011) J. Chromatogr. B , vol.879 , pp. 403-410
    • Tölgyesi, á.1    Sharma, V.K.2    Fekete, J.3
  • 9
    • 84859265710 scopus 로고    scopus 로고
    • Analysis of sub μg/kg lincomycin in honey, muscle, milk eggs using fast liquid chromatography-tandem mass spectrometry
    • Tölgyesi á., Fekete J., Fekete Sz., Sharma V.K., Békési K., Tóth E. Analysis of sub μg/kg lincomycin in honey, muscle, milk eggs using fast liquid chromatography-tandem mass spectrometry. J. Chromatogr. Sci. 2012, 50:190-198.
    • (2012) J. Chromatogr. Sci. , vol.50 , pp. 190-198
    • Tölgyesi, á.1    Fekete, J.2    Fekete, S.3    Sharma, V.K.4    Békési, K.5    Tóth, E.6
  • 10
    • 75149175528 scopus 로고    scopus 로고
    • Simultaneous determination of corticosteroids, androgens and progesterone in river water by liquid chromatography-tandem mass spectrometry
    • Tölgyesi á., Verebey Z., Sharma V.K., Kovacsics L., Fekete J. Simultaneous determination of corticosteroids, androgens and progesterone in river water by liquid chromatography-tandem mass spectrometry. Chemosphere 2010, 78:972-979.
    • (2010) Chemosphere , vol.78 , pp. 972-979
    • Tölgyesi, á.1    Verebey, Z.2    Sharma, V.K.3    Kovacsics, L.4    Fekete, J.5
  • 11
    • 0343092020 scopus 로고    scopus 로고
    • Determination of four nitroimidazole residues in poultry meat by liquid chromatography-mass spectrometry
    • Hurtaud-Pessel D., Delépine B., Laurentie M. Determination of four nitroimidazole residues in poultry meat by liquid chromatography-mass spectrometry. J. Chromatogr. A 2000, 882:89-98.
    • (2000) J. Chromatogr. A , vol.882 , pp. 89-98
    • Hurtaud-Pessel, D.1    Delépine, B.2    Laurentie, M.3
  • 12
    • 33846903885 scopus 로고    scopus 로고
    • Confirmation of four nitroimidazoles in porcine liver by liquid chromatography-tandem mass spectrometry
    • Xia X., Li X., Zhang S., Ding S., Jiang H., Shen J. Confirmation of four nitroimidazoles in porcine liver by liquid chromatography-tandem mass spectrometry. Anal. Chim. Acta 2007, 586:394-398.
    • (2007) Anal. Chim. Acta , vol.586 , pp. 394-398
    • Xia, X.1    Li, X.2    Zhang, S.3    Ding, S.4    Jiang, H.5    Shen, J.6
  • 13
    • 77952238226 scopus 로고    scopus 로고
    • Multiresidue method for the determination of nitroimidazoles and their hydroxy-metabolites in poultry muscle, plasma and egg by isotope dilution liquid chromatography-mass spectrometry
    • Mitrowska K., Posyniak A., Zmudzki J. Multiresidue method for the determination of nitroimidazoles and their hydroxy-metabolites in poultry muscle, plasma and egg by isotope dilution liquid chromatography-mass spectrometry. Talanta 2010, 81:1273-1280.
    • (2010) Talanta , vol.81 , pp. 1273-1280
    • Mitrowska, K.1    Posyniak, A.2    Zmudzki, J.3
  • 14
    • 33846913962 scopus 로고    scopus 로고
    • Validation of a method for the detection and confirmation of nitroimidazoles and the corresponding hydroxy metabolites in pig plasma by high performance liquid chromatography-tandem mass spectrometry
    • Fraselle S., Derop V., Degroodt J.-M., Van Loco J. Validation of a method for the detection and confirmation of nitroimidazoles and the corresponding hydroxy metabolites in pig plasma by high performance liquid chromatography-tandem mass spectrometry. Anal. Chim. Acta 2007, 586:383-393.
    • (2007) Anal. Chim. Acta , vol.586 , pp. 383-393
    • Fraselle, S.1    Derop, V.2    Degroodt, J.-M.3    Van Loco, J.4
  • 15
    • 65349168316 scopus 로고    scopus 로고
    • Development and validation of a rapid method for the determination and confirmation of 10 nitroimidazoles in animal plasma using liquid chromatography tandem mass spectrometry
    • Cronly M., Behan P., Foley B., Malone E., Regan L. Development and validation of a rapid method for the determination and confirmation of 10 nitroimidazoles in animal plasma using liquid chromatography tandem mass spectrometry. J. Chromatogr. B 2009, 877:1494-1500.
    • (2009) J. Chromatogr. B , vol.877 , pp. 1494-1500
    • Cronly, M.1    Behan, P.2    Foley, B.3    Malone, E.4    Regan, L.5
  • 16
    • 53049099867 scopus 로고    scopus 로고
    • Simultaneous determination of 5-nitroimidazoles and nitrofurans in pork by high-performance liquid chromatography-tandem mass spectrometry
    • Xia X., Li X., Zhang S., Ding S., Jiang H., Li J., Shen J. Simultaneous determination of 5-nitroimidazoles and nitrofurans in pork by high-performance liquid chromatography-tandem mass spectrometry. J. Chromatogr. A 2008, 1208:101-108.
    • (2008) J. Chromatogr. A , vol.1208 , pp. 101-108
    • Xia, X.1    Li, X.2    Zhang, S.3    Ding, S.4    Jiang, H.5    Li, J.6    Shen, J.7
  • 17
    • 57749114361 scopus 로고    scopus 로고
    • Validation of a liquid chromatography-tandem mass spectrometry method for the identification and quantification of 5-nitroimidazole drugs and their corresponding hydroxy metabolites in lyophilised pork meat
    • Zeleny R., Harbeck S., Schimmel H. Validation of a liquid chromatography-tandem mass spectrometry method for the identification and quantification of 5-nitroimidazole drugs and their corresponding hydroxy metabolites in lyophilised pork meat. J. Chromatogr. A 2009, 1216:249-256.
    • (2009) J. Chromatogr. A , vol.1216 , pp. 249-256
    • Zeleny, R.1    Harbeck, S.2    Schimmel, H.3
  • 18
    • 70350180948 scopus 로고    scopus 로고
    • Rapid confirmatory method for the determination of 11 nitroimidazoles in egg using liquid chromatography tandem mass spectrometry
    • Cronly M., Behan P., Foley B., Malone E., Regan L. Rapid confirmatory method for the determination of 11 nitroimidazoles in egg using liquid chromatography tandem mass spectrometry. J. Chromatogr. A 2009, 1216:8101-8109.
    • (2009) J. Chromatogr. A , vol.1216 , pp. 8101-8109
    • Cronly, M.1    Behan, P.2    Foley, B.3    Malone, E.4    Regan, L.5
  • 19
    • 45549103013 scopus 로고    scopus 로고
    • Use of molecularly imprinted solid-phase extraction sorbent for the determination of four 5-nitroimidazoles and three of their metabolites from egg-based samples before tandem LC-ESIMS/MS analysis
    • Mohamed R., Mottier P., Treguier L., Richoz-Payot J., Yilmaz E., Tabet J.-C., Guy P.A. Use of molecularly imprinted solid-phase extraction sorbent for the determination of four 5-nitroimidazoles and three of their metabolites from egg-based samples before tandem LC-ESIMS/MS analysis. J. Agric. Food Chem. 2008, 56:3500-3508.
    • (2008) J. Agric. Food Chem. , vol.56 , pp. 3500-3508
    • Mohamed, R.1    Mottier, P.2    Treguier, L.3    Richoz-Payot, J.4    Yilmaz, E.5    Tabet, J.-C.6    Guy, P.A.7
  • 20
    • 0037466642 scopus 로고    scopus 로고
    • Performance of a matrix-comprehensive in-house validation study by means of an especially designed software
    • Uhlig S., Gowik P., Radeck W. Performance of a matrix-comprehensive in-house validation study by means of an especially designed software. Anal. Chim. Acta 2003, 483:351-362.
    • (2003) Anal. Chim. Acta , vol.483 , pp. 351-362
    • Uhlig, S.1    Gowik, P.2    Radeck, W.3
  • 21
    • 61849160530 scopus 로고    scopus 로고
    • In-house validation and factorial effect analysis of a liquid chromatography-tandem mass spectrometry method for the determination of steroids in bovine muscle
    • Schmidt K.S., Stachel C.S., Gowik P. In-house validation and factorial effect analysis of a liquid chromatography-tandem mass spectrometry method for the determination of steroids in bovine muscle. Anal. Chim. Acta 2009, 637:156-164.
    • (2009) Anal. Chim. Acta , vol.637 , pp. 156-164
    • Schmidt, K.S.1    Stachel, C.S.2    Gowik, P.3
  • 22
    • 75949096893 scopus 로고    scopus 로고
    • Performance of columns packed with the new shell Kinetex-C18 particles in gradient elution chromatography
    • Gritti F., Guiochon G. Performance of columns packed with the new shell Kinetex-C18 particles in gradient elution chromatography. J. Chromatogr. A 2010, 1217:1604-1615.
    • (2010) J. Chromatogr. A , vol.1217 , pp. 1604-1615
    • Gritti, F.1    Guiochon, G.2
  • 23
    • 79959376166 scopus 로고    scopus 로고
    • Comparison of LC columns packed with 2.6μm core-shell and sub-2μm porous particles for gradient separation of antibiotics
    • Tylová T., Kameník Z., Flieger M., Olšovská J. Comparison of LC columns packed with 2.6μm core-shell and sub-2μm porous particles for gradient separation of antibiotics. Chromatographia 2011, 74:19-27.
    • (2011) Chromatographia , vol.74 , pp. 19-27
    • Tylová, T.1    Kameník, Z.2    Flieger, M.3    Olšovská, J.4
  • 24
    • 77952672825 scopus 로고    scopus 로고
    • Comparative study of new shell-type, sub-2μm fully porous and monolith stationary phases, focusing on mass-transfer resistance
    • Oláh E., Sz Fekete, Fekete J., Ganzler K. Comparative study of new shell-type, sub-2μm fully porous and monolith stationary phases, focusing on mass-transfer resistance. J. Chromatogr. A 2010, 1217:3642-3653.
    • (2010) J. Chromatogr. A , vol.1217 , pp. 3642-3653
    • Oláh, E.1    Sz Fekete2    Fekete, J.3    Ganzler, K.4
  • 25
    • 78149495855 scopus 로고    scopus 로고
    • Efficiency of the new sub-2μm core-shell (Kinetex™) column in practice, applied for small and large molecule separation
    • Sz.Fekete, Ganzler K., Fekete J. Efficiency of the new sub-2μm core-shell (Kinetex™) column in practice, applied for small and large molecule separation. J. Pharm. Biomed. Anal. 2011, 54:482-490.
    • (2011) J. Pharm. Biomed. Anal. , vol.54 , pp. 482-490
    • Sz.Fekete1    Ganzler, K.2    Fekete, J.3
  • 26
    • 84859269467 scopus 로고    scopus 로고
    • Optimizing the agilent multimode source.
    • S. Fischer, W. Duncan, Optimizing the agilent multimode source. http://www.chem.agilent.com/Library/technicaloverviews/Public/5989-6463EN.pdf.
    • Fischer, S.1    Duncan, W.2
  • 27
    • 80053336977 scopus 로고    scopus 로고
    • Determination of propylenethiourea, the main metabolite of propineb, in tomato by HILIC-MS
    • Tölgyesi L., Kele P., Torkos K. Determination of propylenethiourea, the main metabolite of propineb, in tomato by HILIC-MS. Chromatographia 2010, 71:75-80.
    • (2010) Chromatographia , vol.71 , pp. 75-80
    • Tölgyesi, L.1    Kele, P.2    Torkos, K.3
  • 28
    • 84859265842 scopus 로고    scopus 로고
    • Commission Decision 2002/657/EC, Off. J. Eur. Commun. L221/8.
    • Commission Decision 2002/657/EC, Off. J. Eur. Commun. (2002) L221/8.
    • (2002)
  • 29
    • 84859269468 scopus 로고    scopus 로고
    • Validation of analytical methods: review and strategy, LC-GC international
    • Validation of analytical methods: review and strategy, LC-GC international (1998).
    • (1998)
  • 30
    • 58549085748 scopus 로고    scopus 로고
    • Development of a certified reference material for the content of nitroimidazole parent drugs and hydroxy metabolites in pork meat
    • Zeleny R., Schimmel H., Ulberth F., Emons H. Development of a certified reference material for the content of nitroimidazole parent drugs and hydroxy metabolites in pork meat. Anal. Chim. Acta 2009, 634:237-242.
    • (2009) Anal. Chim. Acta , vol.634 , pp. 237-242
    • Zeleny, R.1    Schimmel, H.2    Ulberth, F.3    Emons, H.4
  • 31
    • 84859267020 scopus 로고    scopus 로고
    • IUPAC Compendium of Chemical Terminology-the Gold Book
    • IUPAC Compendium of Chemical Terminology-the Gold Book (2005-2009) . http://goldbook.iupac.org/I03108.html.
    • (2005)
  • 32
    • 79954569838 scopus 로고    scopus 로고
    • On the use of Kinetex(™) -C(18) core-shell 2.6μm stationary phase to the multiclass determination of antibiotics
    • Samanidou V.F., Karageorgou E.G. On the use of Kinetex(™) -C(18) core-shell 2.6μm stationary phase to the multiclass determination of antibiotics. Drug Test. Anal. 2011, 3:234-244.
    • (2011) Drug Test. Anal. , vol.3 , pp. 234-244
    • Samanidou, V.F.1    Karageorgou, E.G.2
  • 33
    • 84857054589 scopus 로고    scopus 로고
    • Fast liquid chromatography: the domination of core-shell and very fine particles
    • Fekete Sz., Oláh E., Fekete J. Fast liquid chromatography: the domination of core-shell and very fine particles. J. Chromatogr. A 2011, 1228:57-71.
    • (2011) J. Chromatogr. A , vol.1228 , pp. 57-71
    • Fekete, S.1    Oláh, E.2    Fekete, J.3


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