Development and validation of a method for determination of corticosteroids in pig fat using liquid chromatography-tandem mass spectrometry

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 879, Issue 5-6, 2011, Pages 403-410

  Tölgyesi, Ádám ^a,c   Sharma, Virender K ^b   Fekete, Jeno ^c  

^a CENTRAL VETERINARY INSTITUTE   (Hungary)

^b Florida Institute of Technology   (United States)

^c BUDAPEST UNIVERSITY OF TECHNOLOGY AND ECONOMICS   (Hungary)

Author keywords

Corticosteroid; Fat; Liquid chromatography tandem mass spectrometry; Optimization; Validation

Indexed keywords

ACETATE BUFFERS; ANALYSIS TIME; BANNED SUBSTANCES; CONVENTIONAL TECHNIQUES; CORTICOSTEROID; DECISION LIMIT; DETECTION CAPABILITY; DEXAMETHASONES; EU DIRECTIVES; EUROPEAN UNION COMMISSIONS; FAT; FUSED-CORE; ION SUPPRESSION; ISOCRATIC; LC-MS/MS; LIMIT OF DETECTION; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; LIQUID-LIQUID EXTRACTION; MEASURED PARAMETERS; METHANOL-WATER; N-HEXANE; NON-POLAR; PREDNISOLONE; REPRODUCIBILITIES; SAMPLE CLEAN-UP; SAMPLE PREPARATION; SOLID-PHASE EXTRACTION; TIME SIGNALS; VALIDATION;

CHROMATOGRAPHY; DRUG PRODUCTS; HEXANE; HIGH PRESSURE LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; METHANOL; OPTIMIZATION; ORGANIC SOLVENTS; RECOVERY; SIGNAL TO NOISE RATIO;

SOLVENT EXTRACTION;

DEXAMETHASONE; FAT; FLUMETASONE; HEXANE; MEPREDNISONE; METHYLPREDNISOLONE; PREDNISOLONE;

ARTICLE; DRUG DETERMINATION; DRUG STRUCTURE; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; NONHUMAN; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; SWINE; TANDEM MASS SPECTROMETRY;

ADIPOSE TISSUE; ADRENAL CORTEX HORMONES; ANIMALS; CHROMATOGRAPHY, LIQUID; DRUG RESIDUES; LINEAR MODELS; MEAT; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; SWINE; TANDEM MASS SPECTROMETRY;

SUIDAE;

EID: 79451473780     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2010.12.027     Document Type: Article

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