In situ derivatization-liquid liquid extraction as a sample preparation strategy for the determination of urinary biomarker prolyl-4-hydroxyproline by liquid chromatography-tandem mass spectrometry

Journal of Mass Spectrometry

Volumn 47, Issue 3, 2012, Pages 294-302

  Cimlová, Jana ^a,b   Kružberská, Pavla ^a   Švagera, Zdeněk ^c   Hušek, Petr ^a,c   Šimek, Petr ^a  

^a INSTITUTE OF MATHEMATICS   (Czech Republic)

^b INSTITUTE OF CHEMICAL TECHNOLOGY   (Czech Republic)

^c Institute of Clinical   (Czech Republic)

Author keywords

alkyl chloroformate derivatization; LC MS MS; liquid liquid extraction; prolyl 4 hydroxyproline; urine

Indexed keywords

DERIVATIZATIONS; LC-MS/MS; LIQUID LIQUID EXTRACTION; PROLYL-4-HYDROXYPROLINE; URINE;

BODY FLUIDS; FUNCTIONAL GROUPS; GAS CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; REACTION PRODUCTS; SOLVENT EXTRACTION;

LIQUIDS;

CHLOROFORM; HYDROXYPROLINE; ISOBUTANOL; LEVO PROLYL 4 LEVO HYDROXYPROLINE; PYRIDINE; UNCLASSIFIED DRUG;

AQUEOUS SOLUTION; ARTICLE; CATALYSIS; CHEMICAL STRUCTURE; DERIVATIZATION; DOWNSTREAM PROCESSING; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; LIQUID CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; PRIORITY JOURNAL; TANDEM MASS SPECTROMETRY; URINALYSIS;

BIOLOGICAL MARKERS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DIPEPTIDES; DRUG STABILITY; HUMANS; LINEAR MODELS; LIQUID-LIQUID EXTRACTION; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY;

EID: 84859050849     PISSN: 10765174     EISSN: 10969888     Source Type: Journal    
DOI: 10.1002/jms.2952     Document Type: Article

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