Implementation of a design of experiments to study the influence of the background electrolyte on separation and detection in non-aqueous capillary electrophoresis-mass spectrometry

Electrophoresis

Volumn 33, Issue 4, 2012, Pages 583-598

  Posch, Tjorben Nils ^a   Müller, Alexander ^b   Schulz, Wolfgang ^b   Pütz, Michael ^c   Huhn, Carolin ^a  

^a FORSCHUNGSZENTRUM JÜLICH   (Germany)

^b Laboratory for Operation Control and Research   (Germany)

^c KT 34 Toxicology   (Germany)

Author keywords

Design of experiments; Heteroconjugation; Indole alkaloids; Ion pairing; Non aqueous capillary electrophoresis

Indexed keywords

ALKALOIDS; CAPILLARY ELECTROPHORESIS; DESIGN OF EXPERIMENTS; ELECTROOSMOSIS; MASS SPECTROMETRY; METABOLITES; PLANT EXTRACTS; POLYCYCLIC AROMATIC HYDROCARBONS; SALTS;

AMMONIUM SALT; BACKGROUND ELECTROLYTES; CAPILLARY ELECTROPHORESIS-MASS SPECTROMETRIES; GLACIAL ACETIC ACID; HETEROCONJUGATION; INDOLE ALKALOIDS; ION-PAIRING; LOW DIELECTRIC CONSTANTS; NON-AQUEOUS CAPILLARY ELECTROPHORESIS; OPTIMISATIONS;

ELECTROLYTES;

7 HYDROXY MITRACILIATINE; ACETIC ACID; AMMONIUM FORMATE; ELECTROLYTE; HARMOL; INDOLE; ISOPAYNANTHEINE; MITRACILIATINE; MITRAGYNINE; PAYNANTHEINE; SPECIOCILLIATINE; SPECIOGYNINE; TETRAHYDROHARMINE; UNCLASSIFIED DRUG;

AQUEOUS CAPILLARY ELECTROPHORESIS; ARTICLE; CAPILLARY ELECTROPHORESIS; CONTROLLED STUDY; DIELECTRIC CONSTANT; ELECTROOSMOSIS; INTERMETHOD COMPARISON; MASS SPECTROMETRY; MITRAGYNA; NONAQUEOUS CAPILLARY ELECTROPHORESIS; PHASE SEPARATION; PROCESS OPTIMIZATION;

EID: 84858970914     PISSN: 01730835     EISSN: 15222683     Source Type: Journal    
DOI: 10.1002/elps.201100381     Document Type: Article

References (67)

1. Takayama, H., Chem. Pharm. Bull. 2004, 52, 916-928.
2. Porras, S. P., Valkó, I. E., Jyske, P., Riekkola, M.-L., J. Biochem. Biophys. Methods 1999, 38, 89-102.
3. Cherkaoui, S., Veuthey, J.-L., Analusis 1999, 27, 765-771.
4. Porras, S. P., Riekkola, M.-L., Kenndler, E., Chromatographia 2001, 53, 290-294.
5. Bjørnsdottir, I., Hansen, S. H., J. Pharm. Biomed. Anal. 1995, 13, 1473-1481.
6. Chiu, C.-W., Liang, H.-H., Huang, H.-Y., Electrophoresis 2007, 28, 4220-4226.
7. Sturm, S., Seger, C., Stuppner, H., J. Chromatogr. A 2007, 1159, 42-50.
8. Walbroehl, Y., Jorgenson, J. W., J. Chromatogr. A 1984, 315, 135-143.
9. Scriba, G. K. E., J. Chromatogr. A 2007, 1159, 28-41.
10. Kenndler, E., Electrophoresis 2009, 30, S101-S111.
11. Cherkaoui, S., Varesio, E., Christen, P., Veuthey, J.-L., Electrophoresis 1998, 19, 2900-2906.
12. Bjørnsdottir, I., Hansen, S. H., J. Biochem. Biophys. Methods 1999, 38, 155-161.
13. Cherkaoui, S., Rudaz, S., Veuthey, J.-L., Electrophoresis 2001, 22, 491-496.
14. Bjørnsdottir, I., Hansen, S. H., J. Chromatogr. A 1995, 711, 313-322.
15. Marsh, A., Clark, B. J., Altria, K. D., Electrophoresis 2004, 25, 1270-1278.
16. Tomlinson, A. J., Benson, L. M., Gorrod, J. W., Naylor, S., J. Chromatogr. B 1994, 657, 373-381.
17. Tomlinson, A. J., Benson, L. M., Naylor, S., LC-GC Int. 1995, 8, 210-216.
18. Tomlinson, A. J., Benson, L. M., Johnson, K. L., Naylor, S., Electrophoresis 1994, 15, 62-71.
19. Tomlinson, A. J., Benson, L. M., Braddock, W. D., Oda, R. P., Naylor, S., J. High Resolut. Chromatogr. 1994, 17, 729-731.
20. Barthe, L., Ribet, J.-P., Pelissou, M., Degude, M.-J., Fahy, J., Duflos, A., J. Chromatogr. A 2002, 968, 241-250.
21. Geiser, L., Cherkaoui, S., Veuthey, J.-L., J. Chromatogr. A 2002, 979, 389-398.
22. Drange, E., Lundanes, E., J. Chromatogr. A 1997, 771, 301-309.
23. Zarbl, E., Lämmerhofer, M., Franco, P., Petracs, M., Lindner, W., Electrophoresis 2001, 22, 3297-3307.
24. Karbaum, A., Jira, T., Electrophoresis 1999, 20, 3396-3401.
25. Vaher, M., Koel, M., Kaljurand, M., J. Chromatogr. A 2002, 979, 27-32.
26. Carabias-Martínez, R., Rodríguez-Gonzalo, E., Hernández-Méndez, J., Cruz, E. M., Domínguez-Álvarez, J., Electrophoresis 2006, 27, 423-432.
27. Descroix, S., Varenne, A., Geiser, L., Cherkaoui, S., Veuthey, J.-L., Gareil, P., Electrophoresis 2003, 24, 1577-1586.
28. Porras, S. P., Riekkola, M.-L., Kenndler, E., J. Chromatogr. A 2001, 924, 31-42.
29. Servais, A.-C., Fillet, M., Chiap, P., Abushoffa, A. M., Hubert, P., Crommen, J., J. Sep. Sci. 2002, 25, 1087-1095.
30. Porras, S. P., Jyske, P., Riekkola, M.-L., Kenndler, E., J. Microcolumn Sep. 2001, 13, 149-155.
31. Bjørnsdottir, I., HonoréHansen, S., Terabe, S., J. Chromatogr. A 1996, 745, 37-44.
32. Lämmerhofer, M., Zarbl, E., Lindner, W., J. Chromatogr. A 2000, 892, 509-521.
33. Porras, S. P., Kenndler, E., Electrophoresis 2005, 26, 3279-3291.
34. Porras, S. P., Jussila, M., Electrophoresis 2007, 28, 3590-3599.
35. Okada, T., J. Chromatogr. A 1997, 771, 275-284.
36. Sarmini, K., Kenndler, E., J. Biochem. Biophys. Methods 1999, 38, 123-137.
37. Cantu, M. D., Hillebrand, S., Carrilho, E., J. Chromatogr. A 2005, 1068, 99-105.
38. Huhn, C., Neusüß, C., Pelzing, M., Pyell, U., Mannhardt, J., Pütz, M., Electrophoresis 2005, 26, 1389-1397.
39. Haynes, W. M. (Ed.), CRC Handbook of Chemistry & Physics, Internet Edition, Taylor and Francis Group, Boca Raton, Florida 2011.
40. Anurukvorakun, O., Suntornsuk, W., Suntornsuk, L., J. Chromatogr. A 2006, 1134, 326-332.
41. Cherkaoui, S., Mateus, L., Christen, P., Veuthey, J.-L., J. Pharm. Biomed. Anal. 1999, 21, 165-174.
42. Müller, A., Flottmann, D., Schulz, W., Seitz, W., Weber, W. H., Anal. Bioanal. Chem 2008, 390, 1317-1326.
43. Müller, A., Flottmann, D., Schulz, W., Seitz, W., Weber, W., Clean 2007, 35, 329-338.
44. Pütz, M., Huhn, C., Dahlenburg, R., Pyell, U., Beiträge zum XIII. GTFCh-Symposium 2003, 1, 275-282.
45. Hagberg, J., J. Chromatogr. A 2003, 988, 127-133.
46. Varesio, E., Cherkaoui, S., Veuthey, J. L., J. High Resolut. Chromatogr. 1998, 21, 653-657.
47. Sanz-Nebot, V., Benavente, F., Balaguer, E., Barbosa, J., Electrophoresis 2003, 24, 883-891.
48. Staub, A., Giraud, S., Saugy, M., Rudaz, S., Veuthey, J.-L., Schappler, J., Electrophoresis 2010, 31, 388-395.
49. Geiser, L., Cherkaoui, S., Veuthey, J.-L., J. Chromatogr. A 2000, 895, 111-121.
50. Carrasco-Pancorbo, A., Arráez-Román, D., Segura-Carretero, A., Fernández-Gutiérrez, A., Electrophoresis 2006, 27, 2182-2196.
51. Balaguer, E., Neusüß, C., Anal. Chem. 2006, 78, 5384-5393.
52. Dolník, V., J. Chromatogr. A 1996, 744, 115-121.
53. Leinweber, F. C., Otto, M., J. Chromatogr. A 1999, 848, 347-363.
54. Chen, J., Zhao, H., Wang, X., Lee, F. S.-C., Yang, H., Zheng, L., Electrophoresis 2008, 29, 2135-2147.
55. Peri-Okonny, U. L., Kenndler, E., Stubbs, R. J., Guzman, N. A., Electrophoresis 2003, 24, 139-150.
56. Soga, T., Ueno, Y., Naraoka, H., Matsuda, K., Tomita, M., Nishioka, T., Anal. Chem. 2002, 74, 6224-6229.
57. Ruiz-Calero, V., Moyano, E., Puignou, L., Galceran, M. T., J. Chromatogr. A 2001, 914, 277-291.
58. Peters, F. T., Hartung, M., Herbold, M., Schmitt, G., Daldrup, T., Mußhoff, F., Richtlinie der GTFCh zur Qualitätssicherung bei forensisch-toxikologischen Untersuchungen 2009, 01, 1-24.
59. Nilsson, S. L., Bylund, D., Jörntén-Karlsson, M., Petersson, P., Markides, K. E., Electrophoresis 2004, 25, 2100-2107.
60. Rafati, A. A., Bagheri, A., Najafi, M., J. Chem. Eng. Data 2010, 55, 4039-4043.
61. Riekkola, M.-L., Jussila, M., Porras, S. P., Valko, I. E., J. Chromatogr. A 2000, 892, 155-170.
62. Huhn, C., Pyell, U., J. Chromatogr. A 2010, 1217, 4476-4486.
63. Haselberg, R., Ratnayake, C. K., de Jong, G. J., Somsen, G. W., J. Chromatogr. A 2010, 1217, 7605-7611.
64. Douglas, K. T., Sharma, R. K., Walmsley, J. F., Hider, R. C., Mol. Pharmacol. 1983, 23, 614-618.
65. Popovych, O., Tomkins, R. P. T., Nonaqueous Solution Chemistry, R. E. Krieger, New York 1981.
66. Bowser, M. T., Kranack, A. R., Chen, D. D. Y., TrAC, Trends Anal. Chem. 1998, 17, 424-434.
67. Carabias-Martínez, R., Rodríguez-Gonzalo, E., Hernández-Méndez, J., Cruz, E. M., Domínguez-Álvarez, J., Electrophoresis 2006, 27, 423-432.