Derivatization of the tricarboxylic acid cycle intermediates and analysis by online solid-phase extraction-liquid chromatography-mass spectrometry with positive-ion electrospray ionization

Journal of Chromatography A

Volumn 1232, Issue , 2012, Pages 19-26

  Kloos, D ^a,b   Derks, R J E ^b   Wijtmans, M ^a   Lingeman, H ^a   Mayboroda, O A ^b   Deelder, A M ^b   Niessen, W M A ^a   Giera, M ^a,b  

^a VU UNIVERSITY AMSTERDAM   (Netherlands)

^b LEIDEN UNIVERSITY MEDICAL CENTER   (Netherlands)

Author keywords

Carboxylic acids; Derivatization; LC MS; N methyl 2 phenylethanamine; TCA cycle

Indexed keywords

AEROBIC CELLS; ANALYTES; CARBODIIMIDES; CELL SIGNALING; CELLULAR METABOLIC PROCESS; CELLULAR METABOLITES; CHROMATOGRAPHY-MASS SPECTROMETRY; CORE-SHELL; DERIVATIZATION REAGENT; DERIVATIZATIONS; DETECTION LIMITS; ELECTROSPRAY IONIZATION MASS SPECTROMETRY; ENERGY REGULATION; HEART TISSUES; KEY FACTORS; LC-MS; METABOLIC STATE; N-METHYL-2-PHENYLETHANAMINE; ON-LINE SOLID PHASE EXTRACTION; ORDERS OF MAGNITUDE; RAPID ANALYSIS; REVERSED-PHASE LIQUID CHROMATOGRAPHY; SAMPLE MATRIX; SILICA COLUMN; SOLID-PHASE; TCA CYCLE; TRICARBOXYLIC ACID CYCLE; TRICARBOXYLIC ACIDS;

CARBOXYLIC ACIDS; ELECTROSPRAY IONIZATION; ENERGY POLICY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLISM; PHASE SEPARATION; SILICA; TISSUE;

POSITIVE IONS;

DICARBOXYLIC ACID; ETHYLAMINE; N METHYL 2 PHENYLETHANAMINE; TRICARBOXYLIC ACID; UNCLASSIFIED DRUG;

ANIMAL TISSUE; ARTICLE; CITRIC ACID CYCLE; CONTROLLED STUDY; DERIVATIZATION; IONIZATION; LIMIT OF DETECTION; MASS SPECTROMETRY; NONHUMAN; ONLINE ANALYSIS; ONLINE SYSTEM; POSITIVE ION ELECTROSPRAY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; REVERSED PHASE LIQUID CHROMATOGRAPHY; SOLID PHASE EXTRACTION; SWINE;

ANIMALS; CARBODIIMIDES; CARBON ISOTOPES; CARBOXYLIC ACIDS; CHROMATOGRAPHY, REVERSE-PHASE; CITRIC ACID CYCLE; CRICETINAE; KINETICS; LIMIT OF DETECTION; METHAMPHETAMINE; MYOCARDIUM; REPRODUCIBILITY OF RESULTS; SOLID PHASE EXTRACTION; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; SWINE; TANDEM MASS SPECTROMETRY; TEMPERATURE; TISSUE EXTRACTS;

SUIDAE;

EID: 84858075075     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.07.095     Document Type: Article

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