Determination of chemical warfare agents and related compounds in environmental samples by solid-phase microextraction with gas chromatography

Journal of Chromatography A

Volumn 1218, Issue 47, 2011, Pages 8457-8479

  Popiel, Stanisław ^a   Sankowska, Monika ^a  

^a MILITARY UNIVERSITY OF TECHNOLOGY   (Poland)

Author keywords

Chemical warfare agents; Derivatization; Gas chromatography analysis; Review; Solid phase microextraction

Indexed keywords

ANALYTES; CHEMICAL DEFENSE; CHEMICAL WARFARE AGENTS; CONTAMINATED AREAS; DEGRADATION PRODUCTS; DERIVATIZATION METHOD; DERIVATIZATIONS; DETECTION SYSTEM; ENVIRONMENTAL ANALYSIS; ENVIRONMENTAL SAMPLE; FIBER COATINGS; FIELD SAMPLING; GAS CHROMATOGRAPHY ANALYSIS; HEADSPACE ANALYSIS; HEADSPACES; LIQUID-LIQUID EXTRACTION; LOW DETECTION LIMIT; MATRIX; QUALITATIVE AND QUANTITATIVE ANALYSIS; RELATED COMPOUNDS; SAMPLE PREPARATION TECHNIQUES; SOLID PHASE MICROEXTRACTION; SOLID-PHASE EXTRACTION; TOXIC CHEMICALS; TOXIC INDUSTRIAL COMPOUNDS; WATER AND SOIL SAMPLES;

CHEMICAL COMPOUNDS; CHEMICAL WARFARE; CHROMATOGRAPHIC ANALYSIS; DEGRADATION; DETECTORS; GROUNDWATER POLLUTION; INDUSTRIAL CHEMICALS; LIQUIDS; MASS SPECTROMETRY; QUALITY CONTROL; SOILS; SOLVENT EXTRACTION; TOXIC MATERIALS;

GAS CHROMATOGRAPHY;

2 CHLOROBENZYLIDENEMALONONITRILE; ALKYLPHOSPHONIC ACID ESTER; BLISTER AGENT; BLOOD AGENT; CENTRAL DEPRESSANT AGENT; CHEMICAL WARFARE AGENT; CHLORINE; CHLOROPICRIN; CHOKING AGENT; CYANOGEN CHLORIDE; DICHLOROARSINE; DIPHOSGENE; HYDROGEN CYANIDE; INCAPACITATING AGENT; LEWISITE; MUSTARD GAS; NERVE AGENT; NITROMETHANE; PHOSGENE; PSYCHEDELIC AGENT; QUINUCLIDINYL BENZILATE; SARIN; SODIUM CHLORIDE; SOMAN; TABUN; UNCLASSIFIED DRUG; URTICANT;

CHEMICAL ANALYSIS; DECOMPOSITION; ECOTOXICOLOGY; ENVIRONMENTAL EXPOSURE; ENVIRONMENTAL MONITORING; GAS CHROMATOGRAPHY; HEADSPACE SOLID PHASE MICROEXTRACTION; HUMAN; LIMIT OF DETECTION; MASS FRAGMENTOGRAPHY; MASS SPECTROMETRY; MATERIAL COATING; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION; REVIEW; SKIN DISEASE; SOLID PHASE MICROEXTRACTION; TEMPERATURE; TIME;

AIR; CHEMICAL WARFARE AGENTS; CHROMATOGRAPHY, GAS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; SOIL; SOLID PHASE MICROEXTRACTION; WATER;

EID: 80054984939     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.09.066     Document Type: Review

References (118)

1. Convention on the Prohibition of the Development, Production, Stockpiling and Use of Chemical Weapons and on their Destrution, Technical Secretariat of the Organisation for Prohibition of Chemical Weapons, The Hague, 1997 http://www.opcw.nl/.
2. Recommended Operating Procedures for Sampling and Analysis in the Verification of Chemical Disarmament 1994, The Ministry for Foreign Affairs of Finland, Helsinki. M. Rautio (Ed.).
3. Organisation for the Prohibition of Chemical Weapons (OPCW), 1997 http://www.opcw.org/.
4. Zenkevich I.G. Experimentally Measured Retention Indices 2005.
5. Staples E.J. Creating a Compound Library for Chemical Warfare Agents for the Znose 2006.
6. Yang Y.-C., Baker J.A., Ward J.R. Chem. Rev. 1992, 92:1729.
7. Franke S. Lehrbuch der Militärchemie Band 1 1977, Militärverlag der DDR, Berlin.
8. Edwadrs P., Maynard R.L. Chemical Warfare Agents Toxicology and Treatment 2007, 684. Wiley and Sons, Chichester, England. T.C. Marrs, R.L. Maynard, F.R. Sidel (Eds.).
9. Vocci F.J., Yevich T.A., Punte C.L. Toxicol. Appl. Pharmacol. 1963, 5:677.
10. http://www.chemspider.com/.
11. J.A. Cogliano, G.L. Braude, Corrosion, Compatibility, and other Physicochemical Studiem (U), Final Report-Task II, DA 18-108-CML-6602, W.R. Grace and Company, Washington Research Center, Clarksville, MD, UNCLASSIFIED Report (AD359603), 1963.
12. Munro N.B., Talmage S.S., Griffin G.D., Waters L.C., Watson A.P., King J.F., Hauschild V. Environ. Health Perspect. 1999, 107:933.
13. Talmage S.S., Munro N.B., Watson A.P., King J.F., Hauschild V. Chemical Warfare Agents Toxicology and Treatment 2007, 89. Wiley and Sons, Chichester, England. T.C. Marrs, R.L. Maynard, F.R. Sidel (Eds.).
14. H.T. Bausum, G. Reddy, G.J. Leach, Sugested interim estimates of the reference dose (RfD) and reference concetration (RfC) for certain key breakdown products of chemical agents, Report to the USCHPPM Chemical Standards Working Group, US Army Center for Health Promotion and Preventive Medicine, MD, December 10, 1998.
15. Reddy G., Major A.A., Leach G.J. Int. J. Toxicol. 2005, 24:435.
16. D'Agostino P.A. Forensic Science Handbook of Analytical Separations 2008, vol. 6:839. Elsevier B.V.
17. Wheeler H. Chem. Incid. Rep. 1999, 14:10.
18. Mesilaakso M. Chemical Weapons Convention Chemical Analysis: Sample Collection, Preparation and Analytical Methods 2004, Wiley, Chichester, UK.
19. Black R.M., Harrison J.M., Hartley F.R. The Chemistry of Organophosphorus Compounds 1996, Wiley-Interscience, Chichester.
20. Ch.Kientz E. J. Chromatogr. A 1998, 814:1.
21. Mesilaakso M. Chemical weapons chemicals analysis. Encyclopedia of Analytical Chemistry 2000, Wiley, New York.
22. Kostiainen O. Handbook of Analytical Separations, Forensic Science 2000, 405. Elsevier Science B.V., Amsterdam. M.J. Bogusz (Ed.).
23. Lee H.S.N., Sng M.T., Basheer C., Lee H.K. J. Chromatogr. A 2007, 1148:8.
24. Kuitunen M.-L. Chemical Weapons Convention Chemical Analysis: Sample Collection, Preparation and Analytical Methods 2004, 163. Wiley, Chichester, UK. M. Mesilaakso (Ed.).
25. Hendrikse J. Chemical Weapons Convention Chemical Analysis: Sample Collection, Preparation and Analytical Methods 2004, 89. Wiley, Chichester, UK. M. Mesilaakso (Ed.).
26. Boyd-Boland A.A., Magdic S., Pawliszyn J.B. Analyst 1996, 121:929.
27. Eisert R., Levsen K. J. Am. Soc. Mass Spectrom. 1995, 6:1119.
28. Young R., Lopez-Avila V., Beckert W.F. J. High Resolut. Chromatogr. 1996, 19:247.
29. Sng M.T., Lee F.K., Lakso H.A. J. Chromatogr. A 1997, 759:225.
30. Zygmunt B., Zaborowska A., Swiatlowska J., Namiesnik J. J. Curr. Org. Chem. 2007, 11:241.
31. Report of the Twelfth Session of Scientific Advisory Board, OPCW, 2008.
32. Liu M.M., Zeng Z.R., Wang C.L., Tan Y.J., Liu H. Chromatographia 2003, 58:597.
33. Liu M., Zeng Z., Fang H. J. Chromatogr. A 2005, 1076:16.
34. Eldridge J. Jane's Nuclear, Biological and Chemical Defence 2006, Jane's Information Group Limited, Coulsdon, UK.
35. Murray G.M., Lawrence D.S. Chemical Weapons Convention Chemical Analysis: Sample Collection, Preparation and Analytical Methods 2004, 65. Wiley, Chichester, UK. M. Mesilaakso (Ed.).
36. Talmage S.S., Watson A.P., Hauschild V., Munro N.B., King J. Curr. Org. Chem. 2007, 11:285.
37. Chauhan S., Chauhan S., D'Cruz R., Faruqi S., Singh K.K., Varma S., Singh M., Karthik V. Environ. Toxicol. Pharmacol. 2008, 26:113.
38. Raber E., Jin A., Noonan K., McGuire R., Kirvel R.D. Int. J. Environ. Health Res. 2001, 11:128.
39. U.S. Army Potential Military Chemical/Biological Agents and Compounds. FM 3-9, NAVFAC P-467, AFR 355-7 1990, Headquarters, Departments of the Army, Navy, and Air Force, Fort McClellan, AL.
40. Kanamori-Kataoka A.M., Seto Y. J. Health Sci. 2008, 54:513.
41. Kingery A.F., Allen H.E. Toxicol. Environ. Chem. 1994, 47:155.
42. Gustafson R.L., Martell A.E. J. Am. Chem. Soc. 1962, 84:2309.
43. Harmbrook J.L., Howells D.J., Utley D. Pestic. Sci. 1971, 1:172.
44. Ward J.R., Yang Y.-C., Wilson R.B., Burrows W.D., Ackerman L.L. Bioorg. Chem. 1988, 16:12.
45. Sanches M.L., Russell C.R., Randolf C.L. Chemical Weapons Convention: (CWC) Signature Analysis. DNA-TR-92-73 ADB171788 1993, Defense Technical Information Center, Alexandria, VA.
46. U.S. Environmental Protection Agency Building Decontamination Alternatives 2005, National Homeland Security Research Center, Washington, DC.
47. U.S. Army NBC Decontamination. FM 3-5, MCWP 3-37.3 2002, U.S. Army Headquarters, Washington, DC.
48. K. Volchek, M. Finegas, M. Hornof, L. Boudreau, L. Duncan, J. Krishnan, Review of Decontamination and Restoration Technologies for Chemical, Biological and Radiological/Nuclear Counet- Terrorism. Manuscript Report EE-176, Environment Canada, Ottawa, ON, 2005.
49. Groenewold G.S. Main Group Chem. 2010, 9:221.
50. A FOA Briefing Book on Chemical Weapons: Threat, Effects, and Protection 1992, National Defence Research Establishment, Umeå. U. Ivarsson, H. Nilsson, J. Santesson (Eds.).
51. Papirmeister B., Gross C.L., Meier H., Petrali J.P., Johnson J.B. Toxicol. Sci. 1985, 5:134.
52. Army, Marine Corps, Navy, Air Force, Multi Service Tactics, Techniques, and Procedures, Potential Military Chemical/Biological Agents and Compound, 2005.
53. Black M.R., Muir B. J. Chromatogr. A 2003, 1000:253.
54. Sidel F.R. Riot control agent. Textbook of Military Medicine, Medical Aspects of Chemical and Biological Warfare 1997, Office of the Surgeon General, US Army, TMM Publications, Washington, DC, 307 pp.
55. Olajos E.J., Salem H. J. Appl. Toxicol. 2001, 21:355.
56. Beswick F.W. Hum. Toxicol. 1983, 2:247.
57. Sax N.I., Lewis R.J. Dangerous Properties of Industrial Materials 1984, Von Nostrand Reinhold, New York. 7th ed.
58. Olajos E.J., Stopford W. Riot Control Agents, Issues in Toxicology, Safety and Health 2004, CRC Press LLC, Boca Raton, FL.
59. Beswick F.W., Holland P., Kemp K.H. Br. J. Ind. Med. 1972, 29:298.
60. Arthur C.L., Pawliszyn J. Anal. Chem. 1990, 62:2145.
61. Pan L., Pawliszyn J. Anal. Chem. 1997, 69:196.
62. Pawliszyn J. Applications of Solid Phase Microextraction 1999, Royal Society of Analytical Chemistry, Cambridge.
63. Pawliszyn J. Solid Phase Microextraction, Theory and Practice 1997, Wiley-VCH.
64. Pillonel L., Bossett J.O., Tabacchi R. Lebensm. Wiss. U. Technol. 2002, 35:1.
65. Wardencki W., Michulec M., Curylo J.A. J. Food Sci. Technol. 2004, 39:703.
66. Malik A.K., Kaur V., Verma N. Talanta 2006, 68:842.
67. Quintana J.B., Rodriguez I. Anal. Bioanal. Chem. 2006, 384:1447.
68. Pragst F. Anal. Bioanal. Chem. 2007, 388:1393.
69. Ouyang G., Pawliszyn J. Anal. Bioanal. Chem. 2006, 386:1059.
70. Aulakh J.S., Malik A.K., Kaur V., Schmitt-Kopplin P. Anal. Chem. 2005, 35:71.
71. Bicchi C., Cordero C., Liberto E., Sgorbini B., Rubiolo P. J. Chromatogr. A 2008, 1184:220.
72. Kataoka H., Lord H.L., Pawliszyn J. Encyclopedia of Separation Science 2000, Academic Press, London.
73. Shirley R., Mani V., Mindrup R. Am. Environ. Lab 1999, 1-2:21.
74. Prosen H., Zupancic-Kralj L. Trends Anal. Chem. 1999, 18:272.
75. Yang Y., Hawthorne S.B., Miller D.J., Liu Y., Lee M.L. Anal. Chem. 1998, 70:1866.
76. Stashenko E.E., Martinez J.R. Trends Anal. Chem. 2004, 23:553.
77. Hill H.H., Martin S.J., Martin Pure Appl. Chem. 2002, 12:2281.
78. Popiel S., Witkiewicz Z., Szewczuk A. J. Hazard. Mater. B 2005, 123:94.
79. Mazurek M., Witkiewicz Z., Popiel S., Sliwakowski M. J. Chromatogr. A 2002, 919:133.
80. Lakso H.-A., Ng W.F. Anal. Chem. 1997, 69:1866.
81. Atar E., Cheskis S., Amirav A. Anal. Chem. 1991, 63:2061.
82. Cheskis S., Atar E., Amirav A. Anal. Chem. 1993, 65:539.
83. Frishman G., Amirav A. Field Anal. Chem. Technol. 2000, 4:17.
84. Carrick W.A., Cooper D.B., Muir B. J. Chromatogr. A 2001, 925:241.
85. Harvey S.D., Nelson D.A., Wright B.W., Grate J.W. J. Chromatogr. A 2002, 954:217.
86. Smith P.A., Lepage C.R.J., Koch D., Wyatt H.D.M., Hook G.L., Betsinger G., Erickson R.P., Eckenrode B.A. Trends Anal. Chem. 2004, 23:296.
87. Smith P.A., Lepage C.J., Lukacs M., Martin N., Shufutinsky A., Savage P.B. Int. J. Mass Spectrom. 2010, 295:113.
88. Smith P.A., Sng M.T., Eckenrode B.A., Leow S.Y., Koch D., Erickson R.P., Lepage C.R.J., Hook G.L. Chromatogr. J. A 2005, 1067:285.
89. Schneider J.F., Boparai A.S., Reed L.L. J. Chromatogr. Sci. 2001, 39:420.
90. Gate J.W., Patrash S.J., Kaganove S.N., Wise B.M. Anal. Chem. 1999, 71:1033.
91. Hook G.L., Lepage C.J., Miller S.I., Smith P.A. J. Sep. Sci. 2004, 27:1017.
92. Koziel J., Jia M., Pawliszyn J. Anal. Chem. 2000, 72:5178.
93. Augusto F., Koziel J., Pawliszyn J. Anal. Chem. 2001, 72:481.
94. Rearden P., Harrington P.B. Anal. Chim. Acta 2005, 545:13.
95. Massart D.L., Vandeginste B.G.M., Buydens L.M.C., De Jong S., Lewi P.J., Smeyers-Verbeke J. Handbook of Chemometrics and Qualimetrics, Part A 1997, Elsevier, New York, 429 pp.
96. Massart D.L., Vandeginste B.G.M., Buydens L.M.C., De Jong S., Lewi P.J., Smeyers-Verbeke J. Handbook of Chemometrics and Qualimetrics, Part A 1997, Elsevier, New York, 432 pp.
97. D'Agostino P.A., Provost L.R., Visentini J. J. Chromatogr. A 1987, 402:221.
98. M.J. Small, Technical Report 8208, US Army Medical Bioengineering Research and Development Laboratory, Fort Detrick, Frederick, MD, 1983.
99. Hook G.L., Kimm G., Koch D., Savage P.B., Ding B., Smith P.A. J. Chromatogr. A 2003, 992:1.
100. Hook G.L., Kimm G., Betsinger G., Savage P.B., Swift A., Logan T., Smith P.A. J. Sep. Sci. 2003, 26:1091.
101. Sng M.T., Ng W.F. J. Chromatogr. A 1999, 832:173.
102. Contreras J.A., Murray J.A., Tolley S.E., Oliphant J.L., Tolley H.D., Lambert S.A., Lee E.D., Later D.W., Lee M.L. J. Am. Soc. Mass Spectrom. 2008, 19:1425.
103. Smith P.A., Lepage C.R.J., Savage P.B., Bowerbank C.R., Lee E.D., Lukacs M.J. Anal. Chim. Acta 2011, 690:215.
104. Ghaderi S.S., Kulkami P.S., Ledford E.B., Wilkins C.L., Gross M.L. Anal. Chem. 1981, 53:428.
105. Alcaraz A., Hulsey S.S., Whipple R.E., Andresen B.D. Analytical Chemistry Associated with the Destruction of Chemical Weapons 1997, vol. 13:65. NATO ASI Ser. Ser. 1.
106. Kimm G.L., Hook G.L., Smith P.A. J. Chromatogr. A 2002, 971:185.
107. Creek J-A.M., McAnoy A.M., Brinkworth C.S. Rapid Commun. Mass Spectrom. 2010, 24:3419.
108. Szostek B., Aldstadt J.H. J. Chromatogr. A 1998, 807:253.
109. Tomkins B.A., Sega G.A., Ho C.H. J. Chromatogr. A 2001, 909:13.
110. Wooten J.V., Ashley D.L., Calafat A.M. J. Chromatogr. B 2002, 772:147.
111. Liming Z., Jinmei Z., Bo L., Junjun D., Shengli L., Caihong L. Trace level determination of Lewisite in water by solid-phase microextraction and gas chromatography-mass spectrometry with selected ion-monitoring. 2nd International Conference on Bioinformatics and Biomedical Engineering, iCBBE 2008, 3292. (art. no. 4536032).
112. Takekawa K., Oya M., Kido A., Suzuki O. Chromatographia 1998, 47:209.
113. Frison G., Zancanaro F., Favretto D., Ferrara S.D. Rapid Commun. Mass Spectrom. 2006, 20:2932.
114. Smith P.A., Sheely M.V., Kluchinsky T.A. J. Sep. Sci. 2002, 25:917.
115. Hout J.J., Hook G.L., Lapuma P.T., White D.W. J. Occup. Environ. Hyg. 2010, 7:352.
116. Cancho B., Ventura F., Galceran M.T. J. Chromatogr. A 2000, 897:307.
117. Antoniou C.V., Koukouraki E.E., Diamadopoulos E. J. Chromatogr. A 2006, 1132:310.
118. Alwis K.U., Blount B.C., Silva L.K., Smith M.M., Loose K.-H. Environ. Sci. Technol. 2008, 42:2522.