Determination of β-blockers and β-agonists using gas chromatography and gas chromatography-mass spectrometry - A comparative study of the derivatization step

Journal of Chromatography A

Volumn 1218, Issue 44, 2011, Pages 8110-8122

  Caban, Magda ^a   Stepnowski, Piotr ^a   Kwiatkowski, Marek ^a   Migowska, Natalia ^a   Kumirska, Jolanta ^a  

^a UNIVERSITY OF GDA SK   (Poland)

Author keywords

Agonists; Blockers; Comparative study; Derivatization step; GC and GC MS analyses

Indexed keywords

ACEBUTOLOL; ANALYTES; ATENOLOL; COMPARATIVE STUDIES; COMPARATIVE STUDY; DERIVATIZATION PROCEDURES; DERIVATIZATION STEP; DERIVATIZATIONS; DERIVATIZING REAGENTS; ENVIRONMENTAL MATRIXES; ENVIRONMENTAL SCIENCE; ETHYL ACETATES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GC-MS ANALYSIS; GROWING DEMAND; LITERATURE DATA; MASS SPECTRA; METOPROLOL; NADOLOL; PINDOLOL; RAPID SCREENING; SALBUTAMOL; SILYLATIONS; TARGET COMPOUND; TERBUTALINE; TRIFLUOROACETAMIDES; TRIMETHYL SILYLATION; TRIMETHYLCHLOROSILANES; TRIMETHYLSILYL;

ACYLATION; MASS SPECTROMETRY;

GAS CHROMATOGRAPHY;

ACEBUTOLOL; ACETIC ACID ETHYL ESTER; ATENOLOL; BETA ADRENERGIC RECEPTOR BLOCKING AGENT; BETA ADRENERGIC RECEPTOR STIMULATING AGENT; CHLOROTRIMETHYLSILANE; METOPROLOL; N,O BIS(TRIMETHYLSILYL)TRIFLUOROACETAMIDE; NADOLOL; PINDOLOL; PROPRANOLOL; SALBUTAMOL; SILICON DERIVATIVE; SOLVENT; TERBUTALINE; TRIFLUOROACETAMIDE DERIVATIVE; UNCLASSIFIED DRUG;

ACYLATION; ARTICLE; CYCLIZATION; DERIVATIZATION; DRUG DETERMINATION; GAS CHROMATOGRAPHY; INTERMETHOD COMPARISON; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; REACTION TIME; SILYLATION; TEMPERATURE; TERT BUTYLDIMETHYLSILYLATION; TRIMETHYLSILYLATION;

ACYLATION; ADRENERGIC BETA-2 RECEPTOR AGONISTS; ADRENERGIC BETA-ANTAGONISTS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; KINETICS; REPRODUCIBILITY OF RESULTS;

EID: 80054062392     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.08.093     Document Type: Article

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