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Tetrahedron
Volumn 67, Issue 45, 2011, Pages 8628-8634
Palladium on carbon-catalyzed solvent-free and solid-phase hydrogenation and Suzuki-Miyaura reaction
Author keywords

Cross coupling; Hydrogenation; Palladium on carbon; Solid phase synthesis; Solvent free
Indexed keywords

CARBON; PALLADIUM;
EID: 80053593399     PISSN: 00404020     EISSN: 14645416     Source Type: Journal    
DOI: 10.1016/j.tet.2011.09.043     Document Type: Article
Times cited : (45)
References (87)
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    • The palladium species of 5% Pd/HP20 are supported on a polystyrene-polyvinylbenzene-based synthetic adsorbents, DIAION HP20, which is commercially available from Mitsubishi Chemical Corporation Y. Monguchi, Y. Fujita, K. Endo, S. Takao, M. Yoshimura, Y. Takagi, T. Maegawa, and H. Sajiki Chem. - Eur. J. 15 2009 834 837
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    • 3 (Aldrich), 2.8 wt %] was used with quinoline (0.4 equiv) according to the literature, see On the other hand, over-reduction took place, i.e., diphenylethane (2%) formed together with desired cis-stilbene (35%) and trans-stilbene (3%), although the reaction was only slightly promoted to recover the staring diphenylacetylene (60%). The selective semi-hydrogenation to stilbene under the solvent-free conditions seems difficult to achieve
    • 3 (Aldrich), 2.8 wt %] was used with quinoline (0.4 equiv) according to the literature, see H. Lindlar, and R. Dubis Org. Synth. 46 1966 89 92 On the other hand, over-reduction took place, i.e., diphenylethane (2%) formed together with desired cis-stilbene (35%) and trans-stilbene (3%), although the reaction was only slightly promoted to recover the staring diphenylacetylene (60%). The selective semi-hydrogenation to stilbene under the solvent-free conditions seems difficult to achieve
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    • The melting points of the substrates and products, both of which are solid under the reaction conditions in Table 2, are as follows. 4-Azidobenzophenone (entry 6): 73-74 °C, see
    • The melting points of the substrates and products, both of which are solid under the reaction conditions in Table 2, are as follows. 4-Azidobenzophenone (entry 6): 73-74 °C, see Y. Ohba, S. Kubo, M. Nakai, A. Nagai, and M. Yoshimoto Bull. Chem. Soc. Jpn. 59 1986 2317 2320
    • (1986) Bull. Chem. Soc. Jpn. , vol.59 , pp. 2317-2320
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    • Benzoic acid (entry 13): 121 °C, see
    • Benzoic acid (entry 13): 121 °C, see R.H. Eastman, and F.L. Detert J. Am. Chem. Soc. 73 1951 4511 4515
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    • Eastman, R.H.1    Detert, F.L.2

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.