Selective enrichment of the degradation products of organophosphorus nerve agents by zirconia based solid-phase extraction

Journal of Chromatography A

Volumn 1218, Issue 38, 2011, Pages 6612-6620

  Kanaujia, Pankaj K ^a   Pardasani, Deepak ^a   Tak, Vijay ^a   Purohit, Ajay K ^a   Dubey, D K ^a  

^a DEFENCE RESEARCH AND DEVELOPMENT ESTABLISHMENT   (India)

Author keywords

Carboxylic acids; HybridSPE; Nerve agents; Phosphonic acids; Solid phase extraction; Zirconia

Indexed keywords

ALKYLPHOSPHONIC ACIDS; ANALYTES; ANION EXCHANGE; ANIONIC COMPOUNDS; DEGRADATION PRODUCTS; ENVIRONMENTAL MARKER; HYBRIDSPE; LIMIT OF QUANTIFICATIONS; LIMITS OF DETECTION; MODIFIER CONCENTRATION; NERVE AGENT DEGRADATION PRODUCTS; NERVE AGENTS; ORGANOPHOSPHORUS COMPOUNDS; PHOSPHONIC ACIDS; SELECTED ION MONITORING; SELECTIVE ENRICHMENT; SELECTIVE EXTRACTION; SOLID PHASE EXTRACTION METHOD; SOLID-PHASE EXTRACTION; TARGET ANALYTES;

CARBOXYLIC ACIDS; CHEMICAL ANALYSIS; DEGRADATION; DRUG PRODUCTS; PHOSPHORUS COMPOUNDS; ZIRCONIA;

EXTRACTION;

CHEMICAL WARFARE AGENT; METHYLPHOSPHONOTHIOIC ACID S (2 DIISOPROPYLAMINOETHYL) O ETHYL ESTER; ORGANOPHOSPHORUS NERVE AGENT; PHOSPHONIC ACID DERIVATIVE; SARIN; SOLVENT; SOMAN; UNCLASSIFIED DRUG; ZIRCONIUM OXIDE;

ANION EXCHANGE; ARTICLE; CHEMICAL ANALYSIS; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DEGRADATION; ELUTION; GAS CHROMATOGRAPHY; ION MONITORING; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS SPECTROMETRY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; SIGNAL NOISE RATIO; SOLID PHASE EXTRACTION; VALIDATION PROCESS;

ADSORPTION; CHEMICAL WARFARE AGENTS; NEUROTRANSMITTER AGENTS; ORGANOPHOSPHORUS COMPOUNDS; SARIN; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; SOMAN; ZIRCONIUM;

EID: 80052092412     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.07.091     Document Type: Article

References (31)

1. Mesilaakso M. Chemical Weapons Convention Chemical Analysis Sample Collection, Preparation and Analytical Methods 2005, Wiley, Chichester.
2. Criteria for Designation of Laboratories by OPCW-C-I/DEC.61 22 May 1997, Organization for Prohibition of Chemical Weapons, The Hague.
3. Hendrikse J. Chemical Weapons Chemical Analysis: Sample Collection, Preparation, and Analytical Methods 2005, 89. Wiley, Chichester. M. Mesilaakso (Ed.).
4. Hooijschuur E.W.J., Hulst A.G., De Jong Ad.L., De Reuver L.P., Van Krimpen S.H., Van Baar B.L.M., Wils E.R.J., Kientz C.E., Brinkman U.A.Th. Trends Anal. Chem. 2002, 21:116.
5. Convention on the Prohibition of the Development, Production, Stockpiling and Use of Chemical Weapons and their Destruction 1997, Technical Secretariat of the Organization for Prohibition of Chemical Weapons, The Hague, Accessible through internet http://www.opcw.org.
6. Krutzsch W., Trapp R. A Commentary of CWC 1994, Martinus Nijhoff, Dordrecht.
7. Maynard R.L. Chemical Warfare Agents: Toxicology and Treatment 2007, Wiley. 2nd ed. T.C. Marrs, R.L. Maynard, F.R. Sidell (Eds.).
8. Talmage S.S., Munro N.B., Watson A.P., King J.F., Hauschild V. Chemical Warfare Agents: Toxicology and Treatment 2007, Wiley. 2nd ed. T.C. Marrs, R.L. Maynard, F.R. Sidell (Eds.).
9. Kuitunen M.L. Chemical Weapons Convention Chemical Analysis Sample Collection, Preparation and Analytical Methods 2005, Wiley, Chichester, p163. M. Mesilaakso (Ed.).
10. Dubey D.K., Pardasani D., Gupta A.K., Palit M., Kanaujia P.K., Tak V. J. Chromatogr. A 2006, 1107:29.
11. Lee H.S.N., Basheer C., Lee H.K. J. Chromatogr. A 2006, 1124:91.
12. Riches J., Morton I., Read R.W., Black R.M. J. Chromatogr. B 2005, 816:251.
13. Tak V., Pardasani D., Kanaujia P.K., Dubey D.K. J. Chromatogr. A 2009, 1216:4319.
14. Kanaujia P.K., Pardasani D., Gupta A.K., Kumar R., Srivastava R.K., Dubey D.K. J. Chromatogr. A 2007, 1161:98.
15. Fredriksson S.A., Hammarstrom L.G., Henriksson L., Lakso H.A. J. Mass Spectrom. 1995, 30:1133.
16. Rautio M. Recommended Operating Procedures for Sampling and Analysis in the Verification of Chemical Disarmament 1994, Ministry for Foreign Affairs of Finland, Helsinki.
17. Hui M.Z., Qin L. Anal. Chim. Acta 2001, 435:121.
18. Moullec S.L., Begos A., Pichon V., Bellier B. J. Chromatogr. A 2006, 1108:7.
19. Pucci V., Di Palma S., Alfieri A., Bonelli F., Monteagudo E. J. Pharm. Biomed. Anal. 2009, 50:867.
20. Gonzalvez A., Preinerstorfer B., Lindner W. Anal. Bioanal. Chem. 2010, 396:2965.
21. Wan H., Yan J., Yu L., Zhang X., Xue X., Li X., Liang X. Talanta 2010, 82:1701.
22. Kweon H.K., Hakansson K. Anal. Chem. 2006, 78:1743.
23. Cha H.J., Kim N.H., Jeong E.K., Na Y.C. Bull. Korean Chem. Soc. 2010, 31:2322.
24. Nawrocki J., Rigney M.P., McCormick A., Carr P.W. J. Chromatogr. A 1993, 657:229.
25. Li J., Qi H.Y., Shi Y.P. J. Chromatogr. A 2009, 1216:5467.
26. Du D., Ye X., Zhang J., Zeng Y., Tu H., Zhang A., Liu D. Electrochem. Commun. 2008, 10:686.
27. Liu G., Wang J., Barry R., Petersen C., Timchalk C., Gassman P.L., Lin Y. Chem.-Eur. J. 2008, 14:9951.
28. Xu L., Lee H.K. Anal. Chem. 2007, 79:5241.
29. Silvestro L., Gheorghe M.C., Tarcomnicu I., Savu S., Savu S.R., Iordachescu A., Dulea C. J. Chromatogr. B 2010, 878:3134.
30. Zeng W., Xu Y., Constanzer M., Woolf E.J. J. Chromatogr. B 2010, 878:1817.
31. Kosolapoff G.M., Mair L. Organic Phosphorus Compounds 1976, vol. 7. Wiley, New York, p. 9, 22.