Application of a tandem mass spectrometer and core-shell particle column for the determination of 151 pesticides in grains

Journal of Agricultural and Food Chemistry

Volumn 59, Issue 16, 2011, Pages 8589-8608

  Wang, Jian ^a   Chow, Willis ^a   Cheung, Wendy ^a  

^a CANADIAN FOOD INSPECTION AGENCY   (Canada)

Author keywords

grains; LC ESI MS MS; measurement uncertainty; pesticides; UHPLC ESI MS MS

Indexed keywords

ATLANTIS; CORE-SHELL PARTICLE; DESIGNED EXPERIMENTS; ELECTROSPRAY IONIZATION TANDEM MASS SPECTROMETRY; ESI-MS/MS; GRAINS; IMPROVED METHODS; INTERNAL STANDARDS; ISOTOPICALLY LABELED; LC/ESI-MS/MS; MEASUREMENT UNCERTAINTY; NESTED DESIGN; PERFORMANCE PARAMETERS; POROUS PARTICLE; QUICK , EASY , CHEAP , EFFECTIVE , RUGGED , AND SAFE; RUNTIMES; STANDARD CALIBRATION; UHPLC/ESI-MS/MS; ULTRA-HIGH PERFORMANCE;

AGRICULTURAL CHEMICALS; COLUMN CHROMATOGRAPHY; ELECTROSPRAY IONIZATION; EXTRACTION; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; POROUS MATERIALS; STANDARDS; UNCERTAINTY ANALYSIS;

PESTICIDES;

PESTICIDE;

ARTICLE; CEREAL; CHEMISTRY; COMPARATIVE STUDY; ELECTROSPRAY MASS SPECTROMETRY; FOOD CONTAMINATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INSTRUMENTATION; METHODOLOGY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY;

CEREALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FOOD CONTAMINATION; PESTICIDES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY;

EID: 80051713686     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf202158g     Document Type: Article

References (10)

1. Alder, L.; Greulich, K.; Kempe, G.; Vieth, B. Residue analysis of 500 high priority pesticides: Better by GC-MS or LC-MS/MS? Mass Spectrom. Rev. 2006, 25 (6) 838-865 (Pubitemid 44727512)
2. Wang, J.; Chow, W.; Leung, D. Applications of LC/ESI-MS/MS and UHPLC QqTOF MS for the determination of 148 pesticides in fruits and vegetables Anal. Bioanal. Chem. 2010, 396 (4) 1513-1538
3. 18 J. Chromatogr. A 2010, 1217 (10) 1589-1603
4. Gritti, F.; Leonardis, I.; Abia, J.; Guiochon, G. Physical properties and structure of fine core-shell particles used as packing materials for chromatography: Relationships between particle characteristics and column performance J. Chromatogr. A 2010, 1217 (24) 3819-3843
5. Abrahim, A.; Al-Sayah, M.; Skrdla, P.; Bereznitski, Y.; Chen, Y.; Wu, N. Practical comparison of 2.7 μm fused-core silica particles and porous sub-2 μm particles for fast separations in pharmaceutical process development J. Pharm. Biomed. Anal. 2010, 51 (1) 131-137
6. Kansal, M.; Huq, S.; Sanchez, C. Kinetex sorbents for fast LC/MS applications: Successes and challenges. Phenomenex Application Note; http://www.phenomenex.com/lib/po75760510-l-4.pdf; accessed on February 17, 2011.
7. Wang, J.; Wotherspoon, D. Determination of pesticides in apples by liquid chromatography with electrospray ionization tandem mass spectrometry and estimation of measurement uncertainty J. AOAC Int. 2007, 90 (2) 550-567 (Pubitemid 350067252)
8. Wang, J.; Leung, D.; Butterworth, F. Determination of five macrolide antibiotic residues in eggs using liquid chromatography/electrospray ionization tandem mass spectrometry J. Agric. Food Chem. 2005, 53 (6) 1857-65 (Pubitemid 40395745)
9. QuEChERS-A mini-multiresidue method for the analysis of pesticide residues in low-fat products; http://www.quechers.com/default.htm; accessed on May 11, 2011.
10. Method validation and quality control procedures for pesticide residues analysis in food and feed. Document No. SANCO/10684/2009 Supersedes Document No. SANCO/3131/2007 Implemented by 01/01/2010; http://ec.europa.eu/food/plant/ protection/resources/qualcontrol-en.pdf, 2009.