Physical properties and structure of fine core-shell particles used as packing materials for chromatography. Relationships between particle characteristics and column performance

Journal of Chromatography A

Volumn 1217, Issue 24, 2010, Pages 3819-3843

  Gritti, Fabrice ^a,b   Leonardis, Irene ^a,b   Abia, Jude ^a,b   Guiochon, Georges ^a,b  

^a UNIVERSITY OF TENNESSEE   (United States)

^b OAK RIDGE NATIONAL LABORATORY   (United States)

Author keywords

Column performance; Coulter particle size distribution; Halo particles; Height equivalent to a theoretical plate; Inverse size exclusion chromatography; Kinetex particles; Local electrochemical detection; Low temperature nitrogen adsorption; Peak parking method; Pycnometry; Scanning electron microscopy; Shell particles; Shell structure; Silica nanoparticles; Silica particles; Specific surface area; Total pore blocking

Indexed keywords

COLUMN PERFORMANCE; ELECTROCHEMICAL DETECTION; HEIGHT EQUIVALENT TO A THEORETICAL PLATES; LOCAL ELECTROCHEMICAL DETECTION; LOW-TEMPERATURE NITROGEN; PORE BLOCKING; PYCNOMETRY; SHELL STRUCTURE; SILICA NANOPARTICLES; SILICA PARTICLES;

CHEMICAL DETECTION; GAS ADSORPTION; MATERIALS PROPERTIES; NANOPARTICLES; NITROGEN; PARTICLE SIZE; PLATES (STRUCTURAL COMPONENTS); PORE SIZE; POROUS MATERIALS; SCANNING; SCANNING ELECTRON MICROSCOPY; SHELLS (STRUCTURES); SILICA; SIZE DISTRIBUTION; SIZE EXCLUSION CHROMATOGRAPHY; SPECIFIC SURFACE AREA;

COLUMN CHROMATOGRAPHY;

ANTHRACENE; INSULIN; NANOPARTICLE; NAPHTHO[2,3 A]PYRENE; PYRENE DERIVATIVE; SILICATE; UNCLASSIFIED DRUG;

ADSORPTION; ARTICLE; CONTROLLED STUDY; DIFFUSION COEFFICIENT; ELECTROCHEMICAL ANALYSIS; GEL PERMEATION CHROMATOGRAPHY; LOW TEMPERATURE; PARTICLE SIZE; PHYSICAL CHEMISTRY; POROSITY; PRIORITY JOURNAL; SCANNING ELECTRON MICROSCOPY;

ADSORPTION; ANTHRACENES; CHROMATOGRAPHY, GEL; CHROMATOGRAPHY, REVERSE-PHASE; INSULIN; MICROSCOPY, ELECTRON, SCANNING; MICROSCOPY, ELECTRON, TRANSMISSION; MICROSPHERES; NAPHTHALENES; NITROGEN; PARTICLE SIZE; POROSITY; PYRENES;

EID: 77953596053     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.04.026     Document Type: Article

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