Analysis of β-blockers in groundwater using large-volume injection coupled-column reversed-phase liquid chromatography with fluorescence detection and liquid chromatography time-of-flight mass spectrometry

Journal of Separation Science

Volumn 34, Issue 15, 2011, Pages 1796-1804

  Galera, María M ^a   Vázquez, Piedad P ^a   Vázquez, María Del Mar P ^a   García, María Dolores G ^a   Amate, Carmen F ^a  

^a UNIVERSITY OF ALMERÍA   (Spain)

Author keywords

Blockers; Coupled columns; Groundwater; LC; TOF MS

Indexed keywords

ACCURATE MASS; ANALYTES; ATENOLOL; BISOPROLOL; CLEAN UP; COUPLED COLUMN; EMPIRICAL FORMULAS; FLUORESCENCE DETECTION; LARGE VOLUME INJECTION; LC; LIMIT OF QUANTIFICATIONS; MATRIX EFFECTS; METHOD DEVELOPMENT; METOPROLOL; NADOLOL; PRE-CONCENTRATION; REVERSED-PHASE LIQUID CHROMATOGRAPHY; SAMPLE PRETREATMENT; SELECTIVE EXTRACTION; SINGLE-STEP; SOLID PHASIS; SOLID-PHASE EXTRACTION; TARGET COMPOUND; TIME OF FLIGHT MASS SPECTROMETRY; TOF-MS;

COLUMN CHROMATOGRAPHY; EXTRACTION; FINITE DIFFERENCE METHOD; FLUORESCENCE; GROUNDWATER; INDUCTIVELY COUPLED PLASMA; LIQUIDS; MASS SPECTROMETERS; MASS SPECTROMETRY; METHANOL;

LIQUID CHROMATOGRAPHY;

ATENOLOL; BETAXOLOL; BISOPROLOL; GROUND WATER; METHANOL; METOPROLOL; NADOLOL; BETA ADRENERGIC RECEPTOR BLOCKING AGENT;

ACCURACY; ARTICLE; CONTROLLED STUDY; COST MINIMIZATION ANALYSIS; DRUG DETERMINATION; DRUG IDENTIFICATION; DRUG ISOLATION; DRUG PURIFICATION; ELECTROSPRAY MASS SPECTROMETRY; INTERMETHOD COMPARISON; LARGE VOLUME INJECTION COUPLED COLUMN REVERSED PHASE LIQUID CHROMATOGRAPHY WITH FLUORESCENCE DETECTION; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY TIME OF FLIGHT MASS SPECTROMETRY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; REVERSED PHASE LIQUID CHROMATOGRAPHY; SENSITIVITY ANALYSIS; SOLID PHASE EXTRACTION; SPAIN; TIME OF FLIGHT MASS SPECTROMETRY; VALIDATION PROCESS; WATER CONTAMINATION; CHEMISTRY; FLUORESCENCE; MASS SPECTROMETRY; TIME;

ADRENERGIC BETA-ANTAGONISTS; CHROMATOGRAPHY, LIQUID; CHROMATOGRAPHY, REVERSE-PHASE; FLUORESCENCE; GROUNDWATER; MASS SPECTROMETRY; TIME FACTORS;

EID: 79960767313     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201100117     Document Type: Article

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