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Compounds 2b - d are commercially available, and 2e was prepared as reported in the literature:;, Compound 2a was synthesized following the same synthetic strategy than for 2e
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Crystals of compounds rac - 3a - e and the complex between rac -3c and oxalic acid were obtained by slow evaporation of their solutions in organic solvents at rt. Supplementary crystallographic data for this paper (CCDC 791802-791806 and 823794) can also be obtained free of charge via, by emailing data-request@ccdc.cam.ac.uk, or by contacting The Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033
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Crystals of compounds rac-3a - e and the complex between rac -3c and oxalic acid were obtained by slow evaporation of their solutions in organic solvents at rt. Supplementary crystallographic data for this paper (CCDC 791802-791806 and 823794) can also be obtained free of charge via www.ccdc.cam.ac.uk/data-request/cif, by emailing data-request@ccdc.cam.ac.uk, or by contacting The Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033.
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