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79958814075
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note
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- 1): 2961 (w), 2810 (w), 1586 (s), 1501 (w), 1458 (w), 1408 (vs), 1358 (w), 1325 (w), 1299 (w), 1227 (w), 1162 (w), 1133 (w),1065 (w), 1014 (w), 933 (w), 844 (m), 801(m), 787(w).
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35
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79958864016
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note
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3, Z = 2. Refinement of 442 parameters (with 1 restraints) on 9125 independent reflections out of 20117 measured reflections (Rint = 0.0444) led to R1 = 0.0721, wR2 = 0.1606 (all data) and S = 1.063. Five of the camphorate carbon atoms were disordered over two sets of positions and were modelled successfully using partial occupancy factors. Hydrogen atoms were placed in calculated positions.
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