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No rationalization may be proposed about the influence of molecular sieves in petroleum ether since dimethyl and diethyl acetylenedicarboxylates are poorly soluble in this solvent
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72
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79957955668
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73
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79957954160
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This alcohol 5 was particularly prone to degradation. For example, it was prepared from a corresponding allylsilane by hydroboration followed by oxidation and formation of 1,1-dimethyl-1-sila-2-oxacyclopentane and 2-ethylfuran was noticed during storage or chromatography if borane derivatives remained after the oxidation step
-
This alcohol 5 was particularly prone to degradation. For example, it was prepared from a corresponding allylsilane by hydroboration followed by oxidation and formation of 1,1-dimethyl-1-sila-2-oxacyclopentane and 2-ethylfuran was noticed during storage or chromatography if borane derivatives remained after the oxidation step.
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74
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79957931284
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Supplied by Aldrich.
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75
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79957954374
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Supplied by Prolabo
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Supplied by Prolabo.
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