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Volumn 13, Issue 9, 2011, Pages 3189-3196

Synthesis and polymorphism of (4-ClpyH)2[CuCl4]: Solid-gas and solid-solid reactions

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EID: 79954468736     PISSN: 14668033     EISSN: 14668033     Source Type: Journal    
DOI: 10.1039/c0ce00628a     Document Type: Article
Times cited : (39)

References (55)
  • 1
    • 79954496913 scopus 로고    scopus 로고
    • Special issue on inclusion compounds and reactions in crystals
    • Special issue on inclusion compounds and reactions in crystals, CrystEngComm, 2011, 13
    • (2011) CrystEngComm
  • 41
    • 79954461742 scopus 로고    scopus 로고
    • Bruker AXS, Madison, Wisconsin, USA
    • APEX2, V. 2.1-0, Bruker AXS, Madison, Wisconsin, USA, 2008
    • (2008) APEX2, V. 2.1-0
  • 47
    • 0002211129 scopus 로고
    • The solution-phase synthesis, crystal structure determination and crystal structure at 100 K of 2 (phase I) are reported in the ESI
    • H. M. Rietveld J. Appl. Crystallogr. 1969 2 65
    • (1969) J. Appl. Crystallogr. , vol.2 , pp. 65
    • Rietveld, H.M.1
  • 48
    • 4043069861 scopus 로고    scopus 로고
    • The values listed for the scan range (-2.5 ≤ 2 ≤ 15.5°) are those for the middle of detector of the nine. Thus, data with fewer detectors are collected at angles lower than the starting 2 value and higher than the end value Rietveld refinements were conducted for the range 1.0 ≤ 2 ≤ 16.0° for patterns until all of compound 1 had been consumed. Subsequent refinements were conducted for the range 2.5 ≤ 2 ≤ 16.0° as no peaks for phase I or phase II of compound 2 are observed at 2 < 2.5°
    • A. N. Fitch J. Res. Natl. Inst. Stand. Technol. 2004 109 133
    • (2004) J. Res. Natl. Inst. Stand. Technol. , vol.109 , pp. 133
    • Fitch, A.N.1
  • 54
    • 0001078330 scopus 로고    scopus 로고
    • The Rietveld fit for scan 4 (15-20 min after HCl exposure) is provided in the ESI and shows that at this stage the material is all unreacted 1 Since the final measurement powder pattern was measured at a point in the capillary close to the open end (i.e. where the transformation will have progressed furthest) it is estimated that the phase transition monitored at the central position in the capillary will take between 40 and 55 min under the conditions of the experiment
    • L. Lei Z. Whang X. Xin Thermochim. Acta 1997 297 193
    • (1997) Thermochim. Acta , vol.297 , pp. 193
    • Lei, L.1    Whang, Z.2    Xin, X.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.