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The values listed for the scan range (-2.5 ≤ 2 ≤ 15.5°) are those for the middle of detector of the nine. Thus, data with fewer detectors are collected at angles lower than the starting 2 value and higher than the end value Rietveld refinements were conducted for the range 1.0 ≤ 2 ≤ 16.0° for patterns until all of compound 1 had been consumed. Subsequent refinements were conducted for the range 2.5 ≤ 2 ≤ 16.0° as no peaks for phase I or phase II of compound 2 are observed at 2 < 2.5°
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