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To be precise, as shown in Figure S5, the emulsions (after diluting by 5-10-fold excess of water) exhibited a bimodal particle size distribution. This observation was tentatively attributed to the simultaneous coexistence of polymer particles (smaller size, around 270 nm) and monomer droplets (larger size, around 1090 nm) in the emulsion. Indeed, for this particular example, the percentage of smaller polymer particles was calculated to be 36%, in good correlation with the monomer conversion determined gravimetrically (32%)
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1H NMR spectrum (Figure 5 b); (ii) monomodal distributions are observed in SEC traces of poly(isoprene)s obtained in aqueous media; (iii) the content of double bonds is 96% or higher for these chains.
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1H NMR spectrum (Figure 5 b); (ii) monomodal distributions are observed in SEC traces of poly(isoprene)s obtained in aqueous media; (iii) the content of double bonds is 96% or higher for these chains.
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