Derivatization and fragmentation pattern analysis of natural and synthetic steroids, as their trimethylsilyl (oxime) ether derivatives by gas chromatography mass spectrometry: Analysis of dissolved steroids in wastewater samples

Journal of Chromatography A

Volumn 1218, Issue 14, 2011, Pages 1878-1890

  Andrasi N ^a   Helenkar A ^a   Záray, Gy ^a   Vasanits, A ^a   Molnar Perl I ^a  

^a EÖTVÖS LORÁND UNIVERSITY   (Hungary)

Author keywords

Aquatic environmental pollutant; Fragmentation patterns; Gas chromatography mass spectrometry; Oximation; Steroids; Trimethylsilylation

Indexed keywords

ENVIRONMENTAL POLLUTANTS; FRAGMENTATION PATTERNS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; OXIMATION; STEROIDS; TRIMETHYL SILYLATION;

ALCOHOLS; CHOLESTEROL; ETHERS; EXTRACTION; LIPIDS; MASS SPECTROMETRY; OPTIMIZATION; POLLUTION; WASTEWATER;

GAS CHROMATOGRAPHY;

ANDROSTANOLONE; ANDROSTENEDIONE; ANDROSTERONE; CHOLESTEROL; COPROSTEROL; ESTRIOL; ETHINYLESTRADIOL; ETONOGESTREL; GESTODENE; LEVONORGESTREL; MEDROXYPROGESTERONE ACETATE; MESTRANOL; NORETHISTERONE; PROGESTERONE; SITOSTEROL; STEROID; STIGMASTEROL; TESTOSTERONE; TRANSANDROSTERONE; TRANSDEHYDROANDROSTERONE; TRIMETHYLSILYL DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CALIBRATION; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; CONTROLLED STUDY; DERIVATIZATION; FRAGMENTATION REACTION; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; QUANTITATIVE STUDY; REPRODUCIBILITY; RESIDUE ANALYSIS; SEPARATION TECHNIQUE; SOLID PHASE EXTRACTION; WASTE WATER MANAGEMENT; WATER POLLUTANT;

ETHERS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; OXIMES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SEWAGE; SOLID PHASE EXTRACTION; STEROIDS; TRIMETHYLSILYL COMPOUNDS; WATER POLLUTANTS, CHEMICAL;

EID: 79952627790     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.01.051     Document Type: Article

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