A new reliable sample preparation for high throughput focused steroid profiling by gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1217, Issue 43, 2010, Pages 6652-6660

  Anizan, Sébastien ^a   Bichon, Emmanuelle ^a   Monteau, Fabrice ^a   Cesbron, Nora ^a   Antignac, Jean Philippe ^a,b   Le Bizec, Bruno ^a  

^a LUNAM UNIVERSITÉ   (France)

^b CEMAGREF   (France)

Author keywords

Chemical food safety; GC MS; Mass spectrometry; Metabolomic; Microextraction by packed sorbent (MEPS); Steroid hormones

Indexed keywords

FOOD SAFETY; GC-MS; METABOLOMICS; MICROEXTRACTION; STEROID HORMONE;

BODY FLUIDS; CHEMICAL CONTAMINATION; CHROMATOGRAPHIC ANALYSIS; DEGRADATION; ENDOCRINOLOGY; GAS CHROMATOGRAPHY; HEALTH; HORMONES; LIPIDS; MASS SPECTROMETRY; METABOLISM; METABOLITES; SORBENTS; SORPTION; THROUGHPUT;

EXTRACTION;

11 KETO,5BETA ANDROSTANEDIONE; 16ALPHA HYDROXYANDROSTERONE; 2ALPHA HYDROXYTESTOSTERONE; 5 ANDROSTANE 3BETA,17ALPHA DIOL; 5ALPHA ANDROSTANE 3BETA,17ALPHA DIOL; 5BETA ANDROSTANE 3ALPHA,17ALPHA DIOL; 6 ALPHA HYDROXYESTRADIOL; 7BETA HYDROXYPREGNENOLONE; ANDROSTENEDIONE; ETIOCHOLANOLONE; SEX HORMONE; UNCLASSIFIED DRUG;

ANIMAL EXPERIMENT; ARTICLE; CONTROLLED STUDY; HIGH THROUGHPUT SCREENING; MASS FRAGMENTOGRAPHY; METABOLOMICS; NONHUMAN; PRIORITY JOURNAL; RELIABILITY; REPRODUCIBILITY; SEX HORMONE DETERMINATION; SOLID PHASE MICROEXTRACTION; URINALYSIS;

ANABOLIC AGENTS; ANDROSTENEDIONE; ANIMALS; CATTLE; FEMALE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HIGH-THROUGHPUT SCREENING ASSAYS; MALE; MULTIVARIATE ANALYSIS; OSMOLAR CONCENTRATION; PRINCIPAL COMPONENT ANALYSIS; REPRODUCIBILITY OF RESULTS; SOLID PHASE MICROEXTRACTION; STEROIDS;

ANIMALIA; BOS;

EID: 77957255924     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.04.062     Document Type: Article

References (42)

1. Council Directive 88/146/EC.
2. Council Directive 96/22/EC.
3. Mooney M., Elliott C., Le Bizec B. Trends Anal. Chem. 2009, 28:665-675.
4. Noppe H., Le Bizec B., Verheyden K., De Brabander H. Anal. Chim. Acta 2008, 611:1-16.
5. Buisson C., Hebestreit M., Weigert A.P., Heinrich K., Fry H., Flenker U., Banneke S., Prevost S., Andre F., Schaenzer W., Houghton E., Le Bizec B. J. Chromatogr. A 2005, 1093:69-80.
6. Hebestreit M., Flenker U., Buisson C., Andre F., Le Bizec B., Fry H., Lang M., Weigert A.P., Heinrich K., Hird S., Schanzer W. J. Agric. Food Chem. 2006, 54:2850-2858.
7. Rambaud L., Bichon E., Cesbron N., André F., Bizec B.L. Anal. Chim. Acta 2005, 532:165-176.
8. Gaillard Y., Vayssette F., Balland A., Pépin G. J. Chromatogr. B 1999, 735:189-205.
9. Gratacós-Cubarsí M., Castellari M., Valero A., García-Regueiro J. J. Chromatogr. B 2006, 834:14-25.
10. Arts C.J.M., Van Baak M.J., Den Hartog J.M.P. J. Chromatogr. Biomed. Appl. 1991, 564:429-444.
11. Nielen M.W., Lasaroms J.J., Essers M.L., Sanders M.B., Heskamp H.H., Bovee T.F., van Rhijn J., Groot M.J. Anal. Chim. Acta 2007, 586:30-34.
12. Cawley A.T., Hine E.R., Trout G.J., George A.V., Kazlauskas R. Forensic Sci. Int. 2004, 143:103-114.
13. Maume D., Le Bizec B., Pouponneau K., Deceuninck Y., Solere V., Paris A., Antignac J., Andre F. Anal. Chim. Acta 2003, 483:289-297.
14. Moon J., Jung H., Moon M.H., Chung B.C., Choi M.H. J. Am. Soc. Mass Spectrom. 2009, 20:1626-1637.
15. Dumas M., Debrauwer L., Beyet L., Lesage D., Andre F., Paris A., Tabet J. Anal. Chem. 2002, 74:5393-5404.
16. Rijk J.C.W., Lommen A., Essers M.L., Groot M.J., Van Hende J.M., Doeswijk T.G., Nielen M.W.F. Anal. Chem. 2009, 81:6879-6888.
17. Arthur C.L., Pawliszyn J. Anal. Chem. 1990, 62:2145-2148.
18. Zhang Z., Yang M.J., Pawliszyn J. Anal. Chem. 1994, 66:844A-853A.
19. Risticevic S., Niri V., Vuckovic D., Pawliszyn J. Anal. Bioanal. Chem. 2009, 393:781-795.
20. Supelco, SPME Application Guide, 3rd edition.
21. Vas G., Vékey K. J. Mass Spectrom. 2004, 39:233-254.
22. Carpinteiro J., Quintana J., Rodríguez I., Carro A., Lorenzo R., Cela R. J. Chromatogr. A 2004, 1056:179-185.
23. Okeyo P., Rentz S.M., Snow N.H. J. High Resolut. Chrom. 1997, 20:171-173.
24. Okeyo P.D., Snow N.H. J. Microcol. Sep. 1998, 10:551-556.
25. Yang L., Luan T., Lan C. J. Chromatogr. A 2006, 1104:23-32.
26. Zhang Z., Duan H., Zhang L., Chen X., Liu W., Chen G. Talanta 2009, 78:1083-1089.
27. Abdel-Rehim M, 2003. AstraZeneca application " syringe for solid phase microextraction" Current Patents Gazette, week 0310, WO 03019149, p. 77.
28. Abdel-Rehim M. J. Chromatogr. B 2004, 801:317-321.
29. Abdel-Rehim M. J. Chromatogr. A 2010, 1217:2569-2580.
30. Vita M., Skansen P., Hassan M., Abdel-Rehim M. J. Chromatogr. B 2005, 817:303-307.
31. Morales-Cid G., Cárdenas S., Simonet B.M., Valcárcel M. Anal. Chem. 2009, 81:3188-3193.
32. Abdel-Rehim M., Dahlgren M., Blomberg L. J. Sep. Sci. 2006, 29:1658-1661.
33. Jagerdeo E., Abdel-Rehim M. J. Am. Soc. Mass Spectrom. 2009, 20:891-899.
34. SGE Analytical Science, Dioxins 2008, Poster TP-0180-M.
35. Van Renterghem P., Van Eenoo P., Van Thuyne W., Geyer H., Schänzer W., Delbeke F. J. Chromatogr. B 2008, 876:225-235.
36. Courant F., Pinel G., Bichon E., Monteau F., Antignac J., Bizec B.L. Analyst 2009, 134:1637-1646.
37. Cruz-Vera M., Lucena R., Cárdenas S., Valcárcel M. Trends Anal. Chem. 2009, 28:1164-1173.
38. Pawliszyn J., Pawliszyn B., Pawliszyn M. Chem. Educ. 1997, 2.
39. Snow N.H. J. Chromatogr. A 2000, 885:445-455.
40. Jurado C., Gimenez M., Soriano T., Menendez M., Repetto M. J. Anal. Toxicol. 2000, 24:11-16.
41. Pinel G., Rambaud L., Cacciatore G., Bergwerff A., Elliott C., Nielen M., Le Bizec B. J. Steroid Biochem. Mol. Biol. 2008, 110:30-38.
42. G. Pinel, L. Rambaud, F. Monteau, C. Elliot, B. Le Bizec, J. Steroid Biochem. Mol. Biol., (2009), in press. doi:10.1016/j.jsbmb.2010.01.012.