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note
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70: C, 15.02; H, 2.02; N, 2.80; Cr, 2.60; Cu, 6.36; Mo, 43.19 (%). Found: C, 15.21; H, 2.07; N, 2.66; Cr, 2.75; Cu, 6.72; Mo, 43.34 (%).
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note
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2 using the SHELXTL crystallographic software package. Anisotropic thermal parameters were used to refine all non-hydrogen atoms except for O7W, O8W, and O9W of compound 1 and O8W of compound 2. Hydrogen atoms on the 1,10-phenanthroline ligands were placed on calculated positions and included in the refinement riding on their respective parent atoms. All the hydrogen atoms for protonation were located in the difference Fourier maps, and their positions were refined using isotropic thermal parameters. Those hydrogen atoms attached to lattice water molecules were not located.
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