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6 crystals. Pure title compounds could be obtained by reacting a stoichiometric mixture of the same reagents in a fused-silica tube at 800 °C for 2 h, followed by quenching to air.
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26
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78651328254
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note
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int = 6.83%, GOF = 1.209, 86 parameters, R1 = 3.79%, wR2 = 8.27% for I > 2ω(I). No evidence of supercell, merohedral, or nonmerohedral twinning was found.
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27
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78651264443
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note
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int = 6.70%, GOF = 1.123, 112 parameters, R1 = 4.38%, wR2 = 7.64% for I > 2ω(I).
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