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Crystal data for KZrPSe6 at 298(2) K: Synchrotron radiation (λ, 0.406 63 Å, Pmc21 a, 3.7079(10) Å, b, 15.074(5) Å, c, 18.491(6) Å, V, 1033.5(5) Å3, Z, 4, ρcalcd, 4.080 g/cm3, μ, 5.624 mm-1, F(000, 1112, θ, 0.77°-20.65°, Index ranges:-5 ≤ h ≤ 5,-22 ≤ k ≤ 23,-28 < l < 31, 30 002 total reflections, 5045 independent reflection with R(int, 0.1827, Completeness to θ, 19.72°: 95, Refinement method: Full-matrix least-squares on F2, Data/restraints/parameters, 5045/0/108, Refinement on F2, GOF, 1.35, Final R indices [I > 3σ(I, Robs, 0.0644, wRobs, 0.1220. R indices all data, Rall, 0.1885, wRall, 0.1646
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