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European Journal of Organic Chemistry

Volumn , Issue 29, 2010, Pages 5650-5658

A facile synthesis of substituted indenones and piperidine-2,6-diones from the baylis-hillman acetates

(2) Basavaiah, Deevi a Lenin, Dandamudi V a

a UNIVERSITY OF HYDERABAD (India)

Author keywords

Alkylation; Baylis Hillman reaction; Carbocycles; Cyclization; Synthetic methods

Indexed keywords

EID: 78249248703 PISSN: 1434193X EISSN: 10990690 Source Type: Journal
DOI: 10.1002/ejoc.201000739 Document Type: Article

Times cited : (24)

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- We also isolated approximately 20-30 mg of an unknown impure product in the 0.5 mmol scale reaction. Although there was no significant formation of the tetralone derivatives, the presence of some minor amounts of such derivatives is not ruled out because the yields of the indenone derivatives was only 38-40%.
- We also isolated approximately 20-30 mg of an unknown impure product in the 0.5 mmol scale reaction. Although there was no significant formation of the tetralone derivatives, the presence of some minor amounts of such derivatives is not ruled out because the yields of the indenone derivatives was only 38-40%.

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- We also isolated approximately 30-40% of the trans-cinnamic acid (in addition to the desired indenone derivative).
- We also isolated approximately 30-40% of the trans-cinnamic acid (in addition to the desired indenone derivative).

98
- 78249277780
- Detailed X-ray crystallographic data is available from the Cambridge Crystallographic Data Centre, 12 Union road, Cambridge CB2 1EZ, UK, for compounds 8d (CCDC-775027), 10a (CCDC-775028), and 11a (CCDC-776461).
- Detailed X-ray crystallographic data is available from the Cambridge Crystallographic Data Centre, 12 Union road, Cambridge CB2 1EZ, UK, for compounds 8d (CCDC-775027), 10a (CCDC-775028), and 11a (CCDC-776461).

99
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- In this case also the formation of minor amounts of the tetralone derivative cannot be ruled out because the yields of the products were not quantitative.
- In this case also the formation of minor amounts of the tetralone derivative cannot be ruled out because the yields of the products were not quantitative.

100
- 78249261736
- [3k,3l] Our data is in agreement with those reported in the literature.
- [3k,3l] Our data is in agreement with those reported in the literature.

101
- 78249233477
- [3l] indicates that 7a is a low melting solid (44-46 °C). Since yields of the compound were very low, we did not attempt to obtain the compound as a solid.
- [3l] indicates that 7a is a low melting solid (44-46 °C). Since yields of the compound were very low, we did not attempt to obtain the compound as a solid.

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