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3, T = 112(2) K, F(000) = 1444, μ(Mo-Ka) = 1.108 mm-1, block, 6717 reflections measured, 3321 unique (Rint = 0.0217), 160 parameters, R1 = 0.0937 [I>2σ(I)], wR2 = 0.2808 [I>2σ(I)], GOF = 1.109
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3, T = 112(2) K, F(000) = 1444, μ(Mo-Ka) = 1.108 mm-1, block, 6717 reflections measured, 3321 unique (Rint = 0.0217), 160 parameters, R1 = 0.0937 [I>2σ(I)], wR2 = 0.2808 [I>2σ(I)], GOF = 1.109.
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