Reversed-phase chiral HPLC and LC/MS analysis with tris(chloromethylphenylcarbamate) derivatives of cellulose and amylose as chiral stationary phases

Journal of Chromatography A

Volumn 1217, Issue 44, 2010, Pages 6942-6955

  Peng, Liming ^a   Jayapalan, Swapna ^a   Chankvetadze, Bezhan ^b   Farkas, Tivadar ^a  

^a Phenomenex   (United States)

^b TBILISI STATE UNIVERSITY   (Georgia)

Author keywords

Electrospray LC MS; Method development and optimization; Polysaccharide derived chiral stationary phases; Reversed phase HPLC

Indexed keywords

ACETONITRILE; CYCLODEXTRINS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METHANOL; POSITIVE IONS; SEPARATION; STEREOCHEMISTRY;

CELLULOSE TRIS(3 ,5-DIMETHYLPHENYLCARBAMATE); CHIRAL PHARMACEUTICALS; CHIRAL STATIONARY PHASIS; ELECTROSPRAYS; LOW CONCENTRATION LEVELS; METHOD DEVELOPMENT; REVERSED PHASE HPLC; STRUCTURAL DIVERSITY;

CELLULOSE;

ACETONITRILE; AMMONIUM ACETATE; AMMONIUM BICARBONATE; AMYLOSE; AMYLOSE TRIS(2 CHLORO 5 METHYLPHENYLCARBAMATE); BICARBONATE; CELLULOSE; CELLULOSE TRIS(3 CHLORO 4 METHYLPHENYLCARBAMATE); DIETHYLAMINE; FORMIC ACID; MEBEVERINE; METHANOL; METHAQUALONE; NAPROPAMIDE; NOMIFENSINE; REBOXETINE; TETRAMISOLE; THALIDOMIDE; TOLPERISONE; UNCLASSIFIED DRUG; ZOPICLONE;

AQUEOUS SOLUTION; ARTICLE; CHIRALITY; CONCENTRATION RESPONSE; CONTROLLED STUDY; DRUG DETERMINATION; DRUG ISOLATION; ELECTROSPRAY MASS SPECTROMETRY; ENANTIOSELECTIVITY; INTERMETHOD COMPARISON; MASS SPECTROMETRY; MOLECULAR RECOGNITION; PERFORMANCE MEASUREMENT SYSTEM; PRIORITY JOURNAL; PROCESS OPTIMIZATION; RACEMIC MIXTURE; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SCREENING TEST; SEPARATION TECHNIQUE; STRUCTURE ANALYSIS; TANDEM MASS SPECTROMETRY; TEMPERATURE SENSITIVITY;

EID: 77957652255     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.08.075     Document Type: Article

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