Gas chromatographic-tandem mass spectrometric determination of anabolic steroids and their esters in hair: Application in doping control and meat quality control

Journal of Chromatography B: Biomedical Sciences and Applications

Volumn 735, Issue 2, 1999, Pages 189-205

  Gaillard, Yvan ^a   Vayssette, François ^a   Balland, Antoine ^b   Pépin, Gilbert ^a  

^a Laboratoire d'Expertises TOXLAB   (France)

^b Laboratoires ACE   (France)

Author keywords

Anabolic steroids; Doping; Hair; Steroids; Testosterone esters

Indexed keywords

ACETIC ACID ETHYL ESTER; ANABOLIC AGENT; BOLDENONE; ESTER; ETHINYLESTRADIOL; METANDIENONE; METHANOL; METHYLTESTOSTERONE; NANDROLONE; NANDROLONE DECANOATE; REAGENT; SODIUM HYDROXIDE; TESTOSTERONE CIPIONATE; TESTOSTERONE ESTER; TESTOSTERONE PROPIONATE; TESTOSTERONE UNDECANOATE;

ANALYTIC METHOD; ANIMAL TISSUE; ARTICLE; CONTROLLED STUDY; DERIVATIZATION; DOPING; EXTRACTION; GAS CHROMATOGRAPHY; HAIR; HUMAN; HUMAN TISSUE; INSTRUMENTATION; LIQUID; MEAT; NONHUMAN; PRIORITY JOURNAL; QUALITY CONTROL; SAMPLE; SOLID PHASE EXTRACTION; STANDARD; TANDEM MASS SPECTROMETRY; URINALYSIS;

ADULT; ANABOLIC AGENTS; ANIMALS; DOPING IN SPORTS; ESTERS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HAIR; HUMANS; MALE; MEAT; QUALITY CONTROL; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY;

EID: 0032747376     PISSN: 13872273     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0378-4347(99)00416-8     Document Type: Article

References (56)

1. Laure P. Santé Publique. 9:1997;145.
2. de Mondenard J.P. Dictionnaire des Substances et Procédés Dopants en Pratique Sportive. 1991;24 Masson, Paris.
3. Franke W.W., Berendonk B. Clin. Chem. 43:1997;1262.
4. de Mondenard J.P. Dictionnaire des Substances et Procédés Dopants en Pratique Sportive. 1991;25 Masson, Paris.
5. Berendonke B. Doping Dokumente. Von der Forschung zum Betrug. 1991;Springer-Verlag, Berlin.
6. Franke W.W. Funktion und Instrumentalisierung des Sports in der DDR. Pharmakologische Manipulationen (Doping) und die Rolle der Wissenschaft. Vol. III/2:1995;905 German Parliement Ed.
7. Höppner M. Technik. Stasi Report. Vol. II:1977;243.
8. Schäker W., Schubert K., Oettel M., Miedlich U., Gedrat J., Clausnitzer C., Bernstein B. Schäker W. Zur Anwendung von Steroidsubstanzen (STS) im Training und Tiereexperiment sowie zur Qualitätsprüfung der STS-Präparate. 1991;1 FSF, Leipzig.
9. Breo D.L. JAMA. 263:1990;1697.
10. Anonymous, Le Monde, August 15, 1998, p. 14.
11. Delbeke F.T. Int. J. Sports Med. 17:1996;434.
12. de Mondenard J.P. Dictionnaire des Substances et Procédés Dopants en Pratique Sportive. 1991;139 Masson, Paris.
13. Anonymous, France Soir, September 7, 1998, p. 2.
14. J.P. Bidet, L'Equipe, September 8, 1998, p. 3.
15. Y. Bordenave, Le Monde, October 8, 1998, p. 29.
16. Y. Bordenave, Le Monde, July 27, 1998, p. 15.
17. Epstein S.S. Int. J. Health Serv. 24:1994;145.
18. Epstein S.S. Int. J. Health Serv. 20:1990;277.
19. ème Congrès Internationale de Médecine Légale et Médecine Sociale de Langue Française, Lille :9-11 September 1998.
20. Debruykere G., VanPeteghem C.H., DeSagher R. Anal. Chim. Acta. 275:1993;49.
21. Gaillard Y., Doucet F., Balland A., Pépin G. J. Chromatogr. B. 703:1997;85.
22. Kicman A.T., Brooks V. J. Pharm. Biomed. Anal. 6:1988;473.
23. Reznik Y., Herrou M., Dehennin L., Lemaire M., Leymarie P. J. Clin. Endocrinol. Metab. 64:1987;1086.
24. Catlin D.H., Hatton C.K., Starcevic S.H. Clin. Chem. 43:1997;1280.
25. Chung B.C., Choo H.Y.P., Kim T.W., Eom K.D., Kwon O.S., Suh J., Yang J., Park J. J. Anal. Toxicol. 14:1990;105.
26. Gradeen C.Y., Shan S.C., Przybylski P.S. J. Anal. Toxicol. 14:1990;115.
27. DeBoer D., DeJong E.G., Maes R.A.A. J. Anal. Toxicol. 14:1990;117.
28. Munoz-Guerra J., Carreras D., Soriano C., Rodriguez C., Rodriguez A.F. J. Chromatogr. B. 704:1997;129.
29. Schanzer W., Delahaut P., Geyer H., Machnik M., Horning S. J. Chromatogr. B. 687:1996;93.
30. Mesner M.Z., Satzger R.D. J. Chromatogr. Sci. 35:1997;38.
31. Shackleton C.H.L., Chuang H., Kim J., DeLaTorre X., Segura J. Steroids. 62:1997;523.
32. Hold K.M., Wilkins D.G., Crouch D.J., Rollins D.E., Maes D.A. J. Anal. Toxicol. 20:1996;345.
33. Thieme D., Grosse J., Sachs H., Mueller R.K. Proceedings of the Manfred Donike 16th Cologne Workshop on Dope Analysis, Cologne :1998;9.
34. Kintz P. Toxicol. Lett. 102-103:1998;109.
35. Gleixner A., Meyer H.H.D. Fresenius J. Anal. Chem. 357:1997;1198.
36. Gleixner A., Meyer H.H.D. Int. Lab. July:1998;20.
37. Amendement No. 54 Rectifié Official Journal of the French Republic, Paris, No. 106. 16 November 1998;9230.
38. P. Marchand, D. Maume, M.P. Montrade, F. Monteau, B. LeBizec, F. André, Document LDH/LNR/98A, French Ministry of Agriculture.
39. Forensic Sci. Int. 84:1997;3.
40. Gaillard Y., Pépin G. J. Chromatogr. B. 709:1998;69.
41. Robbins C.R. Chemical and Physical Behavior of Human Hair. 1988;Springer, New York.
42. Bhathnagar V., Anjaiah S., Puri N., Ramaihah A. Arch. Biochem. Biophys. 307:1993;183.
43. Howells C., Godfrey M., Sauer M.S. Analyst. 119:1994;2691.
44. Leinonen A., Savonen L., Kuoppasalmi K. Proceedings of the Manfred Donike 12th Cologne Workshop on Dope Analysis, Cologne :1994;25.
45. Segura J., Ventura R., Jurado C. J. Chromatogr. B. 713:1998;61.
46. B. LeBizec, M.P. Montrade, F. André, Document DGAL/92-8065, French Ministry of Agriculture.
47. B. LeBizec, M.P. Montrade, F. André, Document DGAL/92-8066, French Ministry of Agriculture.
48. Draper N.R., Smith H. Applied Regression Analysis. 1988;Wiley, New York.
49. Miller J.N. Analyst. 116:1991;3.
50. Gaillard Y., Peyrefitte C., Cheminel V., Prévosto J.M., Chaulet J.F. Lyon Pharm. 46:1995;67.
51. Nix A.B.J., Wilson D.W. Eur. J. Clin. Pharmacol. 39:1990;203.
52. LeBizec B., Monteau F., Gaudin I., André F. J. Chromatogr. B. 723:1999;157.
53. Dehennin L., Bonnaire Y., Plou P. J. Chromatogr. B. 721:1999;301.
54. Kintz P., Cirimele V., Ludes B. Acta Clin. Belg. Suppl. 1:1999;68.
55. Voet W. Massacre à la Chaîne - Révélations sur 30 Ans de Tricheries. 1999;Calmann-Lévy, Paris.
56. Menthéour E. Secret Défonce - Ma Vérité sur le Dopage. 1999;J.C. Lattés, Paris.