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note
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Crystal data for compound 3: C12H43N6AlMo6O36, Fw=1450.11, Triclinic, space group P1, a=9.0495(18)A ? , b=10.513(2)A ? , c=12.124(2)A ? ,-=100.975(3)-,-=111.852(3)-,- =98.625(3)-, V=1019.6(4)A ? 3, Z=1, DCalcd=2.317Mgm-3,-=0.71073A ? , T=293(2) K, R1(wR2)=0.0335 (0.0919), Bruker Smart Apex-II CCD area detector, Mo-Ka radiation. The structure was solved by direct methods and refined on F2 by full-matrix least-squares methods using SHELXTL 97.
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