Homoleptic platinum(II) and palladium(II) organothiolates and phenylselenolates: Solvothermal synthesis, structural determination, optical properties, and single-source precursors for PdSe and PdS nanocrystals

Chemistry - An Asian Journal

Volumn 5, Issue 9, 2010, Pages 2062-2074

  Chui, Stephen Sin Yin ^a,b   Low, Kam Hung ^a,b   Lu, Jun ^a,b   Roy, V A L ^c   Chan, Sharon Lai Fung ^a,b   Che, Chi Ming ^a,b  

^a University Grants Committee   (Hong Kong)

^b UNIVERSITY OF HONG KONG   (Hong Kong)

^c CITY UNIVERSITY OF HONG KONG   (Hong Kong)

Author keywords

Chain structures; Optical band gaps; Powder X ray diffraction; Self assembly formation; Solvothermal synthesis

Indexed keywords

AMBIPOLAR; AMORPHOUS PRECIPITATE; CHAIN STRUCTURE; CHAIN-LIKE POLYMERS; CHAINLIKE STRUCTURE; CHARGE TRANSPORTING; CRYSTALLINE SOLIDS; DIFFUSE REFLECTANCE SPECTRUM; DROP-CAST; ELEMENTAL ANALYSIS; ETHANOLIC SOLUTION; HEXADECANETHIOL; HOMOLEPTIC; LAYER-LIKE STRUCTURES; OPTICAL BANDS; POLYMERIC CHAIN; POWDER X-RAY DIFFRACTION; SELF-ASSEMBLE; SINGLE-SOURCE PRECURSOR; SOLID SAMPLES; SOLVOTHERMAL CONDITIONS; SOLVOTHERMAL SYNTHESIS; SOLVOTHERMAL-ANNEALING; STRUCTURAL DETERMINATION; XPS; ZIG-ZAG;

BINDING ENERGY; COMPLEXATION; CRYSTALLINE MATERIALS; DIFFRACTION; ELECTRON MOBILITY; ENERGY GAP; FIELD EFFECT TRANSISTORS; FILM PREPARATION; HOLE MOBILITY; METAL IONS; NANOCRYSTALLINE POWDERS; NANOCRYSTALS; OPTICAL BAND GAPS; OPTICAL PROPERTIES; PALLADIUM; PLATINUM; PLATINUM COMPOUNDS; POLYMERS; POWDER METALS; SELF ASSEMBLY; SEMICONDUCTING SELENIUM COMPOUNDS; X RAY DIFFRACTION; X RAYS;

PALLADIUM COMPOUNDS;

EID: 77956454010     PISSN: 18614728     EISSN: 1861471X     Source Type: Journal    
DOI: 10.1002/asia.201000233     Document Type: Article

References (139)

1. For general reviews, see: a) P. J. Hagrman, D. Hagrman, J. Zubieta, Angew. Chem. 1999, 111, 2798-2848;
2. Angew. Chem. Int. Ed. 1999, 38, 2638-2684;
3. b) C. Janiak, Dalton Trans. 2003, 2781-2804;
4. c) A. Y. Robin, K. M. Fromm, Coord. Chem. Rev. 2006,250, 2127-2157
5. d) R. Robson, Dalton Trans. 2008, 5113-5131.
6. D. Schweitzer, S. Kahlich, S. Gaertner, E. Gogu, H. Grimm, I. Heinen, T. Klutz, R. Zamboni, H. J. Keller, G. Renner, NATO Adv. Study Inst. Ser. Ser. B 1990, 248, 97-114
7. b) C.T. Chen, K. S. Suslick, Coord. Chem. Rev. 1993, 128, 293-322
8. c) D.J. Cardin, Adv. Mater. 2002, 14, 553-563;
9. d) K. A. Williams, A.J. Boydston, C.W. Bielawski, Chem. Soc. Rev. 2007, 36, 729-744
10. For magnetic properties, see: e) S. R. Batten, K. S. Murray, Coord. Chem. Rev. 2003, 246, 103-130
11. f) D. Maspoch, D. Ruiz-Molina, J. Veciana, J. Mater. Chem. 2004,14, 2713-2723.
12. For non-linear optical and luminescent properties, see: a) Q. Ye, X. S. Wang, H. Zhao, R. G. Xiong, Chem. Soc. Rev. 2005, 34, 208-225
13. b) C. L. Cahill, D. T. de Lill, M. Frisch, CrystEngComm 2007, 9, 15-26
14. c) H. Zhao, Z. R. Qu, H.Y. Ye, R. G. Xiong, Chem. Soc. Rev. 2008, 37, 84-100.
15. For selective sorption properties, see: a) O. M. Yaghi, H. L. Li, C. Davis, D. Richardson, T. L. Groy, Acc. Chem. Res. 1998,31, 474-484
16. b) M. Eddaoudi, D. B. Moler, H. L. Li, B. L. Chen, T. M. Rein-eke, M. O'Keeffe, O. M. Yaghi, Acc. Chem. Res. 2001, 34, 319-330;
17. c) B. Kesanli, W. B. Lin, Coord. Chem. Rev. 2003,246, 305-326;
18. d) S. Kitagawa, R. Kitaura, S. I. Noro, Angew. Chem. 2004,116, 2388-2430
19. Angew. Chem. Int. Ed. 2004, 43, 2334-2375
20. e) U. Mueller, M. Schubert, F. Teich, H. Puetter, K. Schierle-Arndt, J. Pastré, J. Mater. Chem. 2006, 16, 626-636
21. For catalytic properties, see: f) Z. Wang, G. Chen, K. Ding, Chem. Rev. 2009,109, 322-359.
22. a) J. D. Ranford, J. J. Vittal, D. Wu, X. D. Yang, Angew. Chem. 1999, 111, 3707-3710
23. Angew. Chem. Int. Ed. 1999, 38, 3498-3501
24. b) B. Sreenivasulu, J.J. Vittal, Angew. Chem. 2004, 116, 5893-5896
25. Angew. Chem. Int. Ed. 2004, 43, 5769-5772
26. c) X. Zhang, Y. Xie, Q. Zhao, Y. Tian, New J. Chem. 2003, 27, 827-830
27. d) J. J. Vittal, M. T. Ng, Acc. Chem. Res. 2006,39, 869-877
28. e) W. L. Leong, S. K. Ba-tabyal, S. Kasapis, J. J. Vittal, Chem. Eur. J. 2008,14, 8822-8829.
29. J.J. Vittal, Coord. Chem. Rev. 2007, 251, 1781-1795 and references therein.
30. For CuI, see: a) M. Baumgartner, H. Schmalle, C. Baerlocher, J. Solid State Chem. 1993, 107, 63-75
31. b) P. Espinet, M. C. Lequerica, J. M. Martin-Alvarez, Chem. Eur. J. 1999, 5, 1982-1986
32. c) N. Sand-hyarani, T. Pradeep, J. Mater. Chem. 2001,11, 1294-1299
33. d) C. M. Che, C. H. Li, S. S. Y. Chui, V. A. L. Roy, K. H. Low, C. M. Che, Chem. Eur. J. 2008, 14, 2965-2975.
34. For AgI, see: a) I. G. Dance, Inorg. Chem. 1981,20, 1487-1492
35. b) K. L. Tang, X. J. Xie, L. Zhao, Y. H. Zhang, X. L. Jin, Eur. J. Inorg. Chem. 2004, 78-85
36. c) J. X. Chen, Q. F. Xu, Y. Zhang, Z. N. Chen, J. P. Lang, J. Organomet. Chem. 2004, 689, 1071-1077.
37. For Au1, see: a) I. Schröter, J. Strähle, Chem. Ber. 1991, 124, 2161-2164
38. b) W. Wojnowski, B. Becker, J. Sassmannhausen, E. M. Peters, K. Peters, H. G. Von Schnering, Z. Anorg. Allg. Chem. 1994,620, 1417-1421
39. c) M. R. Wiseman, P. A. Marsh, P.T. Bishop, B.J. Bris-don, M. F. Mahon, J. Am. Chem. Soc. 2000,122, 12598-12599
40. d) S. S. Y. Chui, R. Chen, C. M. Che, Angew. Chem. 2006,118, 1651-1654
41. Angew. Chem. Int. Ed. 2006, 45, 1621-1624.
42. a) D. Craig, I. G. Dance, R. G. Garbutt, Angew. Chem. 1986,98, 178-179
43. Angew. Chem. Int. Ed. Engl. 1986,25, 165-166
44. b) I. G. Dance, R. G. Garbutt, D. C. Craig, M. L. Scudder, Inorg. Chem. 1987,26, 4057-4064
45. c) I. G. Dance, R. G. Garbutt, D. C. Craig, M. L. Scudder, T. D. Bailey, Chem. Commun. 1987, 1164-1167.
46. a) W. Gaete, J. Ros, X. Solans, M. Font-Altaba, J. L. Brianso, Inorg. Chem. 1984, 23, 39-43
47. b) I. G. Dance, M. L. Scudder, R. Secomb, Inorg. Chem. 1985, 24, 1201-1208
48. c) S. A. Ivanov, M. A. Kozee, W. A. Merrill, S. Agarwal, L. F. Dahl, J. Chem. Soc. Dalton Trans. 2002, 4105-4115.
49. a) D. Sellmann, D. Häußinger, F. W. Heinemann, Eur. J. Inorg. Chem. 1999, 1715-1725
50. b) D. Sellmann, F. Geipel, F. W. Heine-mann, Eur. J. Inorg. Chem. 2000, 271-279.
51. a) N. R. Kunchur, Acta Crystallogr. Sect. B 1968,24, 1623-1633
52. b) J. D. Higgin III, J. W. Suggs, Inorg. Chim. Acta 1988,145, 247-252
53. c) I. Schneider, M. Horner, R. N. Olendzki, J. Strahle, Acta Crystallogr. Sect. C 1993,49, 2091-2093
54. d) P. J. Thomas, A. Lava-nya, V. Sabareesh, G. U. Kulkarni, Proc. Indian Acad. Sci. Chem. Sci. 2001, 113, 611-619
55. e) Z. Q. Yang, A. B. Smetana, C. M. Soren-sen, K. J. Klabunde, Inorg. Chem. 2007,46, 2427-2431.
56. a) S. Dey, V. K. Jain, A. Klein, W. Kaim, Inorg. Chem. Commun. 2004,7, 601-603
57. b) L. B. Kumbhare, V. K. Jain, P. P. Phadnis, M. Nethaji, J. Organomet. Chem. 2007, 692, 1546-1556.
58. a) F. G. Mann, D. Purdie, J. Chem. Soc. 1935, 1549-1563
59. b) R. G. Hayter, F. S. Humiec, J. Inorg. Nucl. Chem. 1964,26, 807-810
60. c) W. Beck, K. H. Stetter, S. Tadros, K. E. Schwarzhans, Chem. Ber. 1967,100, 3944-3954
61. d) M. E. Peach, J. Inorg. Nucl. Chem. 1973,35, 1046-1048.
62. a) L. Cattalini, J. S. Coe, S. Degetto, A. Dondoni, A. Vigato, Inorg. Chem. 1972, 11, 1519-1524
63. b) T. B. Rauchfuss, J. S. Shu, D. M. Roundhill, Inorg. Chem. 1976,15, 2096-2101.
64. a) S. C. Chan, M. C. W. Chan, Y. Wang, C. M. Che, K. K. Cheung, N. Y. Zhu, Chem. Eur. J. 2001,7, 4180-4190
65. b) W. Lu, B. X. Mi, M. C. W. Chan, Z. Hui, C. M. Che, N. Y. Zhu, S. T. Lee, J. Am. Chem. Soc. 2004,126, 4958-4971
66. c) W. Lu, V. A. L. Roy, C. M. Che, Chem. Commun. 2006, 3972-3974
67. d) Y. Sun, K. Ye, H. Zhang, J. Zhang, L. Zhao, B. Li, G. Yang, B. Yang, Y. Wang, S. W. Lai, C. M. Che, Angew. Chem. 2006,118, 5738-5741
68. Angew. Chem. Int. Ed. 2006,45, 5610-5613
69. e) C. M. Che, X. F. Xiang, S. S. Y. Chui, X. Z. Xu, V. A. L. Roy, J. J. Yan, W. F. Fu, P. T. Lai, I. D. Williams, Chem. Asian J. 2008,3, 1092-1103
70. f) M. Y. Yuen, V. A. L. Roy, W. Lu, S. C. F. Kui, G. S. M. Tong, M. H. So, S. S. Y. Chui, M. Muccini, J. Q. Ning, S. J. Xu, C. M. Che, Angew. Chem. 2008,120, 10043-10047
71. Angew. Chem. Int. Ed. 2008,47, 9895-9899.
72. a) I. Nakanishi, K. Matsumoto, S. Ooi, Acta Crystallogr. Sect. C 1991, 47, 2073-2076
73. b) G. Rivera, S. Bernes, C. Rodriguze de Barbarin, H. Torrens, Inorg. Chem. 2001,40, 5575-5580.
74. E. M. Padilla, C. M. Jensen, Polyhedron 1991,10, 89-93.
75. X. Ribas, J. C. Dias, J. Morgado, K. Wurst, M. Almeida, T. Parella, J. Veciana, C. Rovira, Angew. Chem. 2004,116, 4141-4144
76. Angew. Chem. Int. Ed. 2004,43, 4049-4052.
77. A. Eichhofer, P. T. Wood, R. Viswanath, R. A. Mole, Eur. J. Inorg. Chem. 2007, 4794-4799.
78. a) J. S. Lee, D. Freedman, J. H. Melman, T. J. Emge, F. H. Long, J. G. Brennan, Inorg. Chem. 1998,37, 2512-2519
79. b) M. C. Kuchta, A. L. Rheingold, G. Parkin, New J. Chem. 1999,23, 957-959.
80. S. A. Best, P. Brant, R. D. Feltham, T. B. Rauchfuss, D. M. Round-hill, R. A. Walton, Inorg. Chem. 1977,16, 1976-1979.
81. A. L. Spek, Private Communication, 2007.
82. a) P. Kubelka, F. Munk, Z. Tech. Phys. 1931, 12, 593-601
83. b) P. Ku-belka, J. Opt. Soc. Am. 1948, 38, 448-457
84. c) V. Kumar, S. Kr Sharma, T. P. Sharma, V. Singh, Opt. Mater. 1999,12, 115-119.
85. a) Z. Li, X. Li, P. Lin, S. Du, J. Cluster Sci. 2008,19, 357-366
86. b) Z. H. Li, L. H. Li, L. M. Wu, S. W. Du, Eur. J. Inorg. Chem. 2009, 752-759.
87. a) I. J. Ferrer, P. Diaz-Chao, A. Pascual, C. Sanchez, Thin Solid Films 2007,515, 5783-5786
88. b) P. Diaz-Chao, I. J. Ferrer, J. R. Ares, C. Sanchez, J. Phys. Chem. C 2009,113, 5329-5335.
89. J. Ren, W. Liang, M. H. Whangbo, Crystal and electronic structure analysis using CAESAR version 2.0. 1998. This program can be downloaded free of charge via the URL: http://www.primec.com.
90. a) A. C. Sutorik, J. Albritton-Thomas, C. R. Kannewurf, M. G. Ka-natzidis, J. Am. Chem. Soc. 1994, 116, 7706-7713
91. b) I. Tsuji, H. Kato, A. Kudo, Chem. Mater. 2006,18, 1969-1975.
92. A. Birri, B. Harvey, G. Hogarth, E. Subasi, F. Ugur, J. Organomet. Chem. 2007,692, 2448-2455.
93. A. Singhal, V. K. Jain, R. Mishra, B. Varghese, J. Mater. Chem. 2000,10, 1121-1124.
94. Z. Q. Yang, K. J. Klabunde, C. M. Sorensen, J. Phys. Chem. C 2007,111, 18143-18147.
95. A. Ghezelbash, M. B., Jr. Sigman, B. A. Korgel, Nano Lett. 2004,4, 537-542.
96. J. Zaumseil, R. H. Friend, H. Sirringhaus, Nat. Mater. 2006,5, 69-74.
97. S. M. Sze, Physics of Semiconductor Devices, Wiley, New York, 1981.
98. a) X. C. Huang, J. P. Zhang, Y. Y. Lin, X. L. Yu, X. M. Chen, Chem. Commun. 2004, 1100-1101
99. b) B. Ding, L. Yi, P. Cheng, D. Z. Liao, S. P. Yan, Inorg. Chem. 2006, 45, 5799-5803
100. c) J. He, Y. G. Yin, T. Wu, D. Li, X. C. Huang, Chem. Commun. 2006, 2845-2847
101. d) S. Z. Zhan, M. Li, J. Z. Hou, J. Ni, D. Li, X. C. Huang, Chem. Eur. J. 2008, 14, 8916-8921.
102. J. P. Zhang, Y. Y. Lin, X. C. Huang, X. M. Chen, J. Am. Chem. Soc. 2005, 127, 5495-5506.
103. a) G. Demazeau, J. Mater. Chem. 1999, 9, 15-18
104. b) X. Y. Liu, M. S. Mo, J. H. Zeng, Y. T. Qian, J. Cryst. Growth J. Crystal Growth 2003, 259, 144-148
105. c) X. F. Wang, X. Q. Liu, L. F. Lai, S. Y. Li, J. Wang, Z. M. Zhou, Q. Cui, X. Chen, M. Y. Cao, Q. Q. Zhang, Adv. Funct. Mater. 2008, 18, 1809-1823.
106. Handbook of Chalcogen Chemistry. New Perspectives in Sulfur, Selenium and Tellurium (Ed.: F. A. Devillanova), RSC Publishing 2007, Chap. 2.1, 33-57.
107. a) K. Ruhlandt-Senge, Inorg. Chem. 1995, 34, 3499-3504
108. b) R. Hauptmann, R. Kliss, G. Henkel, Angew. Chem. 1999, 111, 389-391
109. Angew. Chem. Int. Ed. 1999, 38, 377-379.
110. a) D. Coucouvanis, D. Swenson, N. C. Baenziger, C. Murphy, D. G. Holah, N. Sfarnas, A. Simopoulos, A. Kostikas, J. Am. Chem. Soc. 1981, 103, 3350-3362
111. b) N. Ueyama, T. Sugawara, K. Sasaki, A. Nakamura, S. Yamashita, Y. Wakatsuki, H. Yamazaki, N. Yasuoka, Inorg. Chem. 1988, 27, 741-747
112. c) A. L. Rheingold, K. S. Beall, P. J. Riggs, S. E. Groh, Acta Crystallogr. Sect. C 1993,49, 542-543.
113. J. T. Kim, J. W. Park, S. M. Koo, Polyhedron 2000,19, 1139-1143.
114. a) I. L. Abrahams, C. D. Garner, W. Clegg, J. Chem. Soc. Dalton Trans. 1987, 1577-1579
115. b) H. O. Stephan, K. Griesar, W. Haase, G. Henkel, Z. Naturforsch. B 1994, 49, 1620-1632.
116. a) I. G. Dance, J. Am. Chem. Soc. 1979,101, 6264-6273
117. b) K. S. Hagen, D. W. Stephan, R. H. Holm, Inorg. Chem. 1982,21, 3928-3936
118. c) K. S. Hagen, R. H. Holm, Inorg. Chem. 1983,22, 3171-3174
119. d) T. Costa, J. R. Dorfman, K. S. Hagen, R. H. Holm, Inorg. Chem. 1983,22, 4091-4099
120. e) J. L. Hencher, M. A. Khan, F. F. Said, D. G. Tuck, Polyhedron 1985,4, 1263-1267.
121. a) D. Ohlmann, H. Pritzkow, H. Grutzmacher, M. Anthamatten, R. Glaser, Chem. Commun. 1995, 1011-1012
122. b) D. Fenske, A. Fischer, Angew. Chem. 1995, 107, 340-342
123. Angew. Chem. Int. Ed. Engl. 1995,34, 307-309.
124. K. S. Anjali, J. J. Vittal, Inorg. Chem. Commun. 2000, 3, 708-710.
125. R. Shen, R. Xu, H. Liu, Cryst. Growth Des. 2009,9, 3504-3508.
126. A. Ajayaghosh, Chem. Soc. Rev. 2003, 32, 181-191.
127. a) F. Gronvold, H. Haraldsen, A. Kjekshus, Acta Chem. Scand. 1960, 14, 1879-1893
128. b) A. Kjekshus, Acta Chem. Scand. 1961, 15, 159-168
129. c) S. Soled, A. Wold, O. Gorochov, Mater. Res. Bull. 1976,11, 927-932
130. d) W. Bronger, R. Rennau, D. Schmitz, Z. Anorg. Allg. Chem. 1991,597, 27-32.
131. a) K. M. Fromm, E. D. Gueneau, A. Y. Robin, W. Maudez, J. Sague, R. Bergougnant, Z. Anorg. Allg. Chem. 2005, 631, 1725-1740
132. b) M. Veith, Z. Phys. Chem. 2008,222, 287-305.
133. a) A. Boultif, D. Louer, J. Appl. Crystallogr. 2004, 37, 724-731;
134. b) G. S. Pawley, J. Appl. Crystallogr. 1981,14, 357-361
135. c) A. Alto-mare, R. Caliandro, M. Camalli, C. Cuocci, C. Giacovazzo, A. G. G. Moliterni, R. Rizzi, J. Appl. Crystallogr. 2004,37, 1025-1028
136. d) W. I. F. David, K. Shankland, J. van de Streek, E. Pidcock, W. D. S. Motherwell, J. C. Cole, J. Appl. Crystallogr. 2006,39, 910-915
137. e) G. M. Sheldrick, SHELX-97 Programs for Crystal Structure Analysis (Release 97-2). University of Göttingen, Germany, 1997
138. f) EXPGUI, a graphical user interface for GSAS, B. H. Toby, J. Appl. Crystallogr. 2001, 34, 210-221
139. g) A. C. Larson, R. B. Von Dreele, General Structure Analysis System (GSAS), Report LAUR 86-748, 2004.