A rapid direct solvent extraction method for the extraction of 2-dodecylcyclobutanone from irradiated ground beef patties using acetonitrile

Journal of Food Science

Volumn 75, Issue 6, 2010, Pages

  Hijaz, Faraj ^a   Kumar, Amit ^a   Smith, J Scott ^a  

^a KANSAS STATE UNIVERSITY   (United States)

Author keywords

2 alkylcyclobutanone; 2 DCB; Food irradiation; Radiation; Radiolytic markers

Indexed keywords

2 DODECYLCYCLOBUTANONE; 2-DODECYLCYCLOBUTANONE; ACETONITRILE; ACETONITRILE DERIVATIVE; BIOLOGICAL MARKER; CYCLOBUTANE DERIVATIVE; SOLVENT;

ANIMAL; ARTICLE; CATTLE; CHEMISTRY; COMPARATIVE STUDY; FOOD CONTROL; FOOD IRRADIATION; ISOLATION AND PURIFICATION; MASS FRAGMENTOGRAPHY; MEAT; METHODOLOGY; RADIATION EXPOSURE; REPRODUCIBILITY; TIME;

ACETONITRILES; ANIMALS; BIOLOGICAL MARKERS; CATTLE; CYCLOBUTANES; FOOD INSPECTION; FOOD IRRADIATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; MEAT; REPRODUCIBILITY OF RESULTS; SOLVENTS; TIME FACTORS;

EID: 77955786581     PISSN: 00221147     EISSN: 17503841     Source Type: Journal    
DOI: 10.1111/j.1750-3841.2010.01706.x     Document Type: Article

References (18)

1. Boyd DR, Crone AVJ, Hamilton JTG, Hand MV, Stevenson MH, Stevenson PJ. Synthesis, characterization, and potential use of 2-dodecylcyclobutanone as a marker for irradiated chicken. J Agric Food Chem 1991, 39(4):789-92.
2. The detection of irradiated foods containing fat- gas chromatography/mass spectrometric analysis of 2-alkylcyclobutanone 2003, 1-20. British and European Standard (BS EN 1785), London, British Standards Institution, p
3. Diehl JF. Achievement in food irradiation during the 20th century. Irradiation for food safety and quality 2001, 1-16. Loaharanu PThomas P. In, editors, Lancaster, Pa., Technomic, p
4. Elliott CT, Hamilton L, Stevenson MH, McCaughey WJ, Boyd D. Detection of irradiated chicken meat by analysis of lipid extracts for 2-substituted cyclobutanones using an enzyme-linked-immunosorbent-assay. Analyst 1995, 120(9):2337-41.
5. Gadgil P, Hachmeister KA, Smith JS, Kropf DH. 2-Alkyl-cyclobutanones as irradiation dose indicators in irradiated ground beef patties. J Agric Food Chem 2002, 50(20):5746-50.
6. Gadgil P, Smith JS, Hachmeister KA, Kropf DH. Evaluation of 2-dodecylcyclobutanone as an irradiation dose indicator in fresh irradiated ground beef. J Agric Food Chem 2005, 53(6):1890-93.
7. Gupta MN, Batra R, Tyagi R, Sharma A. Polarity index: the guiding solvent parameter for enzyme stability in aqueous-organic cosolvent mixtures. Biotechnol Prog 1997, 13(3):284-8.
8. Horvatovich P, Miesch M, Hasselmann C, Marchioni E. Supercritical fluid extraction of hydrocarbons and 2-alkylcyclobutanones for the detection of irradiated foodstuffs. J Chromatogr A 2000, 897(1-2):259-68.
9. Le Tellier MH, Nawar WW. 2-alkylcyclobutanones from the radiolysis of triglycerides. Lipids 1972, 7:73-6.
10. Molins RA. Food irradiation principles and applications 2001, 1-21. New York, Wiley, p
11. Ndiaye B, Jamet G, Miesch M, Hasselmann C, Marchioni E. 2-alkylcyclobutanones as markers for irradiated foodstuffs II. The CEN (European Committee for Standardization) method: field of application and limit of utilization. Radiat Phys Chem 1999, 55(4):437-45.
12. Obana H, Furuta M, Tanaka Y. Analysis of 2-alkylcyclobutanones with accelerated solvent extraction to detect irradiated meat and fish. J Agric Food Chem 2005, 53(17):6603-608.
13. Obana H, Furuta M, Tanaka Y. Detection of irradiated meat, fish and their products by measuring 2-alkylcyclobutanones levels after frozen storage. J Food Hyg Soci Japan 2007, 48(6):203-206.
14. Sommers CH, Delincée H, Smith JS, Marchioni E. Toxicological safety of irradiated foods. Food irradiation research and technology 2006, 127-42. Sommers CH, Fan X, In, editors, 1st ed, Ames, Iowa, Blackwell Pub, p
15. Tewfik I. A rapid direct solvent extraction method for the extraction of cyclobutanones from irradiated chicken and liquid whole egg. Int J Food Sci Technol 2008a, 43(1):108-13.
16. Tewfik I. Extraction and identification of cyclobutanones from irradiated cheese employing a rapid direct solvent extraction method. Int J Food Sci Nutr 2008b, 59(7-8):590-98.
17. Tewfik I. Inter-laboratory trial to validate the direct solvent extraction method for the identification of 2-dodecylcyclobutanone in irradiated chicken and whole liquid egg. Food Sci Technol Int 2008c, 14(3):277-83.
18. Tewfik IH, Ismail HM, Sumar S. A rapid supercritical fluid extraction method for the qualitative detection of 2-alkylcyclobutanones in gamma-irradiated fresh and sea water fish. Int J Food Sci Nutr 1999, 50(1):51-6.