Physico-chemical analysis of five hard bitumens: Identification of chemical species and molecular organization before and after artificial aging

Fuel

Volumn 89, Issue 11, 2010, Pages 3330-3339

  Le Guern, M ^a   Chailleux, E ^a   Farcas, F ^b   Dreessen, S ^c   Mabille, I ^d  

^a Laboratoire Centrale de Ponts et Chausées   (France)

^b Lab Central des Ponts et Chaussees   (France)

^c TOTAL   (France)

^d PSL RESEARCH UNIVERSITY   (France)

Author keywords

Asphaltene structure; Bitumen; Size exclusion chromatography

Indexed keywords

AGING EFFECTS; ARTIFICIAL AGING; ASPHALTENE CONTENT; BEFORE AND AFTER; BITUMEN; CHEMICAL SPECIES; FLAME IONIZATION DETECTORS; FTIR SPECTROSCOPY; HIGH-SPEED; IATROSCAN; MODIFIED BITUMEN; MOLECULAR ORGANIZATION; N-HEPTANES; PHYSICO-CHEMICALS; POLYPHOSPHORIC ACIDS; PRESSURE AGING VESSEL; THIN LAYERS;

AGGLOMERATION; ASPHALTENES; BITUMINOUS MATERIALS; CHEMICALS; CRUDE OIL; DIFFERENTIAL SCANNING CALORIMETRY; FOURIER TRANSFORM INFRARED SPECTROSCOPY; GEL PERMEATION CHROMATOGRAPHY; HEPTANE; HYDRAULIC STRUCTURES; IONIZATION OF LIQUIDS; ORGANIC POLYMERS; PETROLEUM REFINING; RESINS; SILICA; SILICA GEL;

SIZE EXCLUSION CHROMATOGRAPHY;

EID: 77955468442     PISSN: 00162361     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.fuel.2010.04.035     Document Type: Article

References (54)

1. J.G. Speight The chemistry and technology of petroleum 3rd ed. 1999 Marcel Dekker New York
2. L.W. Corbett Composition of asphalt based on generic fractionation, using solvent deasphaltening, elution-adsorption chromatography and densimetric characterization Anal Chem 41 1969 576 579
3. F.J. Nellensteyn The constitution of asphalt J Inst Petrol Technol 10 1924 311 325
4. J.P. Pfeiffer, and R.N.J. Saal Asphaltic bitumen as colloid systems J Phys Chem 44 1940 139 149
5. Yen TF. Present status of the structure of petroleum heavy ends and its significance to various technical applications. Preprints of ACS symposium on advances in analysis of petroleum and its products, vol. 17; 1972. p. 102-14.
6. J.-F. Masson, V. Leblond, and J. Margeson Bitumen morphologies by phase-detection atomic force microscopy J Microsc 221 2006 17 29
7. J.-F. Masson, V. Leblond, J. Margeson, and S. Bundalo-Perc Low-temperature bitumen stiffness and viscous paraffinic nano and micro-domains by cryogenic AFM and PDM J Microsc 227 2007 191 202
8. Petersen JC, Robertson RE, Branthaver JF, Harnsberger PM, Duvall JJ, Kim SS, et al. Binder characterization and evaluation, vol. 1. SHRP report A-367. Washington, DC: National Research Council; 1994.
9. Christensen DW, Anderson DA. Rheological evidence concerning the molecular architecture of asphalt cements. In: Proceedings chemistry of bitumen, vol. 2. Rome: 1991. p. 568-95.
10. Redelius P. The structure of asphaltenes in bitumen. Road Mater Pavement Des 2006;143-62 [special issue EATA 2006].
11. C.Y. Cheung, and D. Cebon Deformation mechanisms of pure bitumen J Mater Civil Eng 9 1997 117 129
12. D. Lesueur, J.-F. Gérard, P. Claudy, J.-M. Létoffé, J.-P. Planche, and D. Martin A structure-related model to describe asphalt linear viscoelasticity J Rheol 40 1996 813 836
13. J.M. Krishnan, and K.R. Rajagopal Review of the uses and modeling of bitumen from ancient to modern times Appl Mech Rev 56 2003 149 214
14. J.M. Krishnan, and K.R. Rajagopal On the mechanical behavior of asphalt Mech Mater 37 2005 1085 1100
15. C. Gaestel, R. Smadja, and K.A. Lamminan Contribution la connaissance des propriétés des bitumes routiers Revue Générale des Routes et Aérodromes 466 1971 85 97
16. K. Baginska, and I. Gawel Effect of origin and technology on the chemical composition and colloidal stability of bitumens Fuel Process Technol 85 2004 1453 1462
17. B. Brûlé, G. Ramond, and C. Such Relations composition-structure-propriété des bitumes routiers. Etat des recherches au LCPC Bulletin de Liaison des Laboratoires des Ponts et Chaussées 148 1987 69 81
18. J.P. Planche, P.M. Claudy, J.M. Létoffé, and D. Martin Using thermal analysis methods to better understand asphalt rheology Thermochim Acta 324 1998 223 227
19. Edwards Y, Isacsson U. Wax in bitumen part 2 - characterization and effects. Road Mater Pavement Des 2005;6(4):439-68. (Pubitemid 44954155)
20. J.-F. Masson, G.M. Polomark, and P. Collins Time-dependent microstructure of bitumen and its fractions by modulated differential scanning calorimetry Energy and Fuels 16 2002 470 476
21. J. Lamontagne, P. Dumas, V. Mouillet, and J. Kister Comparison by FTIR spectroscopy of different ageing techniques: application to road bitumens Fuel 80 2001 483 488
22. N. Pieri, J.P. Planche, and J. Kister Caractérisation structurale des bitumes routiers par IRTF et fluorescence UV en mode excitation- émission synchrones Analysis 24 1996 113 122
23. U. Bergmann, O.C. Mullins, and S.P. Cramer X-ray Raman spectroscopy of carbon in asphaltene: light element characterization with bulk sensitivity Anal Chem 72 2000 2609 2612
24. L. Michon, D. Martin, J.-P. Planche, and B. Hanquet Estimation of average structural parameters of bitumens by 13C nuclear magnetic resonance spectroscopy Fuel 76 1 1997 9 15
25. T.F. Yen The colloidal aspect of a macrostructure of petroleum asphalt Fuel Sci Technol Int 10 1992 723 733
26. F. Migliori, and J.-F. Corte Comparative study of RTFOT and PAV aging simulation laboratory tests Transport Res Record 1638 1998 56 63
27. J.-F. Masson, T. Price, and P. Collins Dynamics of Bitumen fractions by thin-layer chromatography/flame ionization detection Energy Fuels 15 2001 955 960
28. J.C. Petersen Quantitative functional group analysis of asphalts using differential infrared spectrometry and selective chemical reactions: theory and application Transport Res Record 1096 1986 1 11
29. Morgan P, Mulder A. The shell bitumen industrial handbook. Shell Bitumen; 1995.
30. X. Lu, and U. Isacsson Effect of ageing on bitumen chemistry and rheology Construct Build Mater 16 2002 15 22
31. N. Pieri, J.-P. Planche, and J. Kister Caractérisation structurale des bitumes routiers par IRTF et Fluorescence UV en mode excitation-emission synchrones Analusis 24 1996 113 122
32. V. Mouillet, F. Farcas, and S. Besson Ageing by UV radiation of an elastomer modified bitumen Fuel 87 2008 2408 2419
33. Brûlé B, Planche JP, King GP, Claudy P, Letoffe JM. Relationships between characterization of asphalt cements by differential scanning calorimetry and their physical properties, vol. 37. American Chemical Society, Division of Petroleum Chemistry; 1990. p. 330-7 [Preprints].
34. D. Lesueur, J.-P. Planche, and P. Dumas Détermination de la teneur en paraffines des bitumes Bulletin des Laboratories des ponts et chaussées 229 2000 3 11
35. J.-F. Masson, G.M. Polomark, and P. Collins Steric hardening and the ordering of asphaltenes in bitumen Energy Fuels 19 2005 120 122
36. Rosset R, Caude M, Jardy A. Chromatographies en phases liquide et supercritique. Masson; 1991. p. 632.
37. Jennings PW. High Pressure liquid chromatography as a method of measuring asphalt composition. Report no. FHWA-MT-7930. Bozeman, Mt.: Dept. of Chemistry, Montana St. Univ.; 1980.
38. K.W. Kim, and J.L. Burati Use of GPC chromatogram to characterize aged asphalt cement J Mater Civil Eng, ASCE 5 1993 41 52
39. Lee Soon-Jae, Amirkhanian Serji N, Kim Kwang W. Laboratory evaluation of the effects of short-term oven aging on asphalt binders in asphalt mixtures using HP-GPC. Construct Build Mater 2009.
40. Coll H. Behavior of micellar solutions in gel permeation chromatography. A theory based on a simple model. In: Altgelt KH, Segal L, editors. Gel permeation chromatography. Marcel Publisher; 1971. p. 329-37.
41. Farcas F. Etude d'une méthode de vieillissement sur route des bitumes. Thesis at Paris VI University; 1996.
42. H.A. Broadhurst, and P.W. Rein Deconvolution of GPC chromatograms of sugar solutions Zuckerindustrie 128 2 2003 96 99
43. Baumgardner GL, Masson J-F, Hardee JR, Menapace AM, Williams AG. Polyphosphoric acid modified asphalt: proposed mechanisms. In: Proceedings of the association of asphalt technologists; 2005. p. 283-305.
44. Masson J-F. Brief review of the chemistry of polyphosphoric acid (PPA) and bitumen. Energy Fuels 2008;22(4):2637-40 [erratum p. 3560].
45. J.-F. Masson, and M. Gagné Ionic pairs in polyphosphoric acid (PPA)-modified bitumen: insights from model compounds Energy Fuels 22 5 2008 3390 3394
46. J.-F. Masson, and M. Gagné Polyphosphoric acid (PPA)-modified bitumen: disruption of the asphaltenes network based on the reaction of nonbasic nitrogen with PPA Energy Fuels 22 5 2008 3402 3406
47. J.-F. Masson, M. Gagné, G. Robertson, and P. Collins Reactions of polyphosphoric acid and bitumen model compounds with oxygenated functional groups: where is the phosphorylation Energy Fuels 22 6 2008 4151 4157
48. J.-F. Masson, and P. Collins FTIR study of the reaction of polyphosphoric acid and model bitumen sulfur compounds Energy Fuels 23 1 2009 440 442
49. J.-F. Masson, P. Collins, J.R. Woods, S. Bundalo-Perc, and J. Margeson Chemistry and effects of polyphosphoric acid on the microstructure, molecular mass, glass transition temperatures and performance grades of asphalts Journal AAPT 78 2009 456 484
50. Corbett LW. Manufacture of petroleum asphalt. In: Hoiberg A, editor. Bituminous materials: asphalts, tars and pitches, vol. 2. Interscience Publishers; 1979. p. 81-122.
51. L.W. Corbett, and R.E. Swarbrick Composition analysis used to explore asphalt hardening Process Assoc Asphalt Paving Technol 29 1960 104 112
52. S.E. Moschopedis, and J.G. Speight The effect of air blowing on the properties and constitution of a natural bitumen J Mater Sci 12 1977 990 998
53. Orange G, Dupuis D, Martin JV, Farcas F, Such C, Marcant B. Chemical modification of bitumen trough polyphosphoric acid: properties - microstructure relationship. In: Third Eurasphalt and Eurobitume congress, Vienna; 2004.
54. Torres J, González JM, Peralta X. Correlation between the fractionation of bitumen according to the methods ASTM D-4124 and IATROSCAN, Eurobitumen, Stockholm; 1993.