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Volumn 13, Issue 9, 2010, Pages 1043-1046

Two 2D inorganic-organic hybrid materials constructed from (V 2O6)n2n- chains linked through metal-organic units [Cd(ip)]/[Ni(ip)(H2O)]

Author keywords

Cadmium; Inorganic organic hybrid materials; Layered materials; Nickel; Vanadium oxide

Indexed keywords


EID: 77955413102     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.06.006     Document Type: Article
Times cited : (11)

References (37)
  • 35
    • 77955422686 scopus 로고    scopus 로고
    • note
    • 2O. Anal. Calcd for compound 2 (%): C, 30.45; H, 2.36; N, 10.93. Found: C, 30.53; H, 2.31; N, 10.96.
  • 36
    • 77955429253 scopus 로고    scopus 로고
    • note
    • - 1, F(000) = 1016, crystal size 0.20 × 0.20 × 0.10 mm, green, prism, T = 293 K. Final R1 = 0.0386, wR2 = 0.0917, and S = 1.036 with 3795 parameters for 12768 reflections with I > 2σ(I). The data were collected on a Rigaku Mercury CCD diffractometer with graphite-monochromatized Mo Kα radiation (λ = 0.71073 Å) and ω scan mode. The structures were solved by direct methods and refined by the full-matrix least squares fitting on F2 by SHELXTL-97. All of non-hydrogen atoms were refined anisotropic. The coordinated water H atoms in 2 were located in a difference Fourier map and refined with restrained O-H distances approximately equal to 0.84(1) Å and H...H distances approximately equal to 1.44(1) Å. The isolated water H atoms were not added. All hydrogen atoms of the organic ligands were generated geometrically (C-H, 0.96 Å; N-H, 0.86 Å).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.