Experimental comparison of measurement techniques for drop size distributions in liquid/liquid dispersions

Experiments in Fluids

Volumn 50, Issue 2, 2011, Pages 259-269

  Maass S ^a   Wollny, S ^b   Voigt, A ^c   Kraume, M ^a  

^a TECHNISCHE UNIVERSITÄT BERLIN   (Germany)

^b ANHALT UNIVERSITY OF APPLIED SCIENCES   (Germany)

^c OTTO VON GUERICKE UNIVERSITY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ANALYSIS RESULTS; DROP SIZE; DROP SIZE DISTRIBUTION; EXACT RESULTS; EXPERIMENTAL COMPARISON; FIBER-OPTICAL; IN-SITU; LIQUID/LIQUID DISPERSION; LIQUID/LIQUID SYSTEMS; MEASUREMENT PRINCIPLE; ON-LINE MEASUREMENT; ON-LINE MEASUREMENT TECHNIQUE; OPTICAL REFLECTANCE; POWER INPUT; REFLECTANCE MEASUREMENTS; SIZE ANALYSIS; SMOOTH SURFACE; STIRRED TANK REACTORS;

BACKSCATTERING; DROPS; MEASUREMENTS; PROBES; REFLECTION; REFLECTOMETERS; SENSORS; SIZE DETERMINATION; SIZE DISTRIBUTION;

MEASUREMENT ERRORS;

EID: 77955273960     PISSN: 07234864     EISSN: None     Source Type: Journal    
DOI: 10.1007/s00348-010-0918-9     Document Type: Article

References (38)

1. C Andrès P Réginault MH Rochat B Chaillot Y Pourcelot 1996 Particle-size distribution of a powder: comparison of three analytical techniques Int J Pharm 144 2 141 146 10.1016/S0378-5173(96)04737-0 (Pubitemid 27043030)
2. JH Bae LL Tavlarides 1989 Laser capillary spectrophotometry for drop-size concentration measurements AIChE J 35 7 1073 1084 10.1002/aic.690350703
3. P Barrett B Glennon 2002 Characterizing the metastable zone width and solubility curve using lasentec FBRM and PVM Chem Eng Res Des 80 A7 799 805 10.1205/026387602320776876 (Pubitemid 35436892)
4. BP Binks 2002 Particles as surfactants-similarities and differences Curr Opin Colloid Interface Sci 7 1-2 21 41 10.1016/S1359-0294(02)00008-0 (Pubitemid 34601086)
5. JA Boxall CA Koh ED Sloan AK Sum DT Wu 2010 Measurement and calibration of droplet size distributions in water-in-oil emulsions by particle video microscope and a focused beam reflectance method Ind Eng Chem Res 49 3 1412 1418 10.1021/ie901228e
6. A Bürkholz R Polke 1984 Laser diffraction spectrometers/experience in particle size analysis Part Charact 1 153 160 10.1002/ppsc.19840010126
7. P Chylek JT Kiehl MKW Ko 1978 Narrow resonance structure in Mie scattering characteristics Appl Opt 17 19 3019 3021 10.1364/AO.17.003019
8. SG Cull JW Lovick GJ Lye P Angeli 2002 Scale-down studies on the hydrodynamics of two-liquid phase biocatalytic reactors Bioprocess Biosyst Eng 25 3 143 153 10.1007/s00449-002-0281-1
9. C Desnoyer O Masbernat C Gourdon 2003 Experimental study of drop size distributions at high phase ratio in liquid-liquid dispersions Chem Eng Sci 58 7 1353 1363 10.1016/S0009-2509(02)00461-X (Pubitemid 36364175)
10. CO Fournier L Fradette PA Tanguy 2009 Effect of dispersed phase viscosity on solid-stabilized emulsions Chem Eng Res Des 87 4A 499 506 10.1016/j.cherd.2008.11.008
11. Fricke M, Voigt A, Sundmacher K (2007) Droplet size distribution of technical macroemulsions: variation of process parameters. In: Proceedings of International Congress for Particle Technology, Nuremberg, 27-29 March 2007, 4 pp
12. A Gäbler M Wegener AR Paschedag M Kraume 2006 The effect of pH on experimental and simulation results of transient drop size distributions in stirred liquid-liquid dispersions Chem Eng Sci 61 9 3018 3024 10.1016/j.ces.2005.10.072 (Pubitemid 43277406)
13. D Greaves J Boxall J Mulligan A Montesi J Creek ED Sloan CA Koh 2008 Measuring the particle size of a known distribution using the focused beam reflectance measurement technique Chem Eng Sci 63 22 5410 5419 10.1016/j.ces.2008.07.023
14. KJ Hay ZC Liu TJ Hanratty 1998 A backlighted imaging technique for particle size measurements in two-phase flows Exp Fluids 25 3 226 232 10.1007/s003480050225 (Pubitemid 128663096)
15. AR Heath PD Fawell PA Bahri JD Swift 2002 Estimating average particle size by focused beam reflectance measurement (FBRM) Part Part Syst Char 19 2 84 95 10.1002/1521-4117(200205)19:2<84::AID-PPSC84>3.0.CO;2-1 (Pubitemid 34638801)
16. B Hu P Angeli OK Matar CJ Lawrence GF Hewitt 2006 Evaluation of drop size distribution from chord length measurements AIChE J 52 3 931 939 10.1002/aic.10714
17. ET Hurlburt TJ Hanratty 2002 Measurement of drop size in horizontal annular flow with the immersion method Exp Fluids 32 6 692 699
18. N Kail W Marquardt H Briesen 2009 Process analysis by means of focused beam reflectance measurements Ind Eng Chem Res 48 6 2936 2946 10.1021/ie800839s
19. M Kraume A Gäbler K Schulze 2004 Influence of physical properties on drop size distributions of stirred liquid-liquid dispersions Chem Eng Technol 27 3 330 334 10.1002/ceat.200402006 (Pubitemid 38498305)
20. MZ Li D Wilkinson 2005 Determination of non-spherical particle size distribution from chord length measurements. Part 1: theoretical analysis Chem Eng Sci 60 12 3251 3265 10.1016/j.ces.2005.01.008 (Pubitemid 40554192)
21. MZ Li D Wilkinson K Patchigolla 2005 Comparison of particle size distributions measured using different techniques Part Sci Technol 23 3 265 284 1110.65100 10.1080/02726350590955912 (Pubitemid 41025747)
22. J Lovick AA Mouza SV Paras GJ Lye P Angeli 2005 Drop size distribution in highly concentrated liquid-liquid dispersions using a light back scattering method J Chem Tech Biotech 80 5 545 552 10.1002/jctb.1205 (Pubitemid 40601683)
23. C Martinez-Bazan JL Montanes JC Lasheras 1999 On the breakup of an air bubble injected into a fully developed turbulent flow. Part 1. Breakup frequency J Fluid Mech 401 157 182 0974.76087 10.1017/S0022112099006680 (Pubitemid 129657826)
24. KA McDonald AP Jackman S Hurst 2001 Characterization of plant suspension cultures using the focused beam reflectance technique Biotechnol Lett 23 4 317 324 10.1023/A:1005646826204 (Pubitemid 32162620)
25. Misek T, Berger R, Schröter J (1985) Standard test systems for liquid extraction, 2nd edn. EFCE Publications, Series 43
26. AM O'Rourke PF MacLoughlin 2005 A comparison of measurement techniques used in the analysis of evolving liquid-liquid dispersions Chem Eng Process 44 8 885 894 10.1016/j.cep.2004.10.001 (Pubitemid 40419436)
27. AW Pacek AW Nienow 1995 Measurement of drop size distribution in concentrated liquid-liquid dispersions-video and capillary techniques Chem Eng Res Des 73 A5 512 518
28. AW Pacek IPT Moore AW Nienow RV Calabrese 1994 Video technique for measuring dynamics of liquid-liquid dispersion during phase inversion AIChE J 40 12 1940 1949 10.1002/aic.690401203 (Pubitemid 287757)
29. Ritter J (2002) Dispergierung und Phasentrennung in gerührten Flüssig/flüssig-Systemen. Ph.D. Thesis, Technische Universität Berlin, 169 pp (in German)
30. J Ritter M Kraume 2000 On-line measurement technique for drop size distributions in liquid/liquid systems at high dispersed phase fractions Chem Eng Technol 23 7 579 582 10.1002/1521-4125(200007)23:7<579::AID-CEAT579>3. 0.CO;2-Y
31. A Ruf J Worlitschek M Mazzotti 2000 Modeling and experimental analysis of PSD measurements through FBRM Part Part Syst Char 17 4 167 179 10.1002/1521-4117(200012)17:4<167::AID-PPSC167>3.0.CO;2-T (Pubitemid 32138799)
32. Sachweh B, Heffels C, Polke R, Rädle M (1998) Light scattering sensor for in-line measurements of mean particle sizes in suspensions. In: Proceedings of 7th European Symposium Particle Characteristics, Nuremberg, pp 635-644
33. MJH Simmons SH Zaidi BJ Azzopardi 2000 Comparison of laser-based drop-size measurement techniques and their application to dispersed liquid-liquid pipe flow Opt Eng 39 2 505 509 10.1117/1.602388 (Pubitemid 30589627)
34. A Tadayyon S Rohani 1998 Determination of particle size distribution by Par-Tec (R) 100: modeling and experimental results Part Part Syst Char 15 3 127 135 10.1002/(SICI)1521-4117(199817)15:3<127::AID-PPSC127>3.0.CO;2-B (Pubitemid 128508503)
35. van de Hulst HC (1981) Light scattering by small particles-structure of matter series. Dover Publications, New York, p 470
36. Wollny S, Sperling R, Heun G, Ritter J, Maa S, Kraume M (2008) Bestimmung von Tropfengröenverteilungen zur Charakterisierung von Rührorganen hinsichtlich der Partikelbeanspruchung. In: Proceedings of ProcessNet Partikelmesstechnik, München, 10-14 March 2008, 2 pp (in German)
37. J Worlitschek T Hocker M Mazzotti 2005 Restoration of PSD from chord length distribution data using the method of projections onto convex sets Part Part Syst Char 22 2 81 98 10.1002/ppsc.200400872 (Pubitemid 41411974)
38. ZQ Yu PS Chow RBH Tan 2008 Interpretation of focused beam reflectance measurement (FBRM) data via simulated crystallization Org Process Res Dev 12 4 646 654 10.1021/op800063n