Minor crops for export: A case study of boscalid, pyraclostrobin, lufenuron and lambda-cyhalothrin residue levels on green beans and spring onions in Egypt

Journal of Environmental Science and Health - Part B Pesticides, Food Contaminants, and Agricultural Wastes

Volumn 45, Issue 6, 2010, Pages 493-500

  Hanafi, Ahmad ^a   Garau, Vincenzo L ^b   Caboni, Pier Luigi ^b   Sarais, Giorgia ^b   Cabras, Paolo ^b  

^a AIN SHAMS UNIVERSITY   (Egypt)

^b UNIVERSITY OF CAGLIARI   (Italy)

Author keywords

cyhalothrin; Boscalid; Gas chromatography nitrogen phosphorus detector (GC NPD); Green beans; High performance liquid chromatography electrospray ionization source mass spectrometry (HPLC ESI MS); Lufenuron; Pyraclostrobin; Spring onions

Indexed keywords

ELECTROSPRAY IONIZATION SOURCES; GREEN BEANS; HPLC-ESI MS; LUFENURON; NITROGEN-PHOSPHORUS DETECTORS; SPRING ONION;

AMIDES; CROPS; ELECTROSPRAY IONIZATION; GAS CHROMATOGRAPHY; IONIZATION OF GASES; LIQUIDS; MASS SPECTROMETRY; PARTICLE DETECTORS; PESTICIDES; PHOSPHORUS; PRODUCT DEVELOPMENT; UREA;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

2 CHLORO N (4 CHLOROBIPHENYL 2 YL)NICOTINAMIDE; 2-CHLORO-N-(4-CHLOROBIPHENYL-2-YL)NICOTINAMIDE; BENZAMIDE DERIVATIVE; BIPHENYL DERIVATIVE; CARBAMIC ACID DERIVATIVE; CYHALOTHRIN; DRUG DERIVATIVE; FLUPHENACUR; NICOTINAMIDE; NITRILE; PESTICIDE RESIDUE; PYRACHLOSTROBIN; PYRAZOLE DERIVATIVE; PYRETHROID; LUFENURON;

BIOACCUMULATION; DISSIPATION; IONIZATION; LEGUME; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PESTICIDE; PESTICIDE RESIDUE; VEGETABLE;

ARTICLE; CHEMISTRY; FOOD CONTAMINATION; HALF LIFE TIME; LEGUME; ONION; ANALOGS AND DERIVATIVES; ANALYSIS; FABACEAE;

BENZAMIDES; BIPHENYL COMPOUNDS; CARBAMATES; FABACEAE; FOOD CONTAMINATION; HALF-LIFE; NIACINAMIDE; NITRILES; ONIONS; PESTICIDE RESIDUES; PYRAZOLES; PYRETHRINS;

ALLIUM CEPA; TRIFLUORO;

EID: 77953954302     PISSN: 03601234     EISSN: 15324109     Source Type: Journal    
DOI: 10.1080/03601234.2010.493466     Document Type: Article

References (20)

1. Horticultural Export Improvement Association (HEIA). HEIA newsletter, 2003, 22, July/September 2003, Cairo, HEIA, Egypt.
2. Food and Agriculture Organization of the United Nations (FAO). Crops and livestock products. FAO: Rome, 2009. Available from: http://faostat.fao.org/site/535/DesktopDefault.aspx?PageID=535 accessed July 2009
3. Food and Agriculture organization of the United Nations (FAO). Statistics, 2004. Production Yearbook 2003, FAO: Rome, 2003, Vol. 57.
4. Wijnands, J. The impact on the Netherlands of Egyptian greenhouse vegetable chain, Report 5.04.10; Agricultural Economics Research Institute (LEI): The Hague, Netherlands. 2004.
5. EU-Pesticides Database. Active Substances (Directive91/414/EEC); EU-Pesticide MRLs (Regulation (EC) No396/2005). 2009. [cited 2009 July 20]. Available from: http://ec.europa.eu/sanco_pesticides/public/index.cfm. (accessed July2009).
6. Barba, A.; Camara, M.A.; Navarro Garcia, S.; Sanchez-Fresneda, C.; Lopez de Hierro, N.; Acebes, A. Disappearance of bromopropy-late residues in artichokes, strawberries and beans. J. Environ. Sci.Health, Part B, 1991, 26, 323-332.
7. Castillo-Sanchez, J.; Aguilera-del Real, A.; Rodriguez-Sanchez, M.; Valverde-Garcia, A. Residue levels, decline curves and plantationdistribution of procymidone in green beans grown in green-house. J. Agric. Food Chem. 2000, 48, 2991-2994.
8. Gil Garcia, M.D.; Martinez Vidal, J.L.; Rodriguez Torreblanca, C.; Gonzalez, C. Determination and degradation of methomyl intomatoes and green beans in greenhouses. J. AOAC Int. 1997, 80,633-638.
9. Talebi, K.; Ghassami, M.R. Residues of profenofos in spring onion.Commun. Agric. Appl. Biol. Sci. 2004, 69, 799-802.
10. Commission Decision 2002/657/EC of 12 August 2002, Imple-menting Council Directive (EC) 96/23 concerning the performanceof analytical methods and the interpretation of the results (text withEEA relevance), Off. J. Eur. Commun. L221, 2002.
11. De Melo Abreu, S.; Correia, M.; Herbert, P.; Santos, L.; Alves, A. Screening of grapes and wine for azoxystrobin, kresoxim-methyland trifloxystrobin fungicides by HPLC with diode array detection. Food Addit. Contam. 2005, 22, 549-556.
12. De Melo Abreu, S.; Caboni, P.L.; Cabras, P.; Garau, V.L.; Alves, A. Validation and global uncertainty of a liquid chromatographic withdiode array detection method for the screening of azoxystrobin, kresoxim-methyl, trifloxystrobin, famoxadone, pyraclostrobin andfenamidone in grapes and wine. Anal. Chim. Acta, 2006, 573-574,291-297.
13. Miliadis, G.E.; Tsiropoulos, N.G.; Aplada-Sarlisa, P.G. High-performance liquid chromatographic determination of benzoy-lurea insecticides residues in grapes and wine using liq-uid and solid-phase extraction. J. Chromatogr. A. 1999, 835,113-120.
14. Silva, M.G.D.; Aquino, A.; Dórea, H.S.; Navickiene, S. Simulta-neous determination of eight pesticide residues in coconut usingMSPD and GC/MS. Talanta 2008, 76, 680-684.
15. Liu, X.; Dong, F.; Qin, D.; Zheng, Y. Residue analysis ofkresoxim-methyl and boscalid in fruits, vegetables and soil usingliquid-liquid extraction and gas chromatography-mass spectrome-try. Biomed Chromatogr. 2009, Aug 2 (Epub ahead of print; DOI:10.1002/bmc.1301)
16. González-Rodríguez, R.M.; Cancho-Grande, B.; Simal-Gándara, J. Multiresidue determination of 11 new fungicides in grapes andwines by liquid-liquid extraction/clean-up and programmable tem-perature vaporization injection with analyte protectants/gas chro-matography/ion trap mass spectrometry. J Chromatogr A, 2009, 1216,6033-42.
17. Pang, G.F.; Cao, Y.Z.; Fan, C.L.; Zhang, J.J.; Li, X.M. Multiresiduegas chromatographic method for determining synthetic pyrethroidpesticides in agricultural products: collaborative study. J AOAC Int. 1999, 82,186-212.
18. Beltran, J.; Peruga, A.; Pitarch, E.; López, F.J.; Hernández, F. Application of solid-phase microextraction for the determination ofpyrethroid residues in vegetable samples by GC-MS. Anal. Bioanal.Chem. 2003, 376, 502-511.
19. Lehotay, S.J. Determination of pesticide residues in foodsby acetonitrile extraction and partitioning with magnesiumsulphate: collaborative study. J AOAC Int. 2007, 90, 485-520.
20. Cho, S.K.; Abd El-Aty, A.M.; Choi, J.H.; Jeong, Y.M.; Shin, H.C.; Chang, B.J.; Lee, C.; Shim, J.H. Effectiveness of pressurized liquid extraction and solvent extraction for the simultaneous quantification of 14 pesticide residues in green tea using GC. J. Sep. Sci. 2008,31,1750-1760.